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91. 发明授权

US4224259A Manufacture of fibrids from polymers 失效
标题翻译：从聚合物制备纤条体
公开(公告)号：US4224259A
公开(公告)日：1980-09-23
申请号：US944644
申请日：1978-09-18
申请人： Bruno Sander , Eckhard Bonitz , Kurt Scherling
发明人： Bruno Sander , Eckhard Bonitz , Kurt Scherling
IPC分类号： D01D5/40 , D01F6/10 , D01F6/22 , B29C6/00
CPC分类号： D01D5/40 , D01F6/10 , D01F6/22
摘要： Fibrids of polymers of styrene, which are obtained in a fluid precipitation medium under the action of shearing forces.
摘要翻译：在剪切力作用下在流体沉淀介质中获得的苯乙烯聚合物的纤维。

92. 发明授权

US4219512A Manufacture of fibrids from polymers 失效
标题翻译：从聚合物制备纤条体
公开(公告)号：US4219512A
公开(公告)日：1980-08-26
申请号：US839661
申请日：1977-10-05
申请人： Richard Sinn , Otto Nagel , Bruno Sander , Eckhard Bonitz , Kurt Scherling , Hans D. Zettler , Dieter Stoehr , Heinz Berbner
发明人： Richard Sinn , Otto Nagel , Bruno Sander , Eckhard Bonitz , Kurt Scherling , Hans D. Zettler , Dieter Stoehr , Heinz Berbner
IPC分类号： D01F6/08 , D01D5/26 , D01D5/40 , D01F6/12 , D01F6/22 , D01F6/56 , D21H13/10 , B22D23/08
CPC分类号： D01F6/12 , D01D5/40 , D21H5/20
摘要： Manufacture of fibrids from polymers or copolymers containing fluorine in a fluid precipitation medium under the action of shearing forces.
摘要翻译：在剪切力的作用下，在流体沉淀介质中由含氟的聚合物或共聚物制备纤条体。

93. 发明授权

US4198461A Polymeric fiber masses, fibers therefrom, and processes for producing the same 失效
标题翻译：聚合纤维团，纤维，及其制造方法
公开(公告)号：US4198461A
公开(公告)日：1980-04-15
申请号：US905702
申请日：1978-05-15
申请人： Leon B. Keller , Robert K. Jenkins
发明人： Leon B. Keller , Robert K. Jenkins
IPC分类号： B29C67/00 , B29C70/36 , B29C70/38 , D01D5/40 , D04H13/00 , B28B1/08 , B06B3/00 , B32B5/26 , B32B5/28
CPC分类号： D04H13/00 , B29C67/00 , B29C70/36 , D01D5/40 , B29C2791/008 , B29K2105/0002 , B29K2223/00 , B29K2301/12 , B29K2995/0041 , B29K2995/0045 , Y10S428/91 , Y10T428/2907 , Y10T428/2913 , Y10T428/31855 , Y10T428/31913 , Y10T428/31931 , Y10T428/31938 , Y10T442/60
摘要： We have prepared a new class of polymeric fibers and masses which are produced by precipitation from solutions of the polymer. The fibers and fiber masses have novel and useful characteristics. A fiber mass of this invention is a coherent, three-dimensional network of interconnected crystalline polymeric fibers and fiber bundles randomly arrayed in all directions. The fibers are smaller in diameter than can be consistently produced by conventional fiber drawing and spinning techniques.The novel fiber masses are produced from solutions of fiber-forming linear organic polymers having regularly repeated chain structures. The polymers are precipitated from these solutions by simultaneously cooling and agitating the polymer solution at vibrations in the sonic frequency range. The fiber masses may then be removed from the solvent or, in the case of a polymerizable solvent, a composite may be formed.
摘要翻译：我们已经准备了一类新的聚合物纤维和质量，它们是通过从聚合物溶液中沉淀制成的。纤维和纤维质量具有新颖和有用的特性。本发明的纤维块是相互连接的三维互连结晶聚合物纤维和纤维束的网络，其随机排列在所有方向上。纤维的直径小于通过常规纤维拉伸和纺丝技术一贯产生的直径。新型纤维质量由具有规则重复链结构的成纤线性有机聚合物溶液制成。通过在声波频率范围内的振动下同时冷却和搅拌聚合物溶液，从这些溶液中沉淀聚合物。然后可以将纤维物质从溶剂中除去，或者在可聚合溶剂的情况下，可以形成复合材料。

