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1. 发明授权

US08450261B2 Cleaning compositions with monocarboxylic acid monomers dicarboxylic monomers, and monomers comprising sulfonic acid groups 有权
标题翻译：用单羧酸单体二羧酸单体和包含磺酸基团的单体的清洁组合物
公开(公告)号：US08450261B2
公开(公告)日：2013-05-28
申请号：US12741461
申请日：2008-10-31
申请人： Masato Nakano , Takahiro Tsumori
发明人： Masato Nakano , Takahiro Tsumori
IPC分类号： C11D3/378 , C11D1/72 , C11D3/2075 , C11D3/326 , C11D3/386 , C11D3/50
CPC分类号： C11D3/378 , C08F2/10 , C08F220/04 , C08F220/38 , C08F222/02
摘要： Laundry detergents or cleaning compositions which comprises a copolymer composition comprising i) a copolymer having a weight-average molecular weight of from about 10,000 to about 50,000 and comprising a) 30-60 mol% structural units derived from monoethylenically unsaturated dicarboxylic acid or dicarboxylate; b) structural units derived from monoethylenically unsaturated monocarboxylic acid or monocarboxylate; c) structural units derived from monomers containing sulfonic acid or sulfonate groups and having no ester bonds or amido bonds; and ii) 10,000 ppm or less of residual monoethylenically unsaturated dicarboxylic acid or dicarboxylate monomer.
摘要翻译：洗涤剂或清洁组合物，其包含共聚物组合物，其包含i）重均分子量为约10,000至约50,000的共聚物，并且包含a）30-60mol％衍生自单烯属不饱和二羧酸或二羧酸酯的结构单元; b）衍生自单烯属不饱和一元羧酸或单羧酸酯的结构单元; c）衍生自含有磺酸或磺酸酯基并且不具有酯键或酰胺键的单体的结构单元; 和ii）10,000ppm或更少的残余单烯属不饱和二羧酸或二羧酸酯单体。

2. 发明申请

US20090198029A1 N-VINYL CYCLIC LACTAM POLYMER, PRODUCTION METHOD THEREOF, AND APPLICATION THEREOF 审中-公开
标题翻译： N-乙烯基环状乳液聚合物，其生产方法及其应用
公开(公告)号：US20090198029A1
公开(公告)日：2009-08-06
申请号：US11915590
申请日：2006-05-26
申请人： Takahiro Tsumori , Daisuke Imai , Yoshikazu Fujii
发明人： Takahiro Tsumori , Daisuke Imai , Yoshikazu Fujii
IPC分类号： C08F4/30 , C08F26/06
CPC分类号： C08F271/02 , C11D3/3776
摘要： To provide: an N-vinyl cyclic lactam polymer, which has excellent dispersibility and adsorptivity, and high calcium-ion capturing capability and can be preferably used in, for example, a detergent additive application; an application thereof; and a production method of the N-vinyl cyclic lactam polymer, the production method being capable of efficiently producing such an N-vinyl cyclic lactam polymer. An N-vinyl cyclic lactam polymer produced by a polymerization of a monomer component containing a carboxyl group-containing unsaturated monomer with a polymer having an N-vinyl cyclic lactam unit, wherein the carboxyl group-containing unsaturated monomer is 200 to 9900 parts by weight, relative to 100 parts by weight of the polymer having an N-vinyl cyclic lactam unit, and the N-vinyl cyclic lactam polymer has a viscosity at 25° C. of 100000 mPa·s or less in an aqueous solution with a solid content of 25% by weight.
摘要翻译：提供：分散性和吸附性优异，钙离子捕获能力高的N-乙烯基环状内酰胺聚合物，优选用于例如洗涤剂添加剂用途中。其应用; 以及N-乙烯基环内酰胺聚合物的制造方法，该制造方法能够有效地制造这种N-乙烯基环状内酰胺类聚合物。通过含有含羧基的不饱和单体的单体组分与具有N-乙烯基环状内酰胺单元的聚合物的聚合制备的N-乙烯基环状内酰胺聚合物，其中含羧基的不饱和单体为200〜9900重量份相对于100重量份的具有N-乙烯基环内酰胺单元的聚合物，N-乙烯基环内酰胺聚合物在固体含量的水溶液中的25℃下的粘度为100000mPa.s以下为25重量％。

