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1. 发明申请

US20190218318A1 Polymerization Process 审中-公开
公开(公告)号：US20190218318A1
公开(公告)日：2019-07-18
申请号：US16336987
申请日：2017-09-07
申请人： ExxonMobil Chemical Patents Inc.
发明人： Corrine L. Brandl , Fred D. Ehrman , James R. Lattner
IPC分类号： C08F210/16 , C08F210/02 , C08F2/34 , C08K5/01
CPC分类号： C08F210/16 , C08F2/00 , C08F2/34 , C08F4/14 , C08F4/24 , C08F4/80 , C08F210/02 , C08F2500/08 , C08F2500/12 , C08K5/01
摘要： A process including contacting one or more monomers, at least one catalyst system, and at least two condensing agents under polymerizable conditions to produce a polyolefin polymer is provided where the vapor pressure of the condensing agents is ±4 bara of the optimum vapor pressure given by the formula: optimum vapor pressure=614−716*D+2.338*P+3.603*ln(MI), where the optimum vapor pressure has units (bara), D is the polyolefin polymer density with units (g/cc), P is the polymerization condition pressure with units (barg), and MI is the polyolefin polymer melt index with units (g/10 min). The invention also relates to a process where at least three condensing agents are used.

2. 发明授权

US09771442B2 Polymerization initiating system and method to produce highly reactive olefin functional polymers 有权
公开(公告)号：US09771442B2
公开(公告)日：2017-09-26
申请号：US14710763
申请日：2015-05-13
申请人： University of Massachusetts , Infineum International Limited
发明人： Rudolf Faust , Jacob Emert
IPC分类号： C08F110/10 , C08F4/14
CPC分类号： C08F110/10 , C08F4/14 , C08F2500/02 , C08F4/54
摘要： A method for producing highly reactive olefin polymers wherein at least 50 mol % of the polymer chains have terminal double bonds, and a novel polymerization initiating system for accomplishing the same includes contacting isobutene or an isobutene-containing monomer mixture, wherein a Lewis acid catalyst is complexed with an oxygen and/or sulfur-containing Lewis base, in an apolar solvent, and wherein an initiator is employed to initiate polymerization of the isobutene or isobutene-containing monomer mixture.

3. 发明申请

US20160176994A1 DEVICE AND METHOD FOR RE-CIRCULATING RAW MATERIAL USED WHEN MANUFACTURING POLYBUTENE 有权
标题翻译：在制造聚氨酯时使用的原材料再循环的装置和方法
公开(公告)号：US20160176994A1
公开(公告)日：2016-06-23
申请号：US14908702
申请日：2014-07-29
申请人： DAELIM INDUSTRIAL CO., LTD.
发明人： Myeong Seok KIM , Min Sup PARK , Kyoung Tae MIN
IPC分类号： C08F110/08 , B01J19/24
CPC分类号： C08F110/08 , B01J8/0457 , B01J19/1862 , B01J19/24 , B01J2219/24 , C08F6/003 , C08F6/02 , C08J11/02 , C08F2/01 , C08F4/14 , C08L23/20
摘要： Disclosed are a device and a method for continuously polymerizing polybutene by removing halogen acid, which is included in a reaction raw material, by adsorbing the halogen acid using an adsorbent and then re-supplying the reaction raw material into a reactor. The device for re-circulating the raw material when manufacturing polybutene comprises a reactor, into which a catalyst and a reaction raw material (diluted with an inactive organic solvent) are supplied and polymerized to produce a reaction product; a neutralizing/washing tank for removing the catalyst from the reaction product and neutralizing the reaction product; a separation tank for separating the reaction product into organic compounds and water; a C4 distillation column for distilling an unreacted raw material and the inactive organic solvent from the organic compounds; and an impurity adsorption column for removing halogen acid from the distilled unreacted raw material and the inactive organic solvent using an adsorbent.
摘要翻译：公开了通过使用吸附剂吸附卤酸，然后将反应原料再供给到反应器中，通过除去反应原料中所含的卤素酸来连续聚合聚丁烯的装置和方法。当制备聚丁烯时，用于再循环原料的装置包括反应器，其中供应催化剂和反应原料（用惰性有机溶剂稀释）并聚合以产生反应产物; 用于从反应产物中除去催化剂并中和反应产物的中和/洗涤槽; 用于将反应产物分离成有机化合物和水的分离罐; 用于从有机化合物中蒸馏未反应的原料和无活性有机溶剂的C4蒸馏塔; 以及使用吸附剂从蒸馏的未反应原料和无活性有机溶剂中除去卤素酸的杂质吸附塔。