94. 发明授权

US4187143A Manufacture of fibrids from poly(amide-imide) resins 失效
标题翻译：从聚（酰胺 - 酰亚胺）树脂制备纤维质
公开(公告)号：US4187143A
公开(公告)日：1980-02-05
申请号：US831749
申请日：1977-09-09
申请人： Bruno Sander , Kurt Scherling , Rolf Steinberger , Eckhard Ropte
发明人： Bruno Sander , Kurt Scherling , Rolf Steinberger , Eckhard Ropte
IPC分类号： D01D5/40 , D01F6/90 , D21B1/00 , D21H13/26 , D21F11/00
CPC分类号： D01F6/90 , B01J19/1806 , B01J19/2405 , D01D5/40 , D21B1/00 , D21H13/26 , Y10T428/2978 , Y10T428/298
摘要： Fibrids are prepared by introducing a solution of a polymer into a liquid precipitation medium while exposing it to shearing forces. A poly(amide-imide) resin solution is admixed with a solvent which is miscible with the resin solvent but which is a non-solvent for the resin itself.
摘要翻译：通过将聚合物溶液引入液体沉淀介质中同时将其暴露于剪切力来制备纤维素。将聚（酰胺 - 酰亚胺）树脂溶液与可与树脂溶剂混溶但是树脂本身的非溶剂的溶剂混合。

95. 发明授权

US4125584A Process for the manufacture of fibrils 失效
标题翻译：原纤维制造工艺
公开(公告)号：US4125584A
公开(公告)日：1978-11-14
申请号：US812031
申请日：1977-07-01
申请人： Robert E. Boehme , Clarence R. Murphy
发明人： Robert E. Boehme , Clarence R. Murphy
IPC分类号： D01F6/04 , D01D5/18 , D01D5/40 , C08G51/12 , B24D3/00
CPC分类号： D01D5/40 , Y10S264/47
摘要： Centrifugal spinning apparatus is provided for the manufacture of fibrils from hot viscous hydrocarbon solutions of olefin polymers having an intrinsic viscosity of at least 3.5. The apparatus consists of an impeller which rotates at high speed in a cylindrical cavity having a discharge port. The impeller has a plurality of blades whose narrow dimensions lie substantially in the plane of the impeller's rotation and whose tips come in close proximity to the inner peripheral surface of the cylindrical cavity. The blades are arranged in at least two substantially-identical sets. Within each set, the blades are offset substantially equidistant from one another, both in the rotational plane of the impeller and in the plane transverse thereto. Two inlet ports are provided in the peripheral surface of the cylindrical cavity to feed liquids to the cylindrical cavity, each of which port is narrow in a plane transverse to the plane of the impeller's rotation and extends over substantially the entire peripheral surface. The inlet ports are positioned near the discharge port of the cylindrical cavity and upstream thereof viewed with respect to the impeller's rotation, so that the bulk of the liquids entering the cavity from the inlet ports are swept away from the discharge port by the impeller's rotation.
摘要翻译： {PG，1离心纺丝设备用于从特性粘度至少为3.5的烯烃聚合物的热粘性烃溶液制造原纤维。该装置由在具有排出口的圆柱形空腔中高速旋转的叶轮组成。叶轮具有多个叶片，其狭窄尺寸基本上位于叶轮的平面（3s旋转中，并且其尖端靠近圆柱形腔的内周表面）。叶片布置在至少两个基本相同的组中。在每组中，叶片在叶轮的旋转平面中和横向于其的平面中彼此基本等距离地偏移。两个入口端口设置在圆柱形空腔的圆周表面中，以将液体供给到圆柱形腔体，每个孔口在垂直于叶轮平面的平面（3s旋转中并且在基本上整个圆周表面上延伸）的窄边。入口端口位于圆柱形腔的排出口附近，并且相对于叶轮（3s的旋转）观察其上游，使得从入口端口进入空腔的大部分液体从排出口被扫除叶轮{3 s旋转。