3. 发明申请

US20070021313A1 Water-soluble amphoteric copolymer, production method thereof, and application thereof 有权
标题翻译：水溶性两性共聚物及其制备方法及其应用
公开(公告)号：US20070021313A1
公开(公告)日：2007-01-25
申请号：US11481965
申请日：2006-07-07
申请人： Daisuke Hattori , Takahiro Tsumori , Yoshikazu Fujii
发明人： Daisuke Hattori , Takahiro Tsumori , Yoshikazu Fujii
IPC分类号： C11D3/02
CPC分类号： C08L33/14 , C08L33/24 , C11D3/3723 , C08L2666/04
摘要： To provide: a water-soluble amphoteric copolymer having excellent hydrophilicity and high adsorption capability, and capable of exhibiting dramatically excellent dispersibility even under high hardness conditions and being preferably used in a detergent composition application, for example; an application thereof; and a production method of such a water-soluble amphoteric copolymer. A water-soluble amphoteric copolymer produced by a copolymerization of a monomer component comprising a cationic monomer (a), an anionic monomer (b), and an unsaturated polyalkylene glycol monomer (c), wherein the monomer (b) is a carboxyl group-containing monomer and/or a sulfonic acid group-containing monomer (d), and the monomer (b) is more than 50% by mole relative to 100% by mole of a total amount of the monomers (a), (b), and (c) if the monomer (b) consists of the carboxyl-group containing monomer, and at least one species of monomer among the monomers (a), (d), and (c) is 30% by mole or less relative to 100% by mole of a total amount of the monomers (a), (d), and (c) if the monomer (b) comprises the sulfonic acid group-containing monomer (d).
摘要翻译：提供：具有优异的亲水性和高吸附能力的水溶性两性共聚物，即使在高硬度条件下也能显示出显着优异的分散性，并且优选用于洗涤剂组合物应用中; 其应用; 以及这种水溶性两性共聚物的制造方法。通过使包含阳离子单体（a），阴离子单体（b）和不饱和聚亚烷基二醇单体（c）的单体组分共聚制备的水溶性两性共聚物，其中单体（b）是羧基 - 含有单体和/或含磺酸基的单体（d），单体（b）相对于单体（a），（b），（b）的总量相对于100摩尔％大于50摩尔％（c）如果单体（b）由含羧基的单体组成，并且单体（a），（d）和（c）中的至少一种单体相对于如果单体（b）包含含磺酸基的单体（d），则单体（a），（d）和（c）的总量为100摩尔％。

