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1. 发明公开

CN117917396A 新型的发光元件用化合物以及包含所述发光元件用化合物的有机发光元件审中-公开
公开(公告)号：CN117917396A
公开(公告)日：2024-04-23
申请号：CN202311333471.X
申请日：2023-10-16
申请人：东进世美肯株式会社
发明人：咸昊完 , 安贤哲 , 闵丙哲 , 李萤振 , 安慈恩 , 权桐热 , 李知垠 , 李卓宰
IPC分类号： C07C69/753 , C07C323/17 , C07C219/24 , C07C255/46 , C07C205/41 , C07F7/08 , C07C69/757 , C07C323/61 , C07C229/48 , C07C205/55 , C07D211/46 , C07D295/24 , C07D309/12 , C07D213/64 , C07D213/68 , C07D239/34 , C07D241/18 , C07D251/22 , C07D307/58 , C07D333/32 , C07D263/38 , C07D277/34 , C07D271/113 , C07D285/13 , C07D249/12 , C07D215/32 , C07D307/83 , C07D333/64 , C07D209/34 , C07D235/26 , C07D263/58 , C07D277/68 , C07D249/18 , C07D519/00 , C07D307/91 , C07D333/76 , C07D209/88 , C07D209/86 , C07C327/24 , C07D335/02 , C07C323/22 , C07C409/38 , C07C381/00 , C07C61/135 , C07C69/716 , C07C327/14 , C07C327/22 , C07C327/36 , C07C257/06 , C07C43/188 , C07C391/00 , C07C395/00 , C09K11/06 , H10K85/60 , H10K85/40 , H10K50/17 , H10K50/15 , H10K50/11 , H10K50/16
摘要：本发明提供一种以下述化学式1表示的发光元件用化合物以及包含所述发光元件用化合物的有机发光元件。 #imgabs0#

2. 发明公开

CN117658817A 新型的发光元件用化合物以及包含所述发光元件用化合物的有机发光元件审中-公开
公开(公告)号：CN117658817A
公开(公告)日：2024-03-08
申请号：CN202311149763.8
申请日：2023-09-07
申请人：东进世美肯株式会社
发明人：咸昊完 , 安贤哲 , 闵丙哲 , 李萤振 , 安慈恩 , 权桐热 , 李知垠 , 李卓宰
IPC分类号： C07C69/80 , C07C69/82 , C07C323/17 , C07C219/24 , C07C255/46 , C07C205/41 , C07F7/08 , C07D295/24 , C07D335/02 , C07D309/12 , C07D213/68 , C07D307/58 , C07D333/32 , C07D263/38 , C07D277/34 , C07D285/13 , C07D215/20 , C07D333/76 , C07D307/91 , C07D249/18 , C07D235/26 , C07D277/68 , C07D307/83 , C07D333/64 , C07D519/00 , C07D209/86 , C07C69/76 , C07C69/753 , C07D295/205 , C07D213/79 , C07D307/68 , C07D333/38 , C07D277/56 , C07D263/34 , C07D271/10 , C07D285/12 , H10K85/60 , C07C329/18 , H10K50/844
摘要：本发明提供一种以下述化学式1表示的发光元件用化合物以及包含所述发光元件用化合物的有机发光元件。

3. 发明公开

CN103864621A 含能材料4,4,8,8-四硝基金刚烷-2,6-二硝酸酯及其制备方法失效
公开(公告)号：CN103864621A
公开(公告)日：2014-06-18
申请号：CN201410059009.X
申请日：2014-02-21
申请人：南京理工大学
发明人：罗军 , 凌亦飞 , 任晓莉 , 张萍萍 , 孙露 , 何晓茜 , 居平文 , 万子娟 , 邹坡
IPC分类号： C07C201/06 , C07C205/41 , C06B25/34
摘要：本发明公开了一种含能材料4,4,8,8-四硝基金刚烷-2,6-二硝酸酯及其制备方法。所述方法以环辛二烯为原料，经过硼氢化氧化、氧化、甲酰化、环合、硝酸酯化、肟化和偕硝化等步骤，最终合成出4,4,8,8-四硝基金刚烷-2,6-二硝酸酯。多硝基金刚烷及金刚烷硝酸酯具有结构对称，密度高，爆炸性能优异，低感度等优点，可广泛用于炸药、推进剂、烟火剂和燃料等领域中。

