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1. 发明授权

US6110529A Method of forming metal films on a substrate by chemical vapor deposition 失效
标题翻译：通过化学气相沉积在基板上形成金属膜的方法
公开(公告)号：US6110529A
公开(公告)日：2000-08-29
申请号：US484654
申请日：1995-06-07
申请人： Robin A. Gardiner , Peter S. Kirlin , Thomas H. Baum , Douglas Gordon , Timothy E. Glassman , Sofia Pombrik , Brian A. Vaartstra
发明人： Robin A. Gardiner , Peter S. Kirlin , Thomas H. Baum , Douglas Gordon , Timothy E. Glassman , Sofia Pombrik , Brian A. Vaartstra
IPC分类号： C07F3/00 , C07F5/00 , C07F7/00 , C07F9/00 , C07F19/00 , C23C16/00 , C23C16/18 , C23C16/30 , C23C16/40 , C23C16/448 , G01T5/08 , G02B6/02 , G02B6/036 , H01L39/24
CPC分类号： C07F3/003 , C07F19/005 , C07F5/003 , C07F7/006 , C07F9/005 , C23C16/18 , C23C16/30 , C23C16/305 , C23C16/40 , C23C16/408 , C23C16/409 , C23C16/4481 , C23C16/4483 , C23C16/45561 , G02B6/02 , H01L39/2441
摘要： A method of forming on a substrate a metal film, comprising depositing said metal film on said substrate via chemical vapor deposition from a metalorganic complex of the formula:MA.sub.Y Xwherein:M is a y-valent metal;A is a monodentate or multidentate organic ligand coordinated to M which allows complexing of MA.sub.y with X;y is an integer having a value of 2, 3 or 4; each of the A ligands may be the same or different; andX is a monodentate or multidentate ligand coordinated to M and containing one or more atoms independently selected from the group consisting of atoms of the elements C, N, H, S, O and F.The metal M may be selected from the group consisting of Cu, Ba, Sr, La, Nd, Ce, Pr, Sm, Eu, Th, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Bi, Tl, Y, Pb, Ni, Pd, Pt, Al, Ga, In, Ag, Au, Co, Rh, Ir, Fe, Ru, Sn, Li, Na, K, Rb, Cs, Ca, Mg, Ti, Zr, Hf, V, Nb, Ta, Cr, Mo, and W. A may be selected from the group consisting of .beta.-diketonates, .beta.-thioketonates, cyclopentadienyls, alkyls, perfluoroalkyls, alkoxides, perfluoroalkoxides, and Schiff bases. X may for example comprise a ligand such as tetraglyme, tetrahydrofuran, bipyridine, crown ether, or thioether.
摘要翻译：一种在衬底上形成金属膜的方法，包括通过化学气相沉积从所述下式的金属有机络合物沉积所述金属膜：其中：M为Y价金属; A是与M配位的单齿或多齿有机配体，其允许将MAy与X配位; y是值为2,3或4的整数; 每个A配体可以相同或不同; 并且X是与M配位并含有独立地选自元素C，N，H，S，O和F的原子的一个或多个原子的单齿或多齿配体。金属M可以选自的Cu，Ba，Sr，La，Nd，Ce，Pr，Sm，Eu，Th，Gd，Tb，Dy，Ho，Er，Tm，Yb，Lu，Bi，Tl，Y，Pb，Ni，，Al，Ga，In，Ag，Au，Co，Rh，Ir，Fe，Ru，Sn，Li，Na，K，Rb，Cs，Ca，Mg，Ti，Zr，Hf，V，Nb，Ta，Cr ，Mo和W.A可以选自β-二酮化合物，β-硫代酮酸酯，环戊二烯基，烷基，全氟烷基，烷氧基化物，全氟烷氧基化物和希夫碱。 X可以例如包括配体如四甘醇二甲醚，四氢呋喃，联吡啶，冠醚或硫醚。