4. 发明授权

US08389458B2 Automatic dishwashing composition containing a sulfonated copolymer 有权
标题翻译：含有磺化共聚物的自动洗碗组合物
公开(公告)号：US08389458B2
公开(公告)日：2013-03-05
申请号：US12863844
申请日：2009-03-27
申请人： Takahiro Tsumori , Masato Nakano
发明人： Takahiro Tsumori , Masato Nakano
IPC分类号： C11D3/37 , C11D3/33
CPC分类号： C11D3/2086 , C08J3/14 , C08L33/00 , C08L33/14 , C08L35/00 , C08L41/00 , C11D3/33 , C11D3/34 , C11D3/3757 , C11D3/378 , C11D3/3902 , C11D3/3942 , C11D3/3947 , C11D7/265 , C11D7/34 , C08L2666/04
摘要： An ADW composition comprising a builder and a water-soluble copolymer which comprises: (a) from about 30 to 60 mol % of the copolymer having a structural unit originating from a monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer having 4 to 6 carbon atoms or its anhydride at; (b) from about 30 to 60 mol % of the copolymer having a structural unit originating from a monoethylenic unsaturated monocarboxylic acid (or monocarboxylate) monomer having 3 to 8 carbon atoms; and (c) from about 5 to 15 mol % of the polymer having a structural unit originating from a monoethylenic unsaturated monomer having a sulfonic (or sulfonate) group; wherein the water-soluble copolymer has a weight average molecular weight of from about 1,000 to about 50,000 wherein the copolymer is polymerized with hydrogen peroxide.
摘要翻译：一种包含助洗剂和水溶性共聚物的ADW组合物，其包含：（a）约30至60摩尔％的具有来自具有4-6个碳原子的单烯属不饱和二羧酸（或二羧酸酯）单体的结构单元的共聚物或其酸酐在（b）具有来自具有3-8个碳原子的单烯属不饱和一元羧酸（或单羧酸酯）单体的结构单元的共聚物的约30至60摩尔％和（c）约5至15摩尔％的具有源自具有磺酸（或磺酸盐）基团的单烯属不饱和单体的结构单元的聚合物; 其中所述水溶性共聚物的重均分子量为约1,000至约50,000，其中所述共聚物与过氧化氢聚合。

5. 发明授权

US07906595B2 Hydrophilic graft polymer 有权
标题翻译：亲水性接枝聚合物
公开(公告)号：US07906595B2
公开(公告)日：2011-03-15
申请号：US12375824
申请日：2007-08-07
申请人： Takahiro Tsumori , Norihiro Wakao
发明人： Takahiro Tsumori , Norihiro Wakao
IPC分类号： C08F283/06
CPC分类号： C08F283/06 , C08F6/006 , C11D3/3788 , D06M15/263 , D06M15/27 , D06M15/53 , D06P1/525 , D06P1/6138 , C08L51/08 , C08F220/08 , C08F220/06
摘要： A hydrophilic graft polymer having the reducing amount of the residual unsaturated monocarboxylic acid, and having very excellent temporal stability is provided.The present invention relates to the hydrophilic graft polymer obtained by graft polymerization of monomer component containing unsaturated monocarboxylic acid onto polyalkylene oxide, wherein mole ratio of side chain moiety derived from the unsaturated monocarboxylic acid is more than 90% by mole relative to total side chain, and residual amount of unsaturated monocarboxylic acid is less than 200 ppm by mass relative to the total mass of said hydrophilic graft polymer.
摘要翻译：提供了具有还原量的残余不饱和单羧酸并且具有非常优异的时间稳定性的亲水性接枝聚合物。本发明涉及通过将含有不饱和一元羧酸的单体组分接枝聚合到聚环氧烷上获得的亲水性接枝聚合物，其中衍生自不饱和一元羧酸的侧链部分的摩尔比相对于总侧链大于90摩尔％相对于所述亲水接枝聚合物的总质量，不饱和一元羧酸的残留量小于200质量ppm。

6. 发明申请

US20070049710A1 Continuous production method of water-soluble polymer and water-soluble polymer 有权
标题翻译：水溶性聚合物和水溶性聚合物的连续制备方法
公开(公告)号：US20070049710A1
公开(公告)日：2007-03-01
申请号：US11512284
申请日：2006-08-30
申请人： Hidekazu Kozuki , Noboru Sakamoto , Takahiro Tsumori , Atsuro Yoneda , Kaori Nakatani , Hideo Wakami
发明人： Hidekazu Kozuki , Noboru Sakamoto , Takahiro Tsumori , Atsuro Yoneda , Kaori Nakatani , Hideo Wakami
IPC分类号： C08F2/00
CPC分类号： C08F2/00 , B01J14/00 , B01J19/0013 , B01J2219/0011 , B01J2219/00123 , C08F220/06
摘要： To provide a continuous production method for producing a water-soluble polymer with a narrow molecular weight distribution with high efficiency. A continuous production method of a water-soluble polymer, comprising the steps of: circulating a circulation liquid containing a monomer having a polymerizable unsaturated bond through a reaction apparatus: having a tank and a circulation line comprising a piping circulating outside the tank, and thereby producing a water-soluble polymer continuously; and discharging part of the circulation liquid from a discharge line, wherein the circulation line is provided with a cooling device at least at one position.
摘要翻译：提供具有高效率的分子量分布窄的水溶性聚合物的连续制造方法。一种水溶性聚合物的连续制造方法，其特征在于，包括以下步骤：使具有聚合性不饱和键的单体的循环液通过反应装置循环，所述反应装置具有罐和循环管线，所述循环管路包括在罐外循环的管道，连续生产水溶性聚合物; 以及从排出管排出所述循环液的一部分，其中所述循环管线至少在一个位置处设置有冷却装置。

7. 发明授权

US07132487B2 (Meth) acrylic acid type polymer and unsaturated polyalkylene glycol type copolymer, and methods for production thereof 有权
标题翻译：（甲基）丙烯酸型聚合物和不饱和聚亚烷基二醇型共聚物及其制备方法
公开(公告)号：US07132487B2
公开(公告)日：2006-11-07
申请号：US11216772
申请日：2005-08-31
申请人： Atsuro Yoneda , Takahiro Tsumori , Yoshikazu Fujii , Shigeru Yamaguchi
发明人： Atsuro Yoneda , Takahiro Tsumori , Yoshikazu Fujii , Shigeru Yamaguchi
IPC分类号： C08F2/00
CPC分类号： C08F20/06 , C08F290/062
摘要： This invention concerns a (meth)acrylic acid type polymer, wherein the value S representing the quantity of an sulfur element introduced which is defined by the formula, S=(quantity of S contained in polymer)/(total quantity of S)×100, is not less than 35. This (meth) acrylic acid type polymer is a water-soluble polymer of a low molecular weight which has only a small impurity content, entails no precipitation of an impurity during the preservation at a low temperature, and excels in dispersibility, chelating ability, and an anti-gelling property.
摘要翻译：本发明涉及一种（甲基）丙烯酸型聚合物，其中代表由式S =（聚合物中所含的S的量）/（S的总量）×100所定义的引入的硫元素的量的值S，不小于35.这种（甲基）丙烯酸类聚合物是低分子量的水溶性聚合物，其杂质含量小，在低温保存期间不会产生杂质沉淀，并且在分散性，螯合能力和抗胶凝性。

8. 发明申请

US20060004162A1 (Meth) acrylic acid type polymer and unsaturated polyalkylene glycol type copolymer, and methods for production thereof 有权
公开(公告)号：US20060004162A1
公开(公告)日：2006-01-05
申请号：US11216772
申请日：2005-08-31
申请人： Atsuro Yoneda , Takahiro Tsumori , Yoshikazu Fujii , Shigeru Yamaguchi
发明人： Atsuro Yoneda , Takahiro Tsumori , Yoshikazu Fujii , Shigeru Yamaguchi
IPC分类号： C08F2/00
CPC分类号： C08F20/06 , C08F290/062
摘要： This invention concerns a (meth)acrylic acid type polymer, wherein the value S representing the quantity of an sulfur element introduced which is defined by the formula, S=(quantity of S contained in polymer)/(total quantity of S)×100, is not less than 35. This (meth) acrylic acid type polymer is a water-soluble polymer of a low molecular weight which has only a small impurity content, entails no precipitation of an impurity during the preservation at a low temperature, and excels in dispersibility, chelating ability, and an anti-gelling property.

9. 发明申请

US20050032999A1 Water-soluble copolymer 审中-公开
标题翻译：水溶性共聚物
公开(公告)号：US20050032999A1
公开(公告)日：2005-02-10
申请号：US10889012
申请日：2004-07-13
申请人： Takahiro Tsumori , Daisuke Hattori , Shigeru Yamaguchi
发明人： Takahiro Tsumori , Daisuke Hattori , Shigeru Yamaguchi
IPC分类号： B01F17/52 , C08F220/06 , C08F222/00 , C08F222/02 , C11D3/37 , C08F20/06
CPC分类号： C08F220/06 , C08F222/02 , C11D3/3757
摘要： An object of the present invention is to provide a three-monomer-based water-soluble copolymer, obtained from an unsaturated monocarboxylic monomer, an unsaturated dicarboxylic monomer, and an unsaturated alcoholic monomer, wherein the water-soluble copolymer can sufficiently exercise excellent performances particularly when used for detergent builders, detergent compositions, water-treating agents, and dispersants. As a means of achieving this object, the water-soluble copolymer according to the present invention has: an unsaturated alcoholic monomer-derived structural unit content of 0.1 to 40 weight % (but not including 40 weight %); and a product of not less than 200 of the calcium-ion-binding ability and the clay dispersibility (which is measured in an aqueous solution having a calcium ion content of 50 ppm in terms of calcium carbonate) under conditions of solid component content=40 weight % and pH=7.5.
摘要翻译：本发明的目的是提供一种由不饱和单羧酸单体，不饱和二羧酸单体和不饱和醇单体得到的三单体型水溶性共聚物，其中水溶性共聚物可以充分地运用优异的性能当用于洗涤剂助洗剂，洗涤剂组合物，水处理剂和分散剂时。作为实现该目的的手段，本发明的水溶性共聚物具有：不饱和醇单体衍生的结构单元含量为0.1〜40重量％（但不包含40重量％）。并且在固体成分含量= 40的条件下，钙离子结合能力和粘土分散性（以碳酸钙计，钙离子含量为50ppm的水溶液中测定）不小于200的产物重量％，pH = 7.5。

10. 发明申请

US20110172459A1 MANUFACTURING METHOD FOR SULFONIC ACID GROUP-CONTAINING ETHER COMPOUND 有权
标题翻译：含硫酸基团化合物的制备方法
公开(公告)号：US20110172459A1
公开(公告)日：2011-07-14
申请号：US13063563
申请日：2009-09-14
申请人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
发明人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
IPC分类号： C07C309/20 , C07C303/20
CPC分类号： C07C309/20 , C07C303/02 , C07C309/09 , C08F216/1466
摘要： The present invention provides a method for efficiently producing a sulfonic acid group-containing ether compound having a high purity and a good polymerizability while preventing production of a byproduct, and provides a sulfonic acid group-containing ether compound containing fewer impurities and having a good radical (co)polymerizability.The present invention provides a method of producing a sulfonic acid group-containing ether compound by reacting a sulfurous acid compound with a compound represented by the formula (1): wherein R1 represents a single bond, a CH2 group, or a CH2CH2 group, and R2 represents H, or a CH3 group, the method comprising the steps of: adjusting pH of a reaction system to 5.5 or greater with use of an alkaline substance; and adding the compound represented by the formula (1) to a reaction vessel containing the sulfurous acid compound.
摘要翻译：本发明提供了一种有效地制备具有高纯度和良好的聚合性同时防止副产物生成的含磺酸基的醚化合物的方法，并且提供了含少量杂质和具有良好基团的含磺酸基的醚化合物（共）聚合性。本发明提供一种通过使亚硫酸化合物与式（1）表示的化合物反应制备含磺酸基醚化合物的方法：其中R1表示单键，CH2基或CH2CH2基，和 R 2表示H或CH 3基团，该方法包括以下步骤：使用碱性物质将反应体系的pH调节至5.5以上; 并将由式（1）表示的化合物加入到含有亚硫酸化合物的反应容器中。

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