4. 发明公开

CN117917394A 新型的发光元件用化合物以及包含所述发光元件用化合物的有机发光元件审中-公开
公开(公告)号：CN117917394A
公开(公告)日：2024-04-23
申请号：CN202311333421.1
申请日：2023-10-16
申请人：东进世美肯株式会社
发明人：咸昊完 , 安贤哲 , 金熙宙 , 安慈恩 , 权桐热 , 李成圭 , 李知垠 , 李卓宰
IPC分类号： C07C69/75 , C07C69/757 , C07C323/61 , C07C229/48 , C07C255/46 , C07C205/55 , C07F7/08 , C07C323/17 , C07C219/24 , C07C205/41 , C07D211/62 , C07D295/205 , C07D309/08 , C07D335/02 , C07D213/79 , C07D213/80 , C07D239/28 , C07D241/24 , C07D251/24 , C07D307/68 , C07D333/38 , C07D263/34 , C07D277/56 , C07D271/10 , C07D285/12 , C07D249/10 , C07D215/48 , C07D215/54 , C07D239/72 , C07D241/44 , C07D263/58 , C07D277/68 , C07D235/24 , C07D249/18 , C07D519/00 , C07C69/608 , C07C69/96 , C07C329/08 , C07C327/24 , C07C257/06 , C07C43/188 , C07C391/00 , C07C395/00 , C09K11/06 , H10K85/60 , H10K85/40 , H10K50/15 , H10K50/11 , H10K50/16 , H10K50/17
摘要：本发明提供一种以下述化学式1表示的发光元件用化合物以及包含所述发光元件用化合物的有机发光元件。 #imgabs0#

5. 发明授权

CN103864621B 含能材料4,4,8,8-四硝基金刚烷-2,6-二硝酸酯及其制备方法失效
公开(公告)号：CN103864621B
公开(公告)日：2016-03-02
申请号：CN201410059009.X
申请日：2014-02-21
申请人：南京理工大学
发明人：罗军 , 凌亦飞 , 任晓莉 , 张萍萍 , 孙露 , 何晓茜 , 居平文 , 万子娟 , 邹坡
IPC分类号： C07C201/06 , C07C205/41 , C06B25/34
摘要：本发明公开了一种含能材料4,4,8,8-四硝基金刚烷-2,6-二硝酸酯及其制备方法。所述方法以环辛二烯为原料，经过硼氢化氧化、氧化、甲酰化、环合、硝酸酯化、肟化和偕硝化等步骤，最终合成出4,4,8,8-四硝基金刚烷-2,6-二硝酸酯。多硝基金刚烷及金刚烷硝酸酯具有结构对称，密度高，爆炸性能优异，低感度等优点，可广泛用于炸药、推进剂、烟火剂和燃料等领域中。

6. 发明专利

JPS54106452A 22NITROETHYLCYCLOPENTANE DERIVATIVE 失效
公开(公告)号：JPS54106452A
公开(公告)日：1979-08-21
申请号：JP1232778
申请日：1978-02-08
申请人： SAGAMI CHEM RES
发明人： KONDOU SEI , TSUNEMOTO DAIEI , UMEMOTO TERUO
IPC分类号： C07C205/41 , C07C67/00 , C07C201/00 , C07C205/44 , C07C205/45
摘要： NEW MATERIAL:The compound of formula I [X is C=O, CH(OH); R, R is H, OH-protecting group; R is alkyl; R is H, alkyl]. EXAMPLE:2alpha-(2-Nitroethyl)-3beta-[3alpha-(1-ethoxyethyloxy)-1-trans -octenyl]-4alpha-(1- ethoxyethyloxy)cyclopentan-1-one. USE:Intermediate of prostaglandins. PROCESS:An objective compound III, wherein X is C=O, is prepared by reacting a compound II with nitromethane in the presence of a base such as NaOH in a solvent such as alcohol, at room temperature. The compound III can be converted to the compound IV where X is CH(OH), by the selective reduction using a reducing agent such as lithium perhydro-9b-boraphenylyl hydride, etc.

7. 发明专利

JPS4817254B1 失效
公开(公告)号：JPS4817254B1
公开(公告)日：1973-05-28
申请号：JP285670
申请日：1970-01-09
IPC分类号： C07C69/34 , B01J23/00 , B01J27/00 , C07B41/00 , C07B43/02 , C07B61/00 , C07C45/54 , C07C51/09 , C07C51/31 , C07C53/126 , C07C55/02 , C07C69/12 , C07C69/14 , C07C205/03 , C07C205/05 , C07C205/40 , C07C205/41 , C07C205/45 , C07C205/51 , C07D321/00
摘要： 1,206,783. Preparation of α,#-disubstituted alkanes. TECHNI-CHEM CO. 3 Oct., 1967 [10 Oct., 1966; 2 Feb., 1967; 29 May, 1967; 15 Aug., 1967], No. 45033/67. Heading C2C. Compounds of the formula wherein X is an electronegative group selected from -NO 2 and -COOR 1 , where R 1 is a C 1-12 hydrocarbon radical, n is an integer from 2 to 17 when X is -NO 2 or an integer from 7 to 17 when X is -COOR 1 , Z is -OH, -OR 1 , -NH 2 , -NHR 1 , -NR 1 2 or -NR 1 R 11 and R 11 is a hydrocarbon radical different from R 1 , are obtained by reacting a compound of the formula with an agent selected from water, aqueous ammonia, an aqueous amine of the formula R 1 NH 2 , R 1 R 11 NH or R 1 2 NH, or a compound providing RO - ions or OH- ions and an alkali metal and where necessary, with a protic solvent providing H + cations, for example an alkanol having less than 7 carbon atoms, water or ammonium hydroxide. The reaction may be carried out in one step in a protic solvent or in two steps by carrying out the first stage of the reaction in an aprotic solvent. The starting materials in which X is an ester group may be obtained by reaction of the corresponding cyclic ketone with a dialkyl carbonate; starting materials wherein X is a nitro group may be prepared by nitration of the corresponding ester derivative. The products of the invention may be further worked up, for example, by hydrolysis of ester derivatives to the free acids or by reduction of the nitro derivatives to give the corresponding amino-derivatives; cyclic ethylene brassylate may be obtained by heating brassylic acid with ethylene glycol followed by depolymerization by heating.