2. 发明授权

US6077965A Metal complexes with an adamantane-like structure 失效
标题翻译：具有金刚烷结构的金属络合物
公开(公告)号：US6077965A
公开(公告)日：2000-06-20
申请号：US284412
申请日：1999-04-14
申请人： Michael Geprags , Rainer Sturmer , Horst Weiss , Susanne Steiger
发明人： Michael Geprags , Rainer Sturmer , Horst Weiss , Susanne Steiger
IPC分类号： C07F7/00 , C07F7/28 , C08F4/60 , C08F10/00 , C07F9/00 , C07F11/00
CPC分类号： C07F7/28 , C07F7/006 , C08F10/00
摘要： In metal complexes of the formula I ##STR1## the substituents have the following meanings: M is a metal of transition group III, IV, V or VI of the Periodic Table of the Elements or a metal of the lanthanide series,Y is a negative leaving atom or a negative leaving group,X and X.sup.1 are negatively charged or uncharged atoms of main group IV, V or VI of the Periodic Table of the Elements,Z is hydrogen, C.sub.1 -C.sub.10 -alkyl, C.sub.3 -C.sub.10 -cycloalkyl, C.sub.1 -C.sub.10 -alkoxy, C.sub.1 -C.sub.10 -alkylthio or dialkylamido having from 1 to 4 carbon atoms in each alkyl radical,R.sup.1 to R.sup.11 are hydrogen, carboorganic or organosilicon radicals,n is 0, 1 or 2 andthe valence of M is 2+n.
摘要翻译： PCT No.PCT / EP97 / 05206 Sec。 371 1999年4月14日第 102（e）1999年4月14日PCT PCT 1997年9月23日PCT公布。公开号WO98 / 16534 日期：1998年4月23日在式I的金属络合物中，取代基具有以下含义：M是元素周期表的III，IV，V或VI族过渡金属或镧系金属，Y是负离子原子或负离去基团，X和X1是元素周期表的主要IV，V或VI族的带负电荷或不带电原子，Z是氢，C1-C10-烷基，C3-C10-环烷基在每个烷基中具有1至4个碳原子的C 1 -C 10 - 烷氧基，C 1 -C 10 - 烷硫基或二烷基酰氨基，R 1至R 11为氢，有机碳或有机硅基，n为0,1或2，并且M的化合价为 2 + n。

3. 发明授权

US5998646A Unsaturated organometallic compounds derived from titanium and process for their preparation 失效
标题翻译：衍生自钛的不饱和有机金属化合物及其制备方法
公开(公告)号：US5998646A
公开(公告)日：1999-12-07
申请号：US185499
申请日：1998-11-04
申请人： Alain Riondel , Michel Camail , Andre Margaillan , Jean-Louis Vernet , Marie Humbert
发明人： Alain Riondel , Michel Camail , Andre Margaillan , Jean-Louis Vernet , Marie Humbert
IPC分类号： C07C51/41 , C07F7/00 , C07F7/28
CPC分类号： C07F7/006 , C07C51/412
摘要： These compounds are denoted by the formula (I): ##STR1## in which R denotes a tert-butyl, tert-amyl or 2-ethylhexyl radical. To prepare them, methacrylic acid is reacted with a tetraalkoxytitanium Ti(OR).sub.4, where R=isopropyl or tert-butyl, to obtain a corresponding compound (I), or with Ti(OR) (OtAm).sub.3, where R=isopropyl or tert-butyl and tAm=tert-amyl, to obtain a compound (I) with R=tert-amyl, the compounds (I) with R=isopropyl or tert-butyl furthermore denoting intermediate synthesis products which can be reacted with tert-amyl alcohol or with 2-ethylhexanol, to obtain a compound (I) in which R denotes tert-amyl or 2-ethylhexyl respectively.
摘要翻译：这些化合物由式（I）表示：其中R表示叔丁基，叔戊基或2-乙基己基。为了制备它们，甲基丙烯酸与四烷氧基钛Ti（OR）4反应，其中R =异丙基或叔丁基，得到相应的化合物（I）或与Ti（OR）（OtAm）3反应，其中R =异丙基或叔丁基，tAm =叔戊基，得到具有R =叔戊基的化合物（I），化合物（I）与R =异丙基或叔丁基进一步表示中间体合成产物，戊醇或2-乙基己醇，得到其中R表示叔戊基或2-乙基己基的化合物（I）。