4. 发明授权

US09296841B2 Preparation of isobutene homo- or copolymer derivatives 有权
标题翻译：异丁烯均聚物或共聚物衍生物的制备
公开(公告)号：US09296841B2
公开(公告)日：2016-03-29
申请号：US13305283
申请日：2011-11-28
申请人： Hannah Maria König , Klaus Mühlbach , Helmut Mach , Ulrich Eichenauer
发明人： Hannah Maria König , Klaus Mühlbach , Helmut Mach , Ulrich Eichenauer
IPC分类号： C08F4/14 , C08F4/26 , C08F10/10 , C08F8/30 , C08F8/32 , C08F8/46 , C08F8/00 , C08F8/34 , C08F110/10 , C08F210/10
CPC分类号： C08F4/14 , C08F4/26 , C08F8/00 , C08F8/30 , C08F8/32 , C08F8/34 , C08F8/46 , C08F10/10 , C08F110/10 , C08F210/10 , C08F4/12 , C08F210/08
摘要： A process for preparing isobutene homo- or copolymer derivatives by (i) polymerizing isobutene or an isobutene-comprising monomer mixture in the presence of an iron halide-donor complex, an aluminum trihalide-donor complex, or an alkylaluminum halide-donor complex, (ii) reacting a resulting high-reactivity isobutene polymer with a compound which introduces a low molecular weight polar group or a substructure thereof, and (iii) in the case of reaction with a substructure, further reacting to complete the formation of the low molecular weight polar group. The homo- or copolymer derivatives include a radical of a hydrophobic polyisobutene polymer having a number-average molecular weight of 110 to 250,000 and low molecular weight polar groups including amino functions, nitro groups, hydroxyl groups, mercaptan groups, carboxylic acid or carboxylic acid derivative functions, sulfonic acid or sulfonic acid derivative functions, aldehyde functions and/or silyl groups.
摘要翻译：（i）在卤化铁 - 给体络合物，三卤化铝 - 供体络合物或烷基铝卤化物 - 供体络合物存在下聚合异丁烯或含异丁烯的单体混合物来制备异丁烯均聚物或共聚物衍生物的方法（ ii）使所得高反应性异丁烯聚合物与引入低分子量极性基团或其下结构的化合物反应，和（iii）在与亚结构反应的情况下，进一步反应以完成低分子量的形成极地组。均聚物或共聚物衍生物包括数均分子量为110至250,000的疏水聚异丁烯聚合物基团和包括氨基官能团的低分子量极性基团，硝基，羟基，硫醇基，羧酸或羧酸衍生物功能，磺酸或磺酸衍生物功能，醛官能团和/或甲硅烷基。

5. 发明申请

US20150322181A1 METHOD FOR PREPARING POLYBUTENE 有权
标题翻译：制备聚氨酯的方法
公开(公告)号：US20150322181A1
公开(公告)日：2015-11-12
申请号：US14801357
申请日：2015-07-16
申请人： DAELIM INDUSTRIAL CO., LTD.
发明人： Myeong Seok KIM , Min Sup PARK , Hyung Jae SEO , Se Hyun LEE
IPC分类号： C08F110/10 , C07C5/13
CPC分类号： C08F110/10 , C07C5/13 , C08F10/10 , C10G45/32 , C10G45/58 , C10G50/00 , C10G69/00 , C10G69/126 , C08F4/14
摘要： Disclosed is a method for preparing a highly reactive polybutene of high quality having low fluorine content and high vinylidene content at high mileage of catalyst with economy. The method for preparing a polybutene includes: performing a selective hydrogenation reaction of diolefin among C4 hydrocarbon components produced from petroleum refineries or naphtha cracking centers, which involve cracking of crude oils, and simultaneously an isomerization reaction of 1-butene to 2-butene and then isolating an isobutene feedstock through fractional distillation; and polymerizing the isobutene feedstock obtained by the fractional distillation.
摘要翻译：公开了一种经济地制备高活性聚丁烯的方法，该方法具有低的含氟量和高亚乙烯基含量，高的催化剂里程。制备聚丁烯的方法包括：在由石油炼厂或石脑油裂解中心生产的C4烃成分中进行二烯烃的选择性氢化反应，其涉及原油裂化，同时进行1-丁烯异丁烯化反应至2-丁烯，然后通过分馏分离异丁烯原料; 并使通过分馏得到的异丁烯原料聚合。

6. 发明授权

US09034998B2 Polymerization initiating system and method to produce highly reactive olefin functional polymers 有权
标题翻译：聚合引发体系和制备高反应性烯烃官能聚合物的方法
公开(公告)号：US09034998B2
公开(公告)日：2015-05-19
申请号：US13328569
申请日：2011-12-16
申请人： Rudolf Faust , Philip Dimitrov , Rajeev Kumar , Jacob Emert , Jun Hua
发明人： Rudolf Faust , Philip Dimitrov , Rajeev Kumar , Jacob Emert , Jun Hua
IPC分类号： C08F4/00 , C08F2/00 , C08F4/14 , C08F210/00 , C08F10/00 , C08F110/10
CPC分类号： C08F110/10 , C08F4/14 , C08F4/16 , C08F4/22 , C08F2500/02 , C08F2500/03 , C08F2500/04
摘要： A method for producing highly reactive olefin polymers wherein at least 50 mol. % of the polymer chains have terminal double bonds, and a novel polymerization initiating system for accomplishing same.
摘要翻译：一种生产高反应性烯烃聚合物的方法，其中至少50mol。聚合物链的％具有末端双键，以及用于实现其的新型聚合引发体系。

