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41. 发明授权

US08529787B2 Colloidal silica containing silica secondary particles having bent structure and/or branched structure, and method for producing same 有权
标题翻译：含有具有弯曲结构和/或支化结构的二氧化硅二次粒子的胶体二氧化硅及其制造方法
公开(公告)号：US08529787B2
公开(公告)日：2013-09-10
申请号：US12998096
申请日：2009-09-01
申请人： Kazuaki Higuchi , Hideki Otsuki
发明人： Kazuaki Higuchi , Hideki Otsuki
IPC分类号： C09K13/00
CPC分类号： C09K3/1409 , C01B33/14 , C01B33/18 , C01B2202/02 , C01B2202/36
摘要： This invention provides a dense, high-purity colloidal silica containing silica secondary particles having a branched and/or bent structure, and a production method thereof. Specifically, this invention provides a method for producing a colloidal silica, comprising the steps of 1) preparing a mother liquid containing an alkali catalyst and water, and having a pH of 9 to 12; and 2) adding a hydrolysis liquid obtained by hydrolysis of an alkyl silicate to the mother liquid, wherein the step of adding the hydrolysis liquid to the mother liquid sequentially comprises A) step 1 of adding the hydrolysis liquid until the pH of the resulting liquid mixture becomes less than 7; B) step 2 of adding an aqueous alkali solution until the pH of the liquid mixture becomes 7 or more; and C) step 3 of adding the hydrolysis liquid while maintaining the pH of the liquid mixture at 7 or more, and a colloidal silica containing silica secondary particles having a branched and/or bent structure, obtained by this method.
摘要翻译：本发明提供一种含有分支和/或弯曲结构的二氧化硅二次颗粒的致密的高纯度胶体二氧化硅及其制备方法。具体而言，本发明提供一种胶体二氧化硅的制造方法，其特征在于，包括以下步骤：1）制备含有碱催化剂和水的母液，pH为9〜12; 和2）将通过水解硅酸烷基酯获得的水解液加入到母液中，其中依次将水解液加到母液中的步骤包括：A）加入水解液直到所得液体混合物的pH 变得小于7; B）添加碱性水溶液直至液体混合物的pH变为7以上为止的步骤2; 和C）在将液体混合物的pH保持在7以上的同时添加水解液的步骤3和通过该方法获得的含有分支和/或弯曲结构的二氧化硅二次粒子的胶体二氧化硅。

42. 发明申请

US20130202519A1 SEPARATION METHOD 审中-公开
标题翻译：分离方法
公开(公告)号：US20130202519A1
公开(公告)日：2013-08-08
申请号：US13640150
申请日：2011-04-07
申请人： Christopher Howard , Neal Skipper , Milo Shaffer
发明人： Christopher Howard , Neal Skipper , Milo Shaffer
IPC分类号： C01B31/02 , H01B1/04
CPC分类号： H01B1/04 , B82Y30/00 , B82Y40/00 , C01B32/17 , C01B32/172 , C01B32/174 , C01B2202/02 , Y10S977/75 , Y10S977/845
摘要： A method for dispersing carbon nanotubes, wherein the nanotubes are contacted with an electronic liquid wherein the ratio to metal atoms in the electronic liquid to carbon atoms in the carbon nanotubes is controlled and a solution of carbon nanotubes obtainable by such a method is described.
摘要翻译：一种用于分散碳纳米管的方法，其中纳米管与电子液体接触，其中电子液体中的金属原子与碳纳米管中的碳原子的比率被控制，并且通过这种方法获得的碳纳米管溶液被描述。