4. 发明授权

US5914408A Olefin polymerization catalysts containing benzothiazole 失效
标题翻译：含有苯并噻唑的烯烃聚合催化剂
公开(公告)号：US5914408A
公开(公告)日：1999-06-22
申请号：US130846
申请日：1998-08-07
申请人： Ramesh Krishnamurti , Sandor Nagy , John Tyrell , Bradley P. Etherton
发明人： Ramesh Krishnamurti , Sandor Nagy , John Tyrell , Bradley P. Etherton
IPC分类号： B01J31/14 , B01J31/22 , C07F7/00 , C07F17/00 , C08F4/642 , C08F4/659 , C08F10/00 , C08F110/02 , B01J31/00
CPC分类号： B01J31/143 , B01J31/14 , B01J31/226 , B01J31/2295 , C07F17/00 , C07F7/006 , C08F10/00 , B01J2531/0236 , B01J2531/46 , B01J2531/48 , C08F2420/04 , C08F4/65908 , C08F4/65912 , C08F4/65916
摘要： A novel metallocene catalyst for the polymerization of olefin (co)polymers is of the general formula:Benzothiazole--E--M--X.sub.m L.sub.nwhere,M is a transition metal of Groups 3-10 of the Periodic Table;E is sulfur or oxygen; E being bond to the transition metal and to the carbon atom between sulfur and nitrogen of the benzothiazole moiety;L is a polymerization-stable anionic ancillary ligand;X is a halogen, alkoxy from C.sub.1 to C.sub.20, siloxy from C.sub.1 to C.sub.20, N(R.sub.1).sub.2, a hydrocarbyl group containing up to about 12 carbon atoms or hydrogen or mixtures thereof; preferably X is halogen, methoxy, ethoxy or siloxy (R.sub.1).sub.3 SiO--, where R.sub.1 is alkyl from C.sub.1 to C.sub.20 ; andm+n equals the valency of the M minus 1.
摘要翻译：用于烯烃（共）聚合物聚合的新型茂金属催化剂具有以下通式：苯并噻唑-E-M-XmL，其中M是周期表第3-10族的过渡金属; E是硫或氧; E键合到过渡金属和苯并噻唑部分的硫和氮之间的碳原子; L是聚合稳定的阴离子辅助配体; X是卤素，C1至C20的烷氧基，C1至C20的甲硅烷氧基，N（R1）2，含有至多约12个碳原子的烃基或氢或其混合物; 优选X是卤素，甲氧基，乙氧基或甲硅烷氧基（R1）3SiO-，其中R1是C1至C20的烷基; 而m + n等于M的化合价减1。

5. 发明授权

US5773637A Perfluoroalkyl sulfonates, their preparation and use 失效
标题翻译：全氟烷基磺酸盐，其制备和用途
公开(公告)号：US5773637A
公开(公告)日：1998-06-30
申请号：US708997
申请日：1996-09-06
申请人： Walter Vladimir Cicha , Andreas Josef Kornath , Ronald James McKinney , V. N. Mallikarjuna Rao , Joseph Stuart Thrasher , Alfred Waterfeld
发明人： Walter Vladimir Cicha , Andreas Josef Kornath , Ronald James McKinney , V. N. Mallikarjuna Rao , Joseph Stuart Thrasher , Alfred Waterfeld
IPC分类号： C07F5/00 , C07F7/00 , C07F9/00 , C07F9/68 , C07F9/90 , C07F9/94 , C07F11/00 , C07F9/70 , C07F7/22
CPC分类号： C07F5/003 , C07F11/005 , C07F7/006 , C07F9/005 , C07F9/68 , C07F9/902 , C07F9/94
摘要： A process is disclosed for preparing a perfluoroalkyl sulfonate of the formula R.sub.a MX.sub.b-c O.sub.g �(SO.sub.3).sub.d (R.sub.f).sub.e !.sub.c. This process involves reacting a reagent of the fonnula R.sub.a MX.sub.b O.sub.g and a second reagent of the formula R'.sub.x E�(SO.sub.3).sub.d (R.sub.f).sub.e !.sub.y, where R is selected from the group consisting of C.sub.1 to C.sub.6 alkyl, C.sub.1 to C.sub.6 perfluoroalkyl, cyclopentadienyl (i.e., C.sub.5 H.sub.5), phenyl and perfluorophenyl; M is selected from the group consisting of transistion metals of groups 3 to 12, main group elements of group 13 to 16 and lanthanide metals; X is selected from the group consisting of F, Cl and Br; R.sub.f is selected from the group consisting of C.sub.h F.sub.2h+1, C.sub.h F.sub.2h, wherein h is an integer from 0 to 10, perfluorophenyl, C.sub.6 F.sub.4 (CF.sub.2).sub.2 i, wherein i is an integer from 0 to 6, provided that when E is boron, R.sub.f is selected from the group consisting of C.sub.h' F.sub.2h'+1, wherein h' is an integer from 1 to 10, perfluorophenyl; R' is selected from the group consisting of C.sub.j H.sub.2j+1, wherein j is an integer from 1 to 4, and phenyl; E is selected from the group consisting of B and Si; a is an integer from 0 to 3; b is an integer from 2 to 6; c is an integer from 1 to 6; d is an integer from 1 to 3; e is an integer from 1 to 4; g is an integer from 0 to 1; x is an integer from 0 to 3; and y is an integer from 1 to 3. Novel perfluoroalkyl sulfonates are provided, as are methods which employ perfluoroalkyl sulfonates as catalysts for increasing the fluorine content of halogenated hydrocarbons and as promoters for hydrocyanation of olefins.
摘要翻译：公开了制备式RaMXb-cOg [（SO3）d（Rf）e] c的全氟烷基磺酸盐的方法。该方法包括使得式IaMXbOg的试剂与式R'xE [（SO3）d（Rf）e] y的第二试剂反应，其中R选自C1至C6烷基，C1至C6全氟烷基，环戊二烯基（即C 5 H 5），苯基和全氟苯基; M选自组3至12的交联金属，第13至16族的主要元素和镧系金属; X选自F，Cl和Br; Rf选自ChF2h + 1，ChF2h，其中h为0至10的整数，全氟苯基，C6F4（CF2）2i，其中i为0至6的整数，条件是当E为硼时，Rf 选自Ch'F2h'+ 1，其中h'是1至10的整数，全氟苯基; R'选自CjH2j + 1，其中j是1至4的整数，和苯基; E选自B和Si; a是从0到3的整数; b是2至6的整数; c是1至6的整数; d为1〜3的整数; e是1至4的整数; g是0到1的整数; x是0到3的整数; y是1至3的整数。提供新的全氟烷基磺酸盐，使用全氟烷基磺酸盐作为用于增加卤代烃的氟含量的催化剂和作为烯烃氢化氰化促进剂的方法。

