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21. 发明申请

US20140018499A1 Nucleation in Aqueous Polymerization of Fluoromonomer 有权
标题翻译：含氟单体的水聚合中的成核
公开(公告)号：US20140018499A1
公开(公告)日：2014-01-16
申请号：US14031335
申请日：2013-09-19
申请人： E I Du Pont De Nemours And Company
发明人： PAUL DOUGLAS BROTHERS , SUBHASH VISHNU GANGAL , DIPTI DILIP KHASNIS
IPC分类号： C08F2/16
CPC分类号： C08F2/16 , C08F14/18 , C08F2/26 , C08F2/28 , C08F2/30
摘要： A process is provided for polymerizing fluoromonomer in an aqueous medium, wherein a dispersion of essentially surfactant-free hydrocarbon-containing oleophilic nucleation sites is first formed in the aqueous medium, and then polymerization is commenced to form a dispersion of fluoropolymer particles at the oleophilic nucleation sites, wherein the nucleation sites can be derived from hydrocarbon-containing compound. The surfactant used to stabilize the fluoropolymer dispersion can also be hydrocarbon-containing.
摘要翻译：提供了一种用于在含水介质中聚合含氟单体的方法，其中首先在水性介质中形成基本上不含表面活性剂的含烃亲油成核位点的分散体，然后开始聚合以在亲油成核时形成含氟聚合物颗粒的分散体其中成核位点可以衍生自含烃化合物。用于稳定含氟聚合物分散体的表面活性剂也可以是含烃的。

22. 发明授权

US08524260B2 Method for encapsulating oils in an aqueous medium with hase polymer emulsions, products obtained, and uses thereof 有权
标题翻译：在具有高分子乳液的水性介质中包封油的方法，获得的产物及其用途
公开(公告)号：US08524260B2
公开(公告)日：2013-09-03
申请号：US12747651
申请日：2008-12-03
申请人： Jean Moro , David Platel , Jean-Marc Suau , Olivier Guerret
发明人： Jean Moro , David Platel , Jean-Marc Suau , Olivier Guerret
IPC分类号： A61K8/02 , A61K9/14 , A61K31/59 , C08F2/16 , C08G8/10 , C08G73/10 , C09D11/02 , C08L75/00
CPC分类号： B01J13/02 , C08F220/06 , C08F220/18 , C08F220/28
摘要： The invention consists of a method for manufacturing an aqueous formulation containing at least one oil, and comprising the steps of mixing at least one associative polymer, one oil, and water, encapsulating the oil by increasing the pH to a value greater than 8, potentially precipitating the mixture by reducing the pH to a value less than 6, and potentially isolating the resulting particles by removing the water. The aqueous formulations, as with the aqueous dispersions, and the resulting solid particles constitute other objects of the invention.
摘要翻译：本发明包括一种制备含有至少一种油的水性制剂的方法，并且包括以下步骤：将至少一种缔合聚合物，一种油和水混合，通过将pH增加至大于8的值来封装油，潜在地通过将pH降低至小于6的值来沉淀混合物，并通过除去水来潜在地分离所得颗粒。含水制剂与水性分散体一样，所得固体颗粒构成本发明的其它目的。

23. 发明授权

US08367784B2 Continuous dosing of extremely fast initiators during polymerization reactions 有权
标题翻译：在聚合反应期间连续计量极快的引发剂
公开(公告)号：US08367784B2
公开(公告)日：2013-02-05
申请号：US12911598
申请日：2010-10-25
申请人： Hans Westmijze , Andreas Petrus Van Swieten , Lambertus Meulenbrugge , Koen Antoon Kornelis Vanduffel
发明人： Hans Westmijze , Andreas Petrus Van Swieten , Lambertus Meulenbrugge , Koen Antoon Kornelis Vanduffel
IPC分类号： C08F2/16
CPC分类号： C08F14/06 , C08F2/18 , C08F2/28
摘要： The invention pertains to a process wherein initiators having a half-life from 0.0001 hour to 0.05 hour at the polymerization temperature are dosed to a polymerization mixture. The dosing of such initiator allows improved control of the polymerization rate and faster polymerization rates, and the process will render a polymer with very low residual initiator levels.
摘要翻译：本发明涉及一种方法，其中在聚合温度下具有0.0001小时至0.05小时半衰期的引发剂加入到聚合混合物中。这种引发剂的计量可以改进聚合速率的控制和更快的聚合速率，并且该方法将使具有非常低的残余引发剂水平的聚合物。