96. 发明授权

US4098640A Manufacture of paper-like and textile-like sheets 失效
标题翻译：制造纸样和纺织样片材
公开(公告)号：US4098640A
公开(公告)日：1978-07-04
申请号：US727583
申请日：1976-09-28
申请人： Bruno Sander , Heinz Berbner , Rolf Steinberger , Eckhard Ropte , Jenoe Kovacs , Joachim Kunde
发明人： Bruno Sander , Heinz Berbner , Rolf Steinberger , Eckhard Ropte , Jenoe Kovacs , Joachim Kunde
IPC分类号： D01D5/40 , D21H13/26 , D21F11/00
CPC分类号： D21H13/26 , D01D5/40
摘要： The manufacture of paper-like and textile-like sheet materials by the use of fibrids which have been obtained by dissolving poly(amide-imide) resins in an organic solvent, mixing the resulting solution with a liquid which is a non-solvent for the polymer and introducing the resulting solution into a liquid precipitation medium while exposing it to shearing forces.The present invention relates to the use, for the manufacture of paper-like and textile-like sheet materials, of novel fibrids, which have been obtained by dissolving poly(amide-imide) resins in an organic solvent, mixing the resulting solution with a liquid which is a non-solvent for the polymer and introducing the resulting solution into a liquid precipitation medium while exposing it to shearing forces.
摘要翻译：通过使用通过将聚（酰胺 - 酰亚胺）树脂溶解在有机溶剂中而获得的纤条体来制造纸状和织物状片状材料，将得到的溶液与作为非溶剂的液体混合聚合物并将所得溶液引入液体沉淀介质中，同时将其暴露于剪切力。

97. 发明授权

US4047862A Cellulose ester fibrillar structure 失效
标题翻译：纤维素酯纤维结构
公开(公告)号：US4047862A
公开(公告)日：1977-09-13
申请号：US638242
申请日：1975-12-08
申请人： Charles Herbert Keith
发明人： Charles Herbert Keith
IPC分类号： A24D3/10 , B01D39/18 , C08B3/24 , D01D5/40 , D21H13/06 , B29C23/00
CPC分类号： D21H13/06 , A24D3/10 , B01D39/18 , C08B3/24 , D01D5/40
摘要： Cellulose ester fibrillar material is produced by forming a cellulose ester dope, pumping the dope to an extrusion orifice, extruding the dope through the orifice into a region of shear and high draw in a precipitation bath containing a non-solvent for said cellulose ester maintained at an elevated temperature. The fibrillar material is preferably subjected to further treatment to reduce the particle size and set the structure by expanding voids and expelling residual solvent. Paper having a high degree of opacity is produced by incorporating the cellulose ester material to obtain light weight paper.
摘要翻译：通过形成纤维素酯原纤维材料来制备纤维素酯原纤维材料，通过将纺丝原液泵送到挤出孔口，将纺丝原液通过孔口挤出到剪切区域，并在含有维持在温度升高。优选对纤维状材料进行进一步处理以减小粒径并通过膨胀空隙并排出残余溶剂来设定结构。具有高度不透明度的纸通过掺入纤维素酯材料获得轻质纸来生产。

