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1. 发明申请

WO9830601A3 METHOD OF CONTROLLING POLYMER MOLECULAR WEIGHT AND STRUCTURE 审中-公开
标题翻译：控制聚合物分子量和结构的方法
公开(公告)号：WO9830601A3
公开(公告)日：1998-12-03
申请号：PCT/US9800601
申请日：1998-01-07
申请人： DU PONT , COMMW SCIENT IND RES ORG , ANDERSON ALBERT G , GRIDNEV ALEXEI , MOAD GRAEME , RIZZARDO EZIO , THANG SAN HOA
发明人： ANDERSON ALBERT G , GRIDNEV ALEXEI , MOAD GRAEME , RIZZARDO EZIO , THANG SAN HOA
IPC分类号： C07D233/38 , C07D235/02 , C08F2/00 , C08F2/38 , C08F4/00 , C08F220/14 , C08F220/18 , C08F293/00
CPC分类号： C07D235/02 , C07D233/38 , C08F2/38 , C08F4/00 , C08F220/14 , C08F293/005 , C08F2220/1825 , C08F2438/02 , C08F212/08
摘要： This invention concerns the preparation of polymers of low polydispersity and/or controlled molecular weight and architecture employing living free radical polymerization initiated by an alkoxyamine initiator or nitroxide plus, optionally, a free radical initiator; the polymer produced thereby; selected nitroxide and alkoxyamine initiators; and a process for making the initiators; the polymeric products being useful in protective coatings.

2. 发明公开

EP0853634A4 CONTROL OF MOLECULAR WEIGHT AND END-GROUP FUNCTIONALITY IN POLYMERS 失效
标题翻译：控制分子量和聚合物的终止
公开(公告)号：EP0853634A4
公开(公告)日：1998-09-30
申请号：EP96931683
申请日：1996-10-04
申请人： COMMW SCIENT IND RES ORG , DU PONT
发明人： RIZZARDO ENZIO , THANG SAN HOA , MOAD GRAEME , CHONG YEN KWONG
IPC分类号： C08L101/00 , C08F2/38 , C08F2/42 , C08F14/06 , C08F214/06 , C08F290/04 , C08F293/00 , C09D201/00 , C09J201/00
CPC分类号： C08F290/04 , C08F2/38 , C08F14/06
摘要： This invention relates to a process for the production of lower molecular weight polymers by free radical-initiated polymerization of unsaturated species characterised by the use of an unsaturated compound of Formula (I) as a chain transfer agent wherein R?1 and R2¿ are the same or different and are selected from the group consisting of hydrogen, optionally substituted alkyl, optionally substituted saturated or aromatic carbocyclic or heterocyclic ring, and halogen; X is selected from the group consisting of chlorine, bromine, optionally substituted alkylsulfonyl, and optionally substituted arylsulfonyl; Y is selected from the group consisting of halogen, a polymer chain, and CR3R4Z, wherein R?3 and R4¿ are the same or different and are selected from the group consisting of hydrogen, optionally substituted alkyl, optionally substituted saturated, unsaturated or aromatic carbocyclic or heterocyclic ring, and halogen; and Z is selected from the group consisting of chlorine, bromine, optionally substituted alkylsulfonyl and optionally substituted arylsulfonyl; provided that when X is optionally substituted alkylsulfonyl or optionally substituted arylsulfonyl, Y is not halogen. The invention also relates to various polymers produced by this process and products comprising these polymers. The process of the invention may also be used in the preparation of A-B type block copolymers.