24. 发明申请

US20120329973A1 INITIATING SYSTEM FOR CATIONIC POLYMERIZATION AND POLYMERIZATION PROCESS 有权
标题翻译：用于阳离子聚合和聚合方法的起始体系
公开(公告)号：US20120329973A1
公开(公告)日：2012-12-27
申请号：US13497453
申请日：2010-09-21
申请人： Yixian Wu , Qiang Huang , Han Zhou , Ruting Jin , Ping He
发明人： Yixian Wu , Qiang Huang , Han Zhou , Ruting Jin , Ping He
IPC分类号： C08F2/16 , C09K3/00 , C08F110/10
CPC分类号： C08F10/10 , C08F210/12 , C08F4/12 , C08F2/20 , C08F236/08 , C08F4/14
摘要： The present invention discloses an initiating system for cationic polymerization and a polymerization process. The present application relates to an initiating system for cationic polymerization of cationic-polymerizable monomers, and a process for cationic polymerization of cationic-polymerizable monomers by using the initiating system. The present invention particular involves an initiating system for cationic polymerization of cationic-polymerizable monomers in an aqueous reaction medium, and a process for cationic polymerization of cationic-polymerizable monomers by using the initiating system in an aqueous reaction medium.
摘要翻译：本发明公开了一种阳离子聚合引发体系和聚合方法。本申请涉及阳离子可聚合单体的阳离子聚合引发体系，以及通过使用引发体系阳离子聚合的单体的阳离子聚合方法。本发明特别涉及阳离子聚合单体在水性反应介质中阳离子聚合的引发体系，以及通过在水性反应介质中使用引发体系阳离子聚合单体的阳离子聚合方法。

25. 发明申请

US20120157646A1 METHOD FOR PRODUCING FLUORINE-CONTAINING POLYMER 有权
标题翻译：生产含氟聚合物的方法
公开(公告)号：US20120157646A1
公开(公告)日：2012-06-21
申请号：US13392733
申请日：2010-08-25
申请人： Katsuhiko Imoto , Shumi Nishii , Yoshinari Fukuhara
发明人： Katsuhiko Imoto , Shumi Nishii , Yoshinari Fukuhara
IPC分类号： C08F2/16 , C08F214/28 , C08F2/24 , C08F214/26
CPC分类号： C08F214/18 , C08F14/18 , C08F14/22 , C08F14/24 , C08F14/26 , C08F214/227 , C08F214/287 , C08F2/16 , C08F2/24 , C08F2/22
摘要： An object of the present invention is to provide a method for producing a fluoropolymer which produces a large number of particles with a small particle size using a specific non-fluorous compound having surfactant ability. The method for producing a fluoropolymer includes aqueous dispersion polymerization of a monomer including at least one fluoroolefin in the presence of a compound represented by the formula: CH2═CHCH2—O—(C═O)CHXCH2COO(CH2)nCH3 (in the formula, X is H or SO3Y wherein Y is NH4 or an alkaline metal; and n is an integer of 0 to 19.)
摘要翻译：本发明的目的是提供一种使用具有表面活性剂的特定非氟化合物生产大量具有小粒径的颗粒的含氟聚合物的方法。含氟聚合物的制造方法包括在由式：CH 2 = CHCH 2 -O-（C = O）CHXCH 2 COO（CH 2）n CH 3表示的化合物存在下，包含至少一种氟烯烃的单体的水分散聚合（式中， X是H或SO 3 Y，其中Y是NH 4或碱金属; n是0至19的整数。）