8. 发明专利

JPH09249602A PRODUCTION OF INDENE COMPOUND AND SYNTHETIC INTERMEDIATE COMPOUND FOR THE SAME 失效
公开(公告)号：JPH09249602A
公开(公告)日：1997-09-22
申请号：JP8047196
申请日：1996-03-11
申请人： TEIJIN LTD
发明人： OKAMOTO MASATO , OSHIDA JUNICHI , TANAKA TOSHIO
IPC分类号： B01J31/22 , C07B53/00 , C07B61/00 , C07C35/27 , C07C67/297 , C07C69/78 , C07C201/12 , C07C205/41 , C07F7/18
摘要： PROBLEM TO BE SOLVED: To obtain the subject compound simply and highly stereoselectively, useful as a synthetic intermediate for CD ring part in the synthesis of 1α, 24- dihydroxyvitamin D3 effective as a medicine. SOLUTION: This indene compound expressed by formula I (R is H, a 2-8C acyl, etc.; A, B are each H or a C-C bond by A and B, etc.; * shows isomers originated from an asymmetric carbon present with a deviation to one of the isomers) is obtained by reacting a compound expressed by formula II with 2-nitro propane in the presence of a double nuclear catalyst constituted by (R) or (S)-binaphthol derivative expressed by formula III R is H, trimethylsilylethinyl, etc.; Ln is lanthanum or samarium} as an asymmetric source to obtain a nitroaldol compound expressed by formula IV, and removing nitro group thereof by reacting with a hydrogenated tributyltin in the presence of a radical initiator.

9. 发明专利

JPH08507773A 失效
公开(公告)号：JPH08507773A
公开(公告)日：1996-08-20
申请号：JP52061594
申请日：1994-03-12
IPC分类号： C07D333/16 , A61K31/04 , A61K31/05 , A61K31/075 , A61K31/085 , A61K31/21 , A61K31/22 , A61K31/34 , A61K31/38 , A61K31/381 , A61K31/382 , A61K31/44 , A61K31/4409 , A61K31/4418 , A61P27/02 , C07C203/04 , C07C205/06 , C07C205/37 , C07C205/41 , C07C205/42 , C07C205/59 , C07C205/60 , C07C219/16 , C07C233/69 , C07C323/20 , C07D213/30 , C07D335/12

10. 发明专利

JPH01135745A NOVEL LIQUID CRYSTAL COMPOUND AND LIQUID CRYSTAL COMPOSITION 失效
公开(公告)号：JPH01135745A
公开(公告)日：1989-05-29
申请号：JP29317887
申请日：1987-11-20
申请人： AJINOMOTO KK
发明人： YOKOTA TADAHIKO , SAKURAI TAKAO , KOMATSU SHIGEMICHI , HONMA MASAO
IPC分类号： C07C331/26 , C07C67/00 , C07C69/675 , C07C69/84 , C07C69/96 , C07C201/00 , C07C205/41 , C07C241/00 , C07C251/24 , C07C253/00 , C07C255/10 , C07C255/24 , C07C255/38 , C07C255/43 , C07C255/55 , C07C255/59 , C07C255/61 , C07C325/00 , C07C331/28 , C07D239/26 , C07D239/34 , C07D241/12 , C07D241/18 , C09K19/20 , C09K19/34 , C09K19/46 , C09K19/54
摘要： NEW MATERIAL:A compound expressed by formula I (R1 and R2 are straight- chain or branched 1-18C alkyl, optically active alkyl halide, alkoxyalkyl, cyano or isothiocyanate; a, b and c are 0, 1 or 2; a+b+c is >=2; A is single bond, -O-, -COO-, -O-COO- or -OCO-; B and D are single bond, -COO-, -OCO-, -N=CH-, -CH=CH-, etc.; X, Y and Z are 1,4-phenylene, 1,4-trans-cyclohexyl, 2,5-pyrimidine, 2,5-pyridine or 2,5-pyrazine). EXAMPLE:2-(4'-Decyloxyphenyl)-5-hexyloxymethylenecarbonyloxypyrimidine. USE:A liquid crystal compound. PREPARATION:An alcohol derivative expressed by formula II is condensed with an alkoxyacetic acid expressed by formula III using a condensing agent, such as N,N'-dicyclohexylcarbodiimide, to afford the aimed compound expressed by formula I.

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