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1. 发明授权

US08450261B2 Cleaning compositions with monocarboxylic acid monomers dicarboxylic monomers, and monomers comprising sulfonic acid groups 有权
标题翻译：用单羧酸单体二羧酸单体和包含磺酸基团的单体的清洁组合物
公开(公告)号：US08450261B2
公开(公告)日：2013-05-28
申请号：US12741461
申请日：2008-10-31
申请人： Masato Nakano , Takahiro Tsumori
发明人： Masato Nakano , Takahiro Tsumori
IPC分类号： C11D3/378 , C11D1/72 , C11D3/2075 , C11D3/326 , C11D3/386 , C11D3/50
CPC分类号： C11D3/378 , C08F2/10 , C08F220/04 , C08F220/38 , C08F222/02
摘要： Laundry detergents or cleaning compositions which comprises a copolymer composition comprising i) a copolymer having a weight-average molecular weight of from about 10,000 to about 50,000 and comprising a) 30-60 mol% structural units derived from monoethylenically unsaturated dicarboxylic acid or dicarboxylate; b) structural units derived from monoethylenically unsaturated monocarboxylic acid or monocarboxylate; c) structural units derived from monomers containing sulfonic acid or sulfonate groups and having no ester bonds or amido bonds; and ii) 10,000 ppm or less of residual monoethylenically unsaturated dicarboxylic acid or dicarboxylate monomer.
摘要翻译：洗涤剂或清洁组合物，其包含共聚物组合物，其包含i）重均分子量为约10,000至约50,000的共聚物，并且包含a）30-60mol％衍生自单烯属不饱和二羧酸或二羧酸酯的结构单元; b）衍生自单烯属不饱和一元羧酸或单羧酸酯的结构单元; c）衍生自含有磺酸或磺酸酯基并且不具有酯键或酰胺键的单体的结构单元; 和ii）10,000ppm或更少的残余单烯属不饱和二羧酸或二羧酸酯单体。

2. 发明申请

US20110172459A1 MANUFACTURING METHOD FOR SULFONIC ACID GROUP-CONTAINING ETHER COMPOUND 有权
标题翻译：含硫酸基团化合物的制备方法
公开(公告)号：US20110172459A1
公开(公告)日：2011-07-14
申请号：US13063563
申请日：2009-09-14
申请人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
发明人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
IPC分类号： C07C309/20 , C07C303/20
CPC分类号： C07C309/20 , C07C303/02 , C07C309/09 , C08F216/1466
摘要： The present invention provides a method for efficiently producing a sulfonic acid group-containing ether compound having a high purity and a good polymerizability while preventing production of a byproduct, and provides a sulfonic acid group-containing ether compound containing fewer impurities and having a good radical (co)polymerizability.The present invention provides a method of producing a sulfonic acid group-containing ether compound by reacting a sulfurous acid compound with a compound represented by the formula (1): wherein R1 represents a single bond, a CH2 group, or a CH2CH2 group, and R2 represents H, or a CH3 group, the method comprising the steps of: adjusting pH of a reaction system to 5.5 or greater with use of an alkaline substance; and adding the compound represented by the formula (1) to a reaction vessel containing the sulfurous acid compound.
摘要翻译：本发明提供了一种有效地制备具有高纯度和良好的聚合性同时防止副产物生成的含磺酸基的醚化合物的方法，并且提供了含少量杂质和具有良好基团的含磺酸基的醚化合物（共）聚合性。本发明提供一种通过使亚硫酸化合物与式（1）表示的化合物反应制备含磺酸基醚化合物的方法：其中R1表示单键，CH2基或CH2CH2基，和 R 2表示H或CH 3基团，该方法包括以下步骤：使用碱性物质将反应体系的pH调节至5.5以上; 并将由式（1）表示的化合物加入到含有亚硫酸化合物的反应容器中。

3. 发明申请

US20100275396A1 CLEANING COMPOSITIONS WITH MONOCARBOXYLIC ACID MONOMERS DICARBOXYLIC MONOMERS, AND MONOMERS COMPRISING SULFONIC ACID GROUPS 有权
标题翻译：用单羧酸单体二羧酸单体和包含磺酸基团的单体的清洁组合物
公开(公告)号：US20100275396A1
公开(公告)日：2010-11-04
申请号：US12741461
申请日：2008-10-31
申请人： Masato Nakano , Takahiro Tsumori
发明人： Masato Nakano , Takahiro Tsumori
IPC分类号： C11D3/37 , C11D3/60 , C11D7/42 , C08F228/02 , A47L25/00
CPC分类号： C11D3/378 , C08F2/10 , C08F220/04 , C08F220/38 , C08F222/02
摘要： Laundry detergents or cleaning compositions which comprises a copolymer composition comprising i) a copolymer having a weight-average molecular weight of from about 10,000 to about 50,000 and comprising a) 30-60 mol % structural units derived from monoethylenically unsaturated dicarboxylic acid or dicarboxylate; b) structural units derived from monoethylenically unsaturated monocarboxylic acid or monocarboxylate; c) structural units derived from monomers containing sulfonic acid or sulfonate groups and having no ester bonds or amido bonds; and ii) 10,000 ppm or less of residual monoethylenically unsaturated dicarboxylic acid or dicarboxylate monomer.
摘要翻译：洗涤剂或清洁组合物，其包含共聚物组合物，其包含i）重均分子量为约10,000至约50,000的共聚物，并且包含a）30-60mol％衍生自单烯属不饱和二羧酸或二羧酸酯的结构单元; b）衍生自单烯属不饱和一元羧酸或单羧酸酯的结构单元; c）衍生自含有磺酸或磺酸酯基并且不具有酯键或酰氨基的单体的结构单元; 和ii）10,000ppm或更少的残余单烯属不饱和二羧酸或二羧酸酯单体。

4. 发明授权

US08389458B2 Automatic dishwashing composition containing a sulfonated copolymer 有权
标题翻译：含有磺化共聚物的自动洗碗组合物
公开(公告)号：US08389458B2
公开(公告)日：2013-03-05
申请号：US12863844
申请日：2009-03-27
申请人： Takahiro Tsumori , Masato Nakano
发明人： Takahiro Tsumori , Masato Nakano
IPC分类号： C11D3/37 , C11D3/33
CPC分类号： C11D3/2086 , C08J3/14 , C08L33/00 , C08L33/14 , C08L35/00 , C08L41/00 , C11D3/33 , C11D3/34 , C11D3/3757 , C11D3/378 , C11D3/3902 , C11D3/3942 , C11D3/3947 , C11D7/265 , C11D7/34 , C08L2666/04
摘要： An ADW composition comprising a builder and a water-soluble copolymer which comprises: (a) from about 30 to 60 mol % of the copolymer having a structural unit originating from a monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer having 4 to 6 carbon atoms or its anhydride at; (b) from about 30 to 60 mol % of the copolymer having a structural unit originating from a monoethylenic unsaturated monocarboxylic acid (or monocarboxylate) monomer having 3 to 8 carbon atoms; and (c) from about 5 to 15 mol % of the polymer having a structural unit originating from a monoethylenic unsaturated monomer having a sulfonic (or sulfonate) group; wherein the water-soluble copolymer has a weight average molecular weight of from about 1,000 to about 50,000 wherein the copolymer is polymerized with hydrogen peroxide.
摘要翻译：一种包含助洗剂和水溶性共聚物的ADW组合物，其包含：（a）约30至60摩尔％的具有来自具有4-6个碳原子的单烯属不饱和二羧酸（或二羧酸酯）单体的结构单元的共聚物或其酸酐在（b）具有来自具有3-8个碳原子的单烯属不饱和一元羧酸（或单羧酸酯）单体的结构单元的共聚物的约30至60摩尔％和（c）约5至15摩尔％的具有源自具有磺酸（或磺酸盐）基团的单烯属不饱和单体的结构单元的聚合物; 其中所述水溶性共聚物的重均分子量为约1,000至约50,000，其中所述共聚物与过氧化氢聚合。

5. 发明授权

US09133422B2 Sulfonic group-containing, maleic acid-based, water-soluble copolymer aqueous solution and powder obtained by drying the aqueous solution 有权
标题翻译：含有磺酸基的马来酸基水溶性共聚物水溶液和干燥水溶液得到的粉末
公开(公告)号：US09133422B2
公开(公告)日：2015-09-15
申请号：US12863865
申请日：2009-03-27
申请人： Takahiro Tsumori , Masato Nakano
发明人： Takahiro Tsumori , Masato Nakano
IPC分类号： C11D7/26 , C11D7/34 , C11D7/54 , C11D3/20 , C11D3/34 , C11D3/39 , C11D3/37 , C08J3/14 , C08L33/00 , C08L35/00 , C11D3/33 , C08L33/14 , C08L41/00
CPC分类号： C11D3/2086 , C08J3/14 , C08L33/00 , C08L33/14 , C08L35/00 , C08L41/00 , C11D3/33 , C11D3/34 , C11D3/3757 , C11D3/378 , C11D3/3902 , C11D3/3942 , C11D3/3947 , C11D7/265 , C11D7/34 , C08L2666/04
摘要： Provided is a copolymer aqueous solution which exerts a high calcium carbonate-deposition suppressing ability even under high hardness condition, has excellent storage stability, and suppresses coloring of a detergent to yellow even when used as a detergent raw material. The water-soluble copolymer aqueous solution includes a water-soluble copolymer and hydrogen peroxide as essential components, in which: the water-soluble copolymer at least includes, as its structure, a structural unit originating from a monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer having 4 to 6 carbon atoms or its anhydride (a) at 30 to 60 mol %, a structural unit originating from a monoethylenic unsaturated monocarboxylic acid (or monocarboxylate) monomer having 3 to 8 carbon atoms (b), and a structural unit originating from a monoethylenic unsaturated monomer having a sulfonic (or sulfonate) group (c); the water-soluble copolymer has a weight average molecular weight of 1,000 or more and 50,000 or less; the water-soluble copolymer aqueous solution has a weight ratio of the hydrogen peroxide of 10 ppm to 50,000 ppm with respect to a solid content of the water-soluble copolymer aqueous solution; and the water-soluble copolymer aqueous solution has a weight ratio of water of 33% to 99%.
摘要翻译：提供即使在高硬度条件下也具有高碳酸钙沉积抑制能力的共聚物水溶液，具有优异的储存稳定性，并且即使用作洗涤剂原料也能抑制洗涤剂的着色。水溶性共聚物水溶液包含水溶性共聚物和过氧化氢作为必要成分，其中：水溶性共聚物至少包含来自单烯属不饱和二羧酸（或二羧酸酯）的结构单元作为其结构，具有4-6个碳原子的单体或其酸酐（a）的含量为30至60摩尔％，源自具有3-8个碳原子的单烯属不饱和一元羧酸（或单羧酸酯）单体（b）的结构单元，以及起始于来自具有磺酸（或磺酸）基团（c）的单烯属不饱和单体; 该水溶性共聚物的重均分子量为1000以上且50,000以下，相对于水溶性共聚物水溶液的固体成分，水溶性共聚物水溶液的过氧化氢重量比为10ppm〜50,000ppm; 水溶性共聚物水溶液的重量比为33〜99％。