6. 发明授权

US5770678A Polymerization of, and depolymerization to, cyclic ethers using selected metal compound catalysts 失效
公开(公告)号：US5770678A
公开(公告)日：1998-06-23
申请号：US762813
申请日：1996-12-09
申请人： Neville Everton Drysdale , Richard Edmund Bockrath , Norman Herron , Joel David Citron
发明人： Neville Everton Drysdale , Richard Edmund Bockrath , Norman Herron , Joel David Citron
IPC分类号： C07D307/06 , C07D307/08 , C07F7/00 , C07F17/00 , C08G63/42 , C08G63/58 , C08G63/685 , C08G65/16 , C08G65/18 , C08G65/20 , C08G65/26 , C08G65/32 , C08G65/321 , C08G65/323 , C08G65/337 , C08G4/00
CPC分类号： C07D307/08 , C07D307/06 , C07F17/00 , C07F7/006 , C08G63/42 , C08G63/58 , C08G63/6856 , C08G65/16 , C08G65/18 , C08G65/20 , C08G65/2645 , C08G65/2648 , C08G65/266 , C08G65/32 , C08G65/321 , C08G65/323 , C08G65/337
摘要： A process for polymerizing oxiranes, oxetanes, oxepanes, dioxolanes, trioxanes, and tetrahydrofurans to their respective polymers by contacting them with a selected metal compound is disclosed; and also a process for depolymerizing polytetrahydrofurans to monomeric tetrahydrofurans by contacting the polymer with a selected metal compound at a temperature of about 100.degree. C. to about 250.degree. C. The catalysts may be in solution or part of a heterogeneous solid, and selected organic compounds are used as accelerators in the polymerizations. The polymeric products, some of which are novel, may be used as polyether monomers for further polymerization, as by reaction with isocyanates to produce polyurethanes, and other useful polymers. Some of the polymeric products are relatively high in molecular weight and are suitable for direct use, for instance as spandex fibers.

7. 发明授权

US5721268A C7 taxane derivatives and pharmaceutical compositions containing them 失效
标题翻译： C7紫杉烷衍生物和含有它们的药物组合物
公开(公告)号：US5721268A
公开(公告)日：1998-02-24
申请号：US462123
申请日：1995-06-05
申请人： Robert A. Holton , Ki-byung Chai
发明人： Robert A. Holton , Ki-byung Chai
IPC分类号： A61P35/02 , C07C227/22 , C07C231/12 , C07C233/87 , C07C271/22 , C07D205/08 , C07D305/14 , C07D407/12 , C07D409/12 , C07F7/00 , C07F7/18 , A61K31/335
CPC分类号： C07C271/22 , C07C227/22 , C07C231/12 , C07C233/87 , C07D205/08 , C07D305/14 , C07D407/12 , C07D409/12 , C07F7/006 , C07F7/1856 , C07F7/186 , C07C2101/14 , C07C2101/16 , C07C2103/62
摘要： Taxane derivatives having alternative C7 substituents.
摘要翻译：具有替代C7取代基的紫杉烷衍生物。