3. 发明授权

EP0711327B1 AQUEOUS DISPERSIONS CONTAINING CYCLOPOLYMER DISPERSANTS 失效
标题翻译：水性分散体，循环变聚合物分散剂CONTAIN
公开(公告)号：EP0711327B1
公开(公告)日：1997-12-29
申请号：EP94925712
申请日：1994-07-29
申请人： DU PONT , COMMW SCIENT IND RES ORG
发明人： MA SHEAU-HWA , THANG SAN HOA , RIZZARDO EZIO , MOAD GRAEME
IPC分类号： C07D239/26 , B01J27/232 , B01J31/02 , B41M1/42 , C07C1/26 , C07C13/28 , C07C17/26 , C07C22/00 , C07C49/213 , C07C49/227 , C07C55/02 , C07C55/22 , C07C55/24 , C07C57/03 , C07C67/347 , C07C69/604 , C07C69/614 , C07C69/618 , C07C69/65 , C07C69/73 , C07C253/30 , C07C255/23 , C07C255/33 , C07C315/04 , C07C317/44 , C07D239/62 , C07D319/06 , C07F9/40 , C08F20/52 , C08F32/06 , C08F36/04 , C08F36/20 , C08F136/20 , C08F220/10 , C08F220/54 , C08F236/20 , C08F244/00 , C08L45/00 , C08L47/00 , C09D11/00 , C09D11/10 , C09D121/00 , C09D147/00
CPC分类号： C08F36/20 , C07C69/604 , C07C69/618 , C07C69/65 , C07D239/62 , C07D319/06 , C07F9/4015 , C09D11/326
摘要： PCT No. PCT/AU94/00433 Sec. 371 Date Jan. 26, 1996 Sec. 102(e) Date Jan. 26, 1996 PCT Filed Jul. 29, 1994 PCT Pub. No. WO95/04026 PCT Pub. Date Feb. 9, 1995Compounds of general formula (I) (I) characterised in that R1 and R2 are independently selected from the group consisting of COOR, CN, aryl, substituted aryl, COOH, halogen, C(O)NHR4, C(O)NR5R6; X and Y are independently selected from the group consisting of H, COOH, COOR, CN, R3CO-, C(O)NHR4, C(O)NR5R6, P(O)(OR7)2 and SO2R8; with the proviso that X and Y are not both H; or X and Y together with the carbon atom to which they are attached form a carbocyclic or heterocyclic ring system which can contain oxygen, sulfur or nitrogen atoms; and R, R3, R4, R5, R6, R7 and R8 are various groups; and polymers and copolymers derived from such compounds.

4. 发明专利

AU2001251439B2 Process of microgel synthesis and products produced therefrom 未知
公开(公告)号：AU2001251439B2
公开(公告)日：2006-11-16
申请号：AU2001251439
申请日：2001-04-06
申请人： COMMW SCIENT IND RES ORG , DU PONT
发明人： RIZZARDO EZIO , CHIEFARI JOHN , WILSON GERRY , BERGE CHARLES T , MAU ALBERT , SWIEGERS GERRY , MAYADUNNE ROSHAN , JOHNSON JEFFERY W , MOAD CATHERINE LOUISE , MOAD GRAEME , THANG SAN
IPC分类号： C08F293/00 , A61K9/06 , C07C327/36 , C08F2/38 , C08L53/00 , C09D153/00

5. 发明专利

ES2221401T3 MICROGELES Y PROCESO PARA SU PREPARACION. 未知
公开(公告)号：ES2221401T3
公开(公告)日：2004-12-16
申请号：ES99932369
申请日：1999-07-09
申请人： DU PONT , COMMW SCIENT IND RES ORG
发明人： BERGE CHARLES T , FRYD MICHAEL , JOHNSON JEFFERY W , MOAD GRAEME , RIZZARDO EZIO , SCOPAZZI CHRISTOPHER
IPC分类号： C08F2/38 , C08F4/40 , C08F265/04 , C08F290/04 , C08F290/06 , C08F293/00
摘要： Proceso para formar un microgel que comprende un núcleo de polímero reticulado y una pluralidad de brazos poliméricos prácticamente lineales unidos al núcleo, comprendiendo el proceso los pasos de: I) introducir monómero monoolefínico, catalizador e iniciador en un reactor en ausencia de monómero multiolefínico y producir un componente prepolímero activable B que tiene un peso molecular medio en peso de 1.000-25.000, comprendiendo dicho prepolímero activable un polímero que contiene grupos halógeno activado, un polímero terminado con grupos tiocarboniltio, o un macromonómero que tiene al menos una funcionalidad activa en polimerización; II) poner al producto de I) en contacto con monómero multiolefínico para producir el componente reticulado A y el componente soluble C, opcionalmente en presencia de iniciador adicional, y también opcionalmente en presencia de iniciador y monómero monoolefínico adicional; pudiendo la relación de componentes A/(B+C) ser controlada a base de variar la relaciónmolar de (Componente B)/(monómero multiolefínico) desde 0, 05/1 hasta 5/1, a base de disminuir dicha relación molar para incrementar la relación de A/(B+C), y a base de incrementar dicha relación molar para disminuir la relación de A/(B+C); teniendo el microgel un peso molecular medio en peso de 104 - 108.

6. 发明专利

DE69917311D1 未知
公开(公告)号：DE69917311D1
公开(公告)日：2004-06-17
申请号：DE69917311
申请日：1999-07-09
申请人： DU PONT , COMMW SCIENT IND RES ORG
发明人： BERGE T , FRYD MICHAEL , JOHNSON W , MOAD GRAEME , RIZZARDO EZIO , SCOPAZZI CHRISTOPHER , THANG HOA
IPC分类号： C08F2/38 , C08F4/40 , C08F265/04 , C08F290/04 , C08F290/06 , C08F293/00

7. 发明专利

BR0109902A 未知
公开(公告)号：BR0109902A
公开(公告)日：2003-06-03
申请号：BR0109902
申请日：2001-04-06
申请人： DU PONT , COMMW SCIENT IND RES ORG
发明人： BERGE CHARLES T , CHIEFARI JOHN , JOHNSON JEFFERY W , MAU ALBERT , MAYADUNNE ROSHAN , MOAD CATHERINE LOUISE , MOAD GRAEME , RIZZARDO EZIO , SWIEGERS GERRY , THANG SAN , WILSON GERRY
IPC分类号： C09K23/52 , A61K9/51 , B01J13/00 , B01J13/14 , C08F2/38 , C08F287/00 , C08F290/04 , C08F293/00 , C08J3/02 , C08L53/00 , C09D153/00 , C07C327/36 , A61K9/06
摘要： The invention provides in one aspect a process for preparing a microgel by RAFT polymerizing in the presence of a RAFT chain transfer agent, one or more solvophobic monomers and one or more solvophilic monomers to form one or more block copolymers comprising one or more solvophobic blocks and one or more solvophilic blocks wherein the solvophobic block is insoluble in a dispersing medium and the solvophilic block is soluble in the dispersing medium. The block copolymer is dispersed in the dispersing medium to form micelles, which is then stabilized to form the microgel. The dispersing medium can be aqueous or lipophilic. The method of the present invention also permits one to encapsulate a wide variety of materials, such as pigments, dye molecules, and aluminum flakes used in metallized paints.