6. 发明授权

US08779184B2 Manufacturing method for sulfonic acid group-containing ether compound 有权
标题翻译：含磺酸基醚化合物的制备方法
公开(公告)号：US08779184B2
公开(公告)日：2014-07-15
申请号：US13063563
申请日：2009-09-14
申请人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
发明人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
IPC分类号： C07C309/00
CPC分类号： C07C309/20 , C07C303/02 , C07C309/09 , C08F216/1466
摘要： The present invention provides a method for efficiently producing a sulfonic acid group-containing ether compound having a high purity and a good polymerizability while preventing production of a byproduct, and provides a sulfonic acid group-containing ether compound containing fewer impurities and having a good radical (co)polymerizability.The present invention provides a method of producing a sulfonic acid group-containing ether compound by reacting a sulfurous acid compound with a compound represented by the formula (1): wherein R1 represents a single bond, a CH2 group, or a CH2CH2 group, and R2 represents H, or a CH3 group, the method comprising the steps of: adjusting pH of a reaction system to 5.5 or greater with use of an alkaline substance; and adding the compound represented by the formula (1) to a reaction vessel containing the sulfurous acid compound.
摘要翻译：本发明提供了一种有效地制备具有高纯度和良好的聚合性同时防止副产物生成的含磺酸基的醚化合物的方法，并且提供了含少量杂质和具有良好基团的含磺酸基的醚化合物（共）聚合性。本发明提供一种通过使亚硫酸化合物与式（1）表示的化合物反应制备含磺酸基醚化合物的方法：其中R1表示单键，CH2基或CH2CH2基，和 R 2表示H或CH 3基团，该方法包括以下步骤：使用碱性物质将反应体系的pH调节至5.5以上; 并将由式（1）表示的化合物加入到含有亚硫酸化合物的反应容器中。

7. 发明申请

US20110009303A1 AUTOMATIC DISHWASHING COMPOSITION CONTAINING A SULFONATED COPOLYMER 有权
标题翻译：自动洗涤组合物含有磺化共聚物
公开(公告)号：US20110009303A1
公开(公告)日：2011-01-13
申请号：US12863844
申请日：2009-03-27
申请人： Takahiro Tsumori , Masato Nakano
发明人： Takahiro Tsumori , Masato Nakano
IPC分类号： C11D3/37 , C11D17/00 , C11D17/06
CPC分类号： C11D3/2086 , C08J3/14 , C08L33/00 , C08L33/14 , C08L35/00 , C08L41/00 , C11D3/33 , C11D3/34 , C11D3/3757 , C11D3/378 , C11D3/3902 , C11D3/3942 , C11D3/3947 , C11D7/265 , C11D7/34 , C08L2666/04
摘要： An ADW composition comprising a builder and a water-soluble copolymer which comprises: (a) from about 30 to 60 mol % of the copolymer having a structural unit originating from a monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer having 4 to 6 carbon atoms or its anhydride at; (b) from about 30 to 60 mol % of the copolymer having a structural unit originating from a monoethylenic unsaturated monocarboxylic acid (or monocarboxylate) monomer having 3 to 8 carbon atoms; and (c) from about 5 to 15 mol % of the polymer having a structural unit originating from a monoethylenic unsaturated monomer having a sulfonic (or sulfonate) group; wherein the water-soluble copolymer has a weight average molecular weight of from about 1,000 to about 50,000 wherein the copolymer is polymerized with hydrogen peroxide.
摘要翻译：一种包含助洗剂和水溶性共聚物的ADW组合物，其包含：（a）约30至60摩尔％的具有来自具有4-6个碳原子的单烯属不饱和二羧酸（或二羧酸酯）单体的结构单元的共聚物或其酸酐在（b）具有来自具有3-8个碳原子的单烯属不饱和一元羧酸（或单羧酸酯）单体的结构单元的共聚物的约30至60mol％; 和（c）约5至15摩尔％的具有源自具有磺酸（或磺酸盐）基团的单烯属不饱和单体的结构单元的聚合物; 其中所述水溶性共聚物的重均分子量为约1,000至约50,000，其中所述共聚物与过氧化氢聚合。

8. 发明申请

US20100298526A1 COPOLYMER COMPOSITION AND METHOD OF PRODUCING THE COMPOSITION 审中-公开
标题翻译：共聚物组合物及其制备方法
公开(公告)号：US20100298526A1
公开(公告)日：2010-11-25
申请号：US12740954
申请日：2008-10-31
申请人： Takahiro Tsumori , Masato Nakano
发明人： Takahiro Tsumori , Masato Nakano
IPC分类号： C08G75/00
CPC分类号： C11D3/378 , C08F2/10 , C08F2/38 , C08F220/04 , C08F220/38 , C08F222/02
摘要： Provided are a copolymer composition which can achieve a high level of compatibility between clay dispersibility under water having high hardness and an anti-iron deposition ability and is suitable for an additive for a detergent, and a method of producing the composition. The copolymer composition of the present invention includes a copolymer (P) which has a weight average molecular weight of 10,000 to 50,000 and contains a structural unit originating from a monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer (a) at 30 to 60 mol %, a structural unit originating from a monoethylenic unsaturated monocarboxylic acid (or monocarboxylate) monomer (b), and a structural unit originating from a sulfonic acid (or sulfonate) group-containing monomer (c) free of an ester bond and an amide bond, and a remaining monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer a content of which in terms of an acid is less than 12,000 ppm.
摘要翻译：提供一种共聚物组合物，其可以实现在具有高硬度和抗铁沉积能力的水下的粘土分散性之间的高水平的相容性，并且适用于洗涤剂用添加剂和制备该组合物的方法。本发明的共聚物组合物包含重均分子量为10,000〜50,000的共聚物（P），含有以30〜60摩尔％的单烯属不饱和二羧酸（或二羧酸酯）单体（a）的结构单元，，来自单烯属不饱和一元羧酸（或单羧酸酯）单体（b）的结构单元和源自不含酯键和酰胺键的含磺酸（或磺酸酯）基团的单体（c）的结构单元，和剩余的单烯属不饱和二羧酸（或二羧酸酯）单体的含量以酸计小于12,000ppm。

9. 发明申请

US20100292122A1 SULFONIC GROUP-CONTAINING, MALEIC ACID-BASED, WATER-SOLUBLE COPOLYMER AQUEOUS SOLUTION AND POWDER OBTAINED BY DRYING THE AQUEOUS SOLUTION 有权
标题翻译：含硫酸基，基于酸性的水溶性共聚物水溶液和粉末通过干燥水溶液获得
公开(公告)号：US20100292122A1
公开(公告)日：2010-11-18
申请号：US12863865
申请日：2009-03-27
申请人： Takahiro Tsumori , Masato Nakano
发明人： Takahiro Tsumori , Masato Nakano
IPC分类号： C08K3/20 , C02F5/10 , C11D3/39
CPC分类号： C11D3/2086 , C08J3/14 , C08L33/00 , C08L33/14 , C08L35/00 , C08L41/00 , C11D3/33 , C11D3/34 , C11D3/3757 , C11D3/378 , C11D3/3902 , C11D3/3942 , C11D3/3947 , C11D7/265 , C11D7/34 , C08L2666/04
摘要： Provided is a copolymer aqueous solution which exerts a high calcium carbonate-deposition suppressing ability even under high hardness condition, has excellent storage stability, and suppresses coloring of a detergent to yellow even when used as a detergent raw material. The water-soluble copolymer aqueous solution includes a water-soluble copolymer and hydrogen peroxide as essential components, in which: the water-soluble copolymer at least includes, as its structure, a structural unit originating from a monoethylenic unsaturated dicarboxylic acid (or dicarboxylate) monomer having 4 to 6 carbon atoms or its anhydride (a) at 30 to 60 mol %, a structural unit originating from a monoethylenic unsaturated monocarboxylic acid (or monocarboxylate) monomer having 3 to 8 carbon atoms (b), and a structural unit originating from a monoethylenic unsaturated monomer having a sulfonic (or sulfonate) group (c); the water-soluble copolymer has a weight average molecular weight of 1,000 or more and 50,000 or less; the water-soluble copolymer aqueous solution has a weight ratio of the hydrogen peroxide of 10 ppm to 50,000 ppm with respect to a solid content of the water-soluble copolymer aqueous solution; and the water-soluble copolymer aqueous solution has a weight ratio of water of 33% to 99%.
摘要翻译：提供即使在高硬度条件下也具有高碳酸钙沉积抑制能力的共聚物水溶液，具有优异的储存稳定性，并且即使用作洗涤剂原料也能抑制洗涤剂的着色。水溶性共聚物水溶液包含水溶性共聚物和过氧化氢作为必要成分，其中：水溶性共聚物至少包含来自单烯属不饱和二羧酸（或二羧酸酯）的结构单元作为其结构，具有4-6个碳原子的单体或其酸酐（a）的含量为30至60摩尔％，源自具有3-8个碳原子的单烯属不饱和一元羧酸（或单羧酸酯）单体（b）的结构单元，以及起始于来自具有磺酸（或磺酸）基团（c）的单烯属不饱和单体; 该水溶性共聚物的重均分子量为1000以上且50,000以下，相对于水溶性共聚物水溶液的固体成分，水溶性共聚物水溶液的过氧化氢重量比为10ppm〜50,000ppm; 水溶性共聚物水溶液的重量比为33〜99％。