26. 发明申请

US20120149840A1 PROCESS FOR PRODUCING AN AQUEOUS POLYMER DISPERSION 审中-公开
标题翻译：生产水性聚合物分散体的方法
公开(公告)号：US20120149840A1
公开(公告)日：2012-06-14
申请号：US13311965
申请日：2011-12-06
申请人： Kevin Müller , Ulrich Berens , Hans J. Schanz
发明人： Kevin Müller , Ulrich Berens , Hans J. Schanz
IPC分类号： C08L23/24 , C08F2/16 , C09D123/24 , C07F15/00 , C08F36/20 , C09J123/24
CPC分类号： C08F2/24 , C07F15/0046 , C08F232/08 , C08L2314/08 , C09D123/0823 , C09D145/00
摘要： Polymerizing an ethylenically unsaturdated monomer in an aqueous medium can produce an aqueous polymer dispersion. The polymerization is in the presence of a dispersant and a metal-carbene complex. The polymerization can also optionally be in the presence of a dispersant, an organic solvent with low solubility in water, or both. The aqueous polymer dispersion resulting from the process can be used to make a polymer powder.
摘要翻译：在水性介质中聚合烯属不饱和单体可以产生聚合物水分散体。聚合反应在分散剂和金属 - 卡宾络合物的存在下进行。聚合还可以任选地存在分散剂，在水中溶解度低的有机溶剂或两者。由该方法得到的聚合物水分散体可用于制备聚合物粉末。

27. 发明授权

US08013085B2 Method for the production of an aqueous polymer dispersion 失效
标题翻译：制备聚合物水分散体的方法
公开(公告)号：US08013085B2
公开(公告)日：2011-09-06
申请号：US10558743
申请日：2004-06-04
申请人： Markus Schmid , Mubarik Mahmood Chowdhry , Dieter Distler , Reinhold J. Leyrer
发明人： Markus Schmid , Mubarik Mahmood Chowdhry , Dieter Distler , Reinhold J. Leyrer
IPC分类号： C08F2/16
CPC分类号： C08F291/00 , C08F295/00
摘要： Process for preparing an aqueous polymer dispersion by polymerizing at least one ethylenically unsaturated monomer B in an aqueous medium in the presence of polymer particles A and at least one dispersant.
摘要翻译：通过在聚合物颗粒A和至少一种分散剂的存在下在水性介质中聚合至少一种烯属不饱和单体B来制备聚合物水分散体的方法。

28. 发明授权

US07973110B2 Copolymer synthesis process 有权
标题翻译：共聚物合成工艺
公开(公告)号：US07973110B2
公开(公告)日：2011-07-05
申请号：US12477565
申请日：2009-06-03
申请人： Klaus K. Lorenz , Alexander Kraus , Barbara Wimmer , Petra Wagner , Christian Scholz , Manfred Bichler
发明人： Klaus K. Lorenz , Alexander Kraus , Barbara Wimmer , Petra Wagner , Christian Scholz , Manfred Bichler
IPC分类号： C08F2/10 , C08F2/16 , C08F216/14
CPC分类号： C04B28/02 , C04B24/2647 , C04B24/2694 , C04B2103/308 , C08F216/1416 , C08F220/26 , Y10S526/915 , C04B2103/302
摘要： Preparing a non-ionic copolymer having a hydrolysable monomer residue and a polyether macromonomer residue in a semicontinuous mode in a polymerization reactor associated with a metering device, including introducing polyether macromonomer and water into the reactor, wherein hydrolysable monomer which is added thereto forms a polymerization reaction mixture; introducing hydrolysable monomer into the metering device; adding hydrolysable monomer into the reactor from the metering device; passing a free radical polymerization initiator into the reactor before and/or during the addition of the hydrolysable monomer, the hydrolysable monomer and the polyether macromonomer reacting by free radical polymerization to form the non-ionic copolymer; and, subjecting the reaction mixture to polymerization while an addition rate of the hydrolysable monomer and/or at least a component of the polymerization initiator is varied stepwise or continuously. No monomer is introduced to incorporate ionic cement binding sites into the non-ionic copolymer.
摘要翻译：在与计量装置相关联的聚合反应器中制备具有可水解单体残基和聚醚大分子单体残基的非离子共聚物，其包括将聚醚大分子单体和水引入反应器，其中加入的可水解单体形成聚合反应混合物; 将可水解单体引入计量装置; 从计量装置将可水解单体加入到反应器中; 在可水解单体加入之前和/或期间将自由基聚合引发剂通入自由基聚合引发剂，可水解单体和聚醚大分子单体通过自由基聚合反应形成非离子共聚物; 并且使反应混合物进行聚合，同时可水解单体和/或至少一种聚合引发剂组分的添加速率逐步或连续地改变。没有引入单体以将离子水泥结合位点引入非离子共聚物。