8. 发明授权

US5691436A Production of silicon-phosphorus containing compositions 失效
标题翻译：生产含硅磷的组合物
公开(公告)号：US5691436A
公开(公告)日：1997-11-25
申请号：US767416
申请日：1996-12-16
申请人： David H. Blount
发明人： David H. Blount
IPC分类号： C07F7/00 , C07F9/06 , C07F9/09 , C07F9/28 , C07F9/40 , C07F7/08 , C07F7/10
CPC分类号： C07F9/409 , C07F7/006 , C07F9/06 , C07F9/095 , C07F9/28
摘要： A mixture of silicon and phosphorus are heated and reacted with halide to produce silicon tetrahalides, silicon-phosphorus halide and phosphorus trihalides compositions. These compositions are reacted with any suitable organic, inorganic-organic and/or inorganic compound to produce novel organic silicon-phosphorus containing compositions. These compositions may be utilized as flame retardants, coating agents, adhesives and many other uses.
摘要翻译：将硅和磷的混合物加热并与卤化物反应以产生四卤化硅，硅 - 磷卤化物和三卤化磷组合物。这些组合物与任何合适的有机，无机 - 有机和/或无机化合物反应以制备新的含有机硅磷的组合物。这些组合物可以用作阻燃剂，包衣剂，粘合剂和许多其它用途。

9. 发明授权

US5367085B1 Preparation of TiCl3 coordination complexes 失效
标题翻译：制备TiCl3配位络合物
公开(公告)号：US5367085B1
公开(公告)日：1997-02-25
申请号：US12366693
申请日：1993-09-20
申请人： ALBERMARLE CORP
发明人： STRICKLER JAMIE R
IPC分类号： C01G23/00 , C07C43/04 , C07C43/11 , C07F7/00 , C07F7/28 , C07F17/00 , C07F3/00
CPC分类号： C07F7/006
摘要： Prepn. of TiCl3 coordination complexes with ethers, comprises adding TiCl3.1/3AlCl3 to an ether solvent to form a solid coordination complex. The solvent comprises a 4-10C cyclic or acyclic ether.

10. 发明授权

US5521136A Process for the preparation of organotitanium compounds and their use in cathodically depositable electrodeposition coating materials 失效
标题翻译：用于制备有机钛化合物的方法及其在阴极沉积电沉积涂料中的应用
公开(公告)号：US5521136A
公开(公告)日：1996-05-28
申请号：US294863
申请日：1994-08-29
申请人： Roland Feola , Willibald Paar , Johann Gmoser
发明人： Roland Feola , Willibald Paar , Johann Gmoser
IPC分类号： C07C31/28 , C07C213/04 , C07C217/28 , C07F7/00 , C09D5/44 , B01J31/00
CPC分类号： C07C213/04 , C07C217/28 , C07C31/28 , C07F7/006 , C09D5/4492
摘要： A process for the preparation of organotitanium compounds and to their use as crosslinking catalysts in cathodically depositable electro-deposition coating materials is described. The organotitanium compounds are obtained by first carrying out partial transesterification of tetraalkyl orthotitanates with alkylene glycols which are capable of forming chelates, and then completing the transesterification of the resulting intermediate with hydroxyl compounds based on modified mono- and/or diepoxide compounds.Cathodically depositable electrodeposition coating materials which contain the organotitanium compounds prepared in accordance with the invention provide, after curing in a temperature range from 160.degree. to 180.degree. C., coating films having excellent stability and the like properties, without the need to use additional crosslinking catalysts based on heavy metals such as lead or tin.
摘要翻译：描述了制备有机钛化合物的方法及其作为阴极沉积的电沉积涂料中的交联催化剂的用途。有机钛化合物通过首先进行四烷基原钛酸酯与能够形成螯合物的亚烷基二醇的部分酯交换获得，然后基于改性的单 - 和/或二环氧化合物完成所得中间体与羟基化合物的酯交换反应。包含根据本发明制备的有机钛化合物的阴极沉积的电沉积涂料在160℃至180℃的温度范围内固化后，提供具有优异稳定性和类似性能的涂膜，而不需要使用额外的交联基于重金属如铅或锡的催化剂。

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