10. 发明申请

US20090198029A1 N-VINYL CYCLIC LACTAM POLYMER, PRODUCTION METHOD THEREOF, AND APPLICATION THEREOF 审中-公开
标题翻译： N-乙烯基环状乳液聚合物，其生产方法及其应用
公开(公告)号：US20090198029A1
公开(公告)日：2009-08-06
申请号：US11915590
申请日：2006-05-26
申请人： Takahiro Tsumori , Daisuke Imai , Yoshikazu Fujii
发明人： Takahiro Tsumori , Daisuke Imai , Yoshikazu Fujii
IPC分类号： C08F4/30 , C08F26/06
CPC分类号： C08F271/02 , C11D3/3776
摘要： To provide: an N-vinyl cyclic lactam polymer, which has excellent dispersibility and adsorptivity, and high calcium-ion capturing capability and can be preferably used in, for example, a detergent additive application; an application thereof; and a production method of the N-vinyl cyclic lactam polymer, the production method being capable of efficiently producing such an N-vinyl cyclic lactam polymer. An N-vinyl cyclic lactam polymer produced by a polymerization of a monomer component containing a carboxyl group-containing unsaturated monomer with a polymer having an N-vinyl cyclic lactam unit, wherein the carboxyl group-containing unsaturated monomer is 200 to 9900 parts by weight, relative to 100 parts by weight of the polymer having an N-vinyl cyclic lactam unit, and the N-vinyl cyclic lactam polymer has a viscosity at 25° C. of 100000 mPa·s or less in an aqueous solution with a solid content of 25% by weight.
摘要翻译：提供：分散性和吸附性优异，钙离子捕获能力高的N-乙烯基环状内酰胺聚合物，优选用于例如洗涤剂添加剂用途中。其应用; 以及N-乙烯基环内酰胺聚合物的制造方法，该制造方法能够有效地制造这种N-乙烯基环状内酰胺类聚合物。通过含有含羧基的不饱和单体的单体组分与具有N-乙烯基环状内酰胺单元的聚合物的聚合制备的N-乙烯基环状内酰胺聚合物，其中含羧基的不饱和单体为200〜9900重量份相对于100重量份的具有N-乙烯基环内酰胺单元的聚合物，N-乙烯基环内酰胺聚合物在固体含量的水溶液中的25℃下的粘度为100000mPa.s以下为25重量％。

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