29. 发明申请

US20110136963A1 METHOD FOR SNYTHESIZING AMPHIPHILIC GRADIENT COPOLYMERS SOLUBLE IN AN ALKALINE MEDIUM 审中-公开
标题翻译：在碱性介质中可溶性水杨酸共聚物的方法
公开(公告)号：US20110136963A1
公开(公告)日：2011-06-09
申请号：US13058383
申请日：2009-08-11
申请人： Laurence Couvreur
发明人： Laurence Couvreur
IPC分类号： C08F2/38 , C08F20/06 , C08F2/16 , C08F2/06 , C08F2/44 , C08L33/02 , C08L53/00 , C08F299/04 , C08K3/22
CPC分类号： C08F2/38 , C08F293/005 , C08F2438/03 , C08L53/00 , C09D153/00 , Y02P20/582 , C08L2666/02 , C08F212/08 , C08F220/06
摘要： The present invention relates to a process for the preparation of amphiphilic gradient copolymers by Controlled Radical Polymerization in the presence of a RAFT (Reversible Addition Fragmentation Transfer) agent. The copolymers of the invention exhibit low polydispersity indices and low viscosities in solution and are readily soluble in an alkaline medium.
摘要翻译：本发明涉及通过在RAFT（可逆加成裂解转移剂）存在下通过受控自由基聚合制备两亲性梯度共聚物的方法。本发明的共聚物在溶液中表现出低的多分散指数和低粘度，并且易溶于碱性介质。

30. 发明授权

US07834079B2 Water-soluble anionic polymer dispersion and method for producing the same 有权
标题翻译：水溶性阴离子聚合物分散体及其制造方法
公开(公告)号：US07834079B2
公开(公告)日：2010-11-16
申请号：US11638541
申请日：2006-12-14
申请人： Sung Wook Han , Seung Chul Lee
发明人： Sung Wook Han , Seung Chul Lee
IPC分类号： C08F2/16 , C08L33/02 , C08L33/26
CPC分类号： C08F2/20 , C08F2/16
摘要： Disclose is a water soluble anionic polymer dispersion containing a radical copolymer created in water salt which includes anionic monomer, non-ionic monomer, ionic dispersant and radical polymerization initiator, and anionic surfactant or non-ionic surfactant. Also disclosed is a water soluble anionic polymer dispersion is characterized by containment of radical copolymer created in salt water which includes anionic monomer, non-ionic monomer, ionic dispersant, and radical polymerization initiator, and anionic surfactant, and non-ionic surfactant. Manufacturing methods for the water soluble anionic polymer dispersions are further disclosed herein.
摘要翻译： Disclose是一种水溶性阴离子聚合物分散体，其含有在水盐中产生的自由基共聚物，其包括阴离子单体，非离子单体，离子分散剂和自由基聚合引发剂，以及阴离子表面活性剂或非离子表面活性剂。还公开了一种水溶性阴离子聚合物分散体，其特征在于包含在盐水中产生的自由基共聚物，其包括阴离子单体，非离子单体，离子分散剂和自由基聚合引发剂，阴离子表面活性剂和非离子表面活性剂。水溶性阴离子聚合物分散体的制造方法在本文中进一步公开。

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