8. 发明专利

DE69617973D1 未知
公开(公告)号：DE69617973D1
公开(公告)日：2002-01-24
申请号：DE69617973
申请日：1996-10-04
申请人： DU PONT , COMMW SCIENT IND RES ORG
发明人： RIZZARDO ENZIO , THANG HOA , MOAD GRAEME , CHONG KWONG
IPC分类号： C08F2/38 , C08F2/42 , C08L101/00 , C08F14/06 , C08F214/06 , C08F290/04 , C08F293/00 , C09D201/00 , C09J201/00
摘要： This invention relates to a process for the production of lower molecular weight polymers by free radical-initiated polymerization of unsaturated species characterized by the use of an unsaturated compound of Formula I as a chain transfer agent:wherein R1 and R2 are the same or different and are selected from the group consisting of hydrogen, optionally substituted alkyl, optionally substituted saturated or aromatic carbocyclic or heterocyclic ring, and halogen;X is selected from the group consisting of chlorine, bromine, optionally substituted alkylsulfonyl, and optionally substituted arylsulfonyl,Y is selected from the group consisting of halogen, a polymer chain, and CR3R4Z, wherein R3 and R4 are the same or different and are selected from the group consisting of hydrogen, optionally substituted alkyl, optionally substituted saturated, unsaturated or aromatic carbocyclic or hetercyclic ring, and halogen; andZ is selected from the group consisting of chlorine, bromine, optionally substituted alkylsulfonyl and optionally substituted arylsulfonyl;provided that when X is optionally substituted alkylsulfonyl or optionally substituted arylsulfonyl, Y is not halogen.The invention also relates to various polymers produced by this process and products comprising these polymers. The process of the invention may also be used in the preparation of A-B type block copolymers.

9. 发明专利

MXPA00005653A 未知
公开(公告)号：MXPA00005653A
公开(公告)日：2001-05-01
申请号：MXPA00005653
申请日：2000-06-08
申请人： DU PONT , COMMW SCIENT IND RES ORG
发明人： CHIEFAIR JOHN , MAYADUNNE ROSHAN TYRREL , MOAD GRAEME , RIZZARDO EZIO , THANG SAN HOA
IPC分类号： C07C327/20 , C07C325/02 , C07C327/36 , C07C327/52 , C07C329/04 , C07C329/12 , C07C329/16 , C07C333/18 , C07C333/20 , C07D207/26 , C07D207/263 , C07D207/32 , C07D209/48 , C08F2/38
摘要： A free radical polymerization process suitable for synthesizingpolymers is disclosed. The process utilizes novel sulfur based chain transfer agents and is widely compatible over a range of monomers and reaction conditions. Novel polymers having low pollydispersity and predictable specific polymer architecture and molecular weight are produced by the process. The polymers produced by the process are suitable for use as binders in automotive OEM and refinish coatings.

10. 发明专利

ES2143557T3 未知
公开(公告)号：ES2143557T3
公开(公告)日：2000-05-16
申请号：ES94931465
申请日：1994-11-02
申请人： COMMW SCIENT IND RES ORG , DU PONT
发明人： RIZZARDO EZIO , THANG SAN HOA , MOAD GRAEME , BERGE CHARLES THOMAS
IPC分类号： C07C69/593 , C07C69/604 , C07C69/618 , C07C255/32 , C07F7/08 , C07F7/10 , C07F7/12 , C08F2/38 , C07C69/65 , C08F118/08 , C08F112/08 , C08F120/14 , C08F120/18
摘要： PCT No. PCT/AU94/00672 Sec. 371 Date Aug. 1, 1996 Sec. 102(e) Date Aug. 1, 1996 PCT Filed Nov. 2, 1994 PCT Pub. No. WO95/12568 PCT Pub. Date May 11, 1995A process for the free radical initiated polymerization of unsaturated species characterized by the use of compound of Formula (I) as chain transfer agents: Formula (I) wherein: X is selected from hydrogen; CN; optionally substituted aryl; COOH; COOR; C(O)NHR6; C(O)NR7R8; and halogen; Q is selected from COOR1; CN; and C(O)NR7R8; Y is selected from hydrogen; C1 to C6 alkyl; C1 to C6 alkyl substituted with one or more substituents selected from hydroxy, amino, C1 to C6 alkoxy, C1 to C6 alkoxycarbonyl, halogen, CN and optionally substituted aryl; C1 to C6 alkenyl; and C1 to C6 alkynyl; Z is selected from COOR2; CN; and optionally substituted aryl; R3 and R4 are the same or different and are selected from hydrogen C1 to C4 alkyl and halogen; or R3 and R4 together with carbon atom to which they are attached form part of a carbocyclic or heterocyclic ring structure; and the other substituents are as defined in the text.

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