7. 发明申请

US20150105525A1 POLYMERIZATION INITIATING SYSTEM AND METHOD TO PRODUCE HIGHLY REACTIVE OLEFIN FUNCTIONAL POLYMERS 有权
标题翻译：聚合反应体系和生产高活性烯烃官能聚合物的方法
公开(公告)号：US20150105525A1
公开(公告)日：2015-04-16
申请号：US14052490
申请日：2013-10-11
申请人： University of Massachusetts , Infineum International Limited
发明人： Rudolf Faust , Rajeev Kumar , Jack Emert
IPC分类号： C08F110/10
CPC分类号： C08F110/10 , C08F4/52 , C08F4/70 , C08F4/80 , C08F4/26 , C08F4/14 , C08F4/12 , C08F4/16 , C08F4/22 , C08F2500/02 , C08F2500/03
摘要： A method for producing highly reactive olefin polymers wherein at least 50 mol. % of the polymer chains have terminal double bonds, and a novel polymerization initiating system for accomplishing same.
摘要翻译：一种生产高反应性烯烃聚合物的方法，其中至少50mol。聚合物链的％具有末端双键，以及用于实现其的新型聚合引发体系。

8. 发明授权

US08829105B2 Low molecular weight polystyrene resin and methods of making and using the same 有权
标题翻译：低分子量聚苯乙烯树脂及其制备和使用方法
公开(公告)号：US08829105B2
公开(公告)日：2014-09-09
申请号：US13740322
申请日：2013-01-14
申请人： Eastman Chemical Company
发明人： Wei Min Cheng , Puthenkovilakom Rajesh Raja , George Joseph Kutsek , John B. Penn
IPC分类号： C08L53/00 , C09B67/00 , C08L31/04 , B01F17/00 , C08K5/00 , C08F12/08 , C09J125/06 , C08F8/04 , C08F112/08
CPC分类号： C09J125/06 , B60C1/00 , C08F8/04 , C08F12/08 , C08F112/08 , C08L25/04 , C08L53/02 , C09J125/04 , C09J153/02 , C08F2/06 , C08F4/14 , C08F4/005
摘要： A low z-average molecular weight, high softening point polystyrene resin having a narrow molecular weight distribution, as well as methods of making and using the same, are provided. The use of an inert solvent and/or the order of addition of reactants during polymerization may contribute to the unique properties of the final homopolymeric resin. The polystyrene resin can be partially or fully hydrogenated and may have particular use as a tackifying agent in a variety of hot melt adhesive and rubber compositions.
摘要翻译：提供了低Z平均分子量，具有窄分子量分布的高软化点聚苯乙烯树脂，以及制备和使用它们的方法。使用惰性溶剂和/或在聚合过程中加入反应物的顺序有助于最终均聚树脂的独特性能。聚苯乙烯树脂可以部分或完全氢化，并且可以在各种热熔粘合剂和橡胶组合物中作为增粘剂具有特别的用途。

9. 发明授权

US08492491B2 Methods for producing telechelic polyolefins from terpene initiators 有权
公开(公告)号：US08492491B2
公开(公告)日：2013-07-23
申请号：US12813411
申请日：2010-06-10
申请人： Casey D. Stokes , Young A. Chang
发明人： Casey D. Stokes , Young A. Chang
IPC分类号： C08F4/52 , C08F4/609
CPC分类号： C08F4/00 , C08F2/38 , C08F4/14 , C08F4/16 , C08F4/52 , C08F12/08 , C08F110/10
摘要： Provided herein are methods for the preparation of telechelic polyolefins via polymerization reaction with a terpene initiator.

10. 发明申请

US20130184425A1 LOW MOLECULAR WEIGHT POLYSTYRENE RESIN AND METHODS OF MAKING AND USING THE SAME 有权
公开(公告)号：US20130184425A1
公开(公告)日：2013-07-18
申请号：US13740320
申请日：2013-01-14
申请人： Eastman Chemical Company
发明人： Wei Min Cheng , Puthenkovilakom Rajesh Raja , George Joseph Kutsek , John B. Penn
IPC分类号： C08F112/08 , C09J125/06
CPC分类号： C09J125/06 , B60C1/00 , C08F8/04 , C08F12/08 , C08F112/08 , C08L25/04 , C08L53/02 , C09J125/04 , C09J153/02 , C08F2/06 , C08F4/14 , C08F4/005
摘要： A low z-average molecular weight, high softening point polystyrene resin having a narrow molecular weight distribution, as well as methods of making and using the same, are provided. The use of an inert solvent and/or the order of addition of reactants during polymerization may contribute to the unique properties of the final homopolymeric resin. The polystyrene resin can be partially or fully hydrogenated and may have particular use as a tackifying agent in a variety of hot melt adhesive and rubber compositions.

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