43. 发明授权

US08496904B2 Single-walled carbon nanotube catalysts and method for preparing same 有权
标题翻译：单壁碳纳米管催化剂及其制备方法
公开(公告)号：US08496904B2
公开(公告)日：2013-07-30
申请号：US11602136
申请日：2006-11-20
申请人： Jun Ma , David Moy
发明人： Jun Ma , David Moy
IPC分类号： D01F9/12 , C01B13/14
CPC分类号： D01F9/127 , B01J21/005 , B01J23/002 , B01J23/005 , B01J23/78 , B01J37/0236 , B01J37/031 , B01J37/08 , B01J37/18 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , B01J2523/22 , B01J2523/842 , B01J2523/845 , B01J2523/41 , B01J2523/31
摘要： An activated catalyst capable of selectively growing single-walled carbon nanotubes when reacted with carbonaceous gas is provided. The activated catalyst is formed by reducing a catalyst that comprises a complex oxide. The complex oxide may be of formula Ax-wFwBy-vGvOz wherein x/y≦2; z/y≦4; 0≦w≦0.3x; 0≦v≦0.3y; A is a Group VIII element; F is an element that is different from A but has, in said composition, the same valence state as A; B is an element different from A and F, and is an element whose simple oxide, in which B is at the same valence state as in the complex oxide, is not reducible in the presence of hydrogen gas at a temperature less than about 900° C.; G is an element different from A, B and F, and is an element whose simple oxide, in which G is at the same valence state as in the complex oxide, is not reducible in the presence of hydrogen gas at a temperature less than about 900° C.; and O is oxygen. The complex oxide is reduced at a temperature less that 950° C. Methods of making, uses for and carbon fibril-containing product made with these activated catalysts are also provided.
摘要翻译：提供能够与碳质气体反应时能够选择性地生长单壁碳纳米管的活化催化剂。通过还原包含复合氧化物的催化剂形成活化的催化剂。复合氧化物可以具有式Ax-wFwBy-vGvOz，其中x / y @ 2; z / y @ 4; 0 @ w @ 0.3x; 0 @ v @ 0.3y; A是VIII族元素; F是与A不同的元素，在所述组合物中具有与A相同的价态; B是与A和F不同的元素，并且是其中B与复合氧化物处于相同价态的简单氧化物在氢气存在下在小于约900°的温度下不可还原的元素 C。; G是不同于A，B和F的元素，并且是其中G与复合氧化物处于相同价态的简单氧化物的元素在氢气存在下在小于约 900°C。而O是氧。复合氧化物在低于950℃的温度下还原。还提供了用这些活化的催化剂制备，用于含有原纤维的产物的方法。

44. 发明授权

US08465647B2 Isolation of single-walled carbon nanotubes from double and multi-walled carbon nanotubes 有权
标题翻译：从双层和多壁碳纳米管分离单壁碳纳米管
公开(公告)号：US08465647B2
公开(公告)日：2013-06-18
申请号：US12636426
申请日：2009-12-11
申请人： Ageeth A. Bol , George S. Tulevski
发明人： Ageeth A. Bol , George S. Tulevski
IPC分类号： B01D11/00 , B01D17/038 , C01B31/02
CPC分类号： B01D21/262 , B01D17/0217 , B82Y30/00 , B82Y40/00 , C01B32/17 , C01B32/172 , C01B2202/02 , Y10S977/845
摘要： A method and system are disclosed for separating single-walled carbon nanotubes from double and multi-walled carbon nanotubes by using the difference in the buoyant density of Single-Walled versus Multi-Walled carbon nanotubes. In one embodiment, the method comprises providing a vessel with first and second solutions. The first solution comprises a quantity of carbon nanotubes, including single-walled carbon nanotubes and double and multi-walled carbon nanotubes. The single walled nanotubes have a first density, the double and multi-walled nanotubes having a second density. The second solution in the vessel has a third density between said first and second densities. The vessel is centrifuged to form first and second layers in the vessel, with the second solution between said first and second layers. The single-walled carbon nanotubes are predominantly in the first layer, and the second and multi-walled carbon nanotubes are predominantly in the second layer.
摘要翻译：公开了通过使用单壁碳纳米管与多壁碳纳米管的浮力密度的差异来从双层和多壁碳纳米管分离单壁碳纳米管的方法和系统。在一个实施例中，该方法包括向船舶提供第一和第二解决方案。第一种解决方案包括一定量的碳纳米管，包括单壁碳纳米管和双层和多壁碳纳米管。单壁纳米管具有第一密度，双壁和多壁纳米管具有第二密度。容器中的第二溶液在所述第一和第二密度之间具有第三密度。将容器离心以在容器中形成第一和第二层，第二溶液在所述第一和第二层之间。单壁碳纳米管主要位于第一层中，第二层和多壁碳纳米管主要位于第二层。