98. 发明授权

US3997648A Fibril formation process 失效
标题翻译：纤维形成过程
公开(公告)号：US3997648A
公开(公告)日：1976-12-14
申请号：US214925
申请日：1972-01-03
申请人： Joseph Calvin Davis , Francis Ross Galiano , Robert William Hill
发明人： Joseph Calvin Davis , Francis Ross Galiano , Robert William Hill
IPC分类号： D01F6/04 , C04B16/06 , D01D5/40 , D01F6/00 , D21H13/14 , B02C18/00
CPC分类号： D01D5/40 , D21H13/14 , D21H5/202
摘要： An improvement in the fibril formation process which includes dissolving at an elevated temperature an olefin polymer having an inherent viscosity of at least 3.5 in a hot hydrocarbon solvent, shearing the hot polyolefin solution to thereby orient the polymer molecules therein, passing the sheared solution through a cooling zone maintained at a temperature well below the precipitation temperature of the solution while maintaining the orientation of the polymer molecules within the solution to thereby precipitate by thermal means the polymer solute of the solution in the form of a solvent swollen fibrous strand, separating a substantial portion of the polymer solvent from the fibrous strand, chopping and then beating the chopped fibrous strand in a liquid which is a nonsolvent for the polymer and which is soluble in the polymer solvent for a time sufficient to break down the fibrous strand into a plurality of fibrils, and separating the fibrils from the nonsolvent liquid. The improvement consists of homogenizing the hot polyolefin/hydrocarbon solvent solution by passing same through a device, such as a gear pump, which imposes a high shear on the solution to thereby remove any small, invisible globules of partially dissolved polyolefin that may be present in the solution prior to the fibril formation steps of the process whereby paper sheets fabricated from the resultant fibrils are free of small knots and lumps and possess a completely smooth surface.
摘要翻译：原纤维形成方法的改进，其包括在高温下将热固性烃溶剂中特性粘度至少为3.5的烯烃聚合物溶解，剪切热聚烯烃溶液，从而使聚合物分子在其中定向，使剪切溶液通过冷却区保持在远低于溶液的沉淀温度的温度，同时保持聚合物分子在溶液中的取向，从而通过热法沉淀出溶剂溶胀的纤维束形式的溶液的聚合物溶质，部分聚合物溶剂从纤维链中切割，然后将该切碎的纤维束以对于聚合物为非溶剂的液体进行打浆，该液体可溶于聚合物溶剂中足以将纤维束分解成多个原纤维，并将原纤维与非溶剂液体分离。该改进包括将热的聚烯烃/烃溶剂溶液通过使其通过诸如齿轮泵的装置来均匀化，该装置在溶液上施加高剪切，从而除去可能存在的部分溶解的聚烯烃中的任何小的不可见小球在该方法的原纤维形成步骤之前的溶液，由此由所得原纤维制成的纸张不具有小结和块状并且具有完全光滑的表面。

99. 发明授权

US3743272A Process of forming polyolefin fibers 失效
标题翻译：形成聚烯烃纤维的工艺
公开(公告)号：US3743272A
公开(公告)日：1973-07-03
申请号：US3743272D
申请日：1971-04-12
申请人： CROWN ZELLERBACH CORP
发明人： NOWOTNY K , SHILLING W
IPC分类号： C08J3/14 , D01D5/40 , B28B1/08
CPC分类号： C08J3/14 , C08J2323/02 , D01D5/40
摘要： The process of forming polyolefin fibers comprising forming a solution of a linear, high molecular weight polyolefin in a solvent at a temperature above the melt dissolution temperature of the polyolefin, and dispersing the polyolefin solution in a precipitant under conditions of shear stress sufficient to form polyolefin fibers having a microfibrillar structure.
摘要翻译：形成聚烯烃纤维的方法包括在高于聚烯烃的熔体溶解温度的温度下在溶剂中形成线性高分子量聚烯烃溶液，并在足以形成聚烯烃的剪切应力条件下将聚烯烃溶液分散在沉淀剂中具有微原纤维结构的纤维。

100. 发明授权

US11618976B2 Method and device for protein fiber production 有权
公开(公告)号：US11618976B2
公开(公告)日：2023-04-04
申请号：US16651232
申请日：2018-10-09
申请人： SPIBER TECHNOLOGIES AB
发明人： My Hedhammar , Mathias Kvick , Fredrik Lundell
IPC分类号： D01D13/00 , D01D13/02 , D01D5/40 , D01F4/00
摘要： A method for producing a protein polymer fiber, the method comprising providing a liquid protein solution in a container for liquid, and repeatedly moving the liquid surface in the container back and forth between a first and a second position. Said movement of the liquid surface is such that the protein polymer solution is allowed to form a film in the interface between the liquid surface of the liquid protein solution and a surrounding fluid. The movement of the liquid surface being performed by respectively raising and lowering the liquid surface relative to the container or by moving an object extending through the liquid surface of the liquid protein solution. Also, a device for performing said method.

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