45. 发明申请

US20130137822A1 MODIFIED CARBON NANOTUBES AND THEIR COMPATIBILITY 有权
标题翻译：改性碳纳米管及其相容性
公开(公告)号：US20130137822A1
公开(公告)日：2013-05-30
申请号：US13702106
申请日：2011-06-10
申请人： Jingwen Guan , Robin Fraser , Benoit Simard
发明人： Jingwen Guan , Robin Fraser , Benoit Simard
IPC分类号： C08F226/02
CPC分类号： C08F226/02 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , C01B2202/06 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C09C1/44 , Y10S977/746
摘要： Modified carbon nanotubes are provided having carbon nanotube core covalently bound through C—C bonds to a polymer shell surrounding the carbon nanotube core. The polymer shell is a polymer having functional groups pointing outwardly from the shell. The functional groups are compatible with or able to covalently connect to another polymer. Such modified carbon nanotubes are more readily dispersed in a homogeneous manner in another polymer and may be used as a reinforcing filler in a polymer matrix. The modified carbon nanotubes with a core-shell structure in which the core has a substantially unidirectional orientation within the shell are produced by reacting neutral carbon nanotubes with 4-vinylaniline through a diazonium reaction in presence of one or more types of multifunctional monomers carrying a vinyl moiety and one or more functional groups for compatibilization with or connection to another polymer. The reaction is conducted at an elevated temperature without isolation of intermediates and without addition of any extra initiator or catalyst to form a polymer shell in situ around the carbon nanotube. The polymer shell is covalently bound to CNT sidewall through C—C bonds and has functional groups outwardly pointing from the shell for compatibilization with or connection to another polymer.
摘要翻译：提供了具有通过C-C键共价键合到碳纳米管芯周围的聚合物壳的碳纳米管芯的改性碳纳米管。聚合物壳是具有从壳向外指向的官能团的聚合物。官能团与另一种聚合物相容或能共价连接。这种改性碳纳米管更容易以均匀的方式分散在另一种聚合物中，并且可以用作聚合物基质中的增强填料。具有核 - 壳结构的改性碳纳米管通过在一种或多种携带乙烯基的多官能单体的存在下，通过重氮化反应使中性碳纳米管与4-乙烯基苯胺反应，从而制备芯在壳内具有基本上单向取向部分和一个或多个与另一种聚合物相容或连接的官能团。反应在升高的温度下进行，而不分离中间体，并且不加入任何额外的引发剂或催化剂以在碳纳米管周围原位形成聚合物壳。聚合物壳通过C-C键共价结合到CNT侧壁上，并且具有从壳体向外指向的官能团，用于与另一种聚合物相容或连接。

46. 发明授权

US08420717B2 Polyol functionalized water soluble carbon nanostructures 失效
标题翻译：多元醇官能化水溶性碳纳米结构
公开(公告)号：US08420717B2
公开(公告)日：2013-04-16
申请号：US12670068
申请日：2008-07-23
申请人： Valery N. Khabashesku , Oleksandr Kuznetsov , Rui Lobo
发明人： Valery N. Khabashesku , Oleksandr Kuznetsov , Rui Lobo
IPC分类号： C08G59/18 , C08L63/00 , C08K9/04 , C08K7/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/152 , C01B32/174 , C01B32/18 , C01B32/28 , C01B2202/02 , C01B2202/04 , C01B2202/06
摘要： A method of making a water soluble carbon nanostructure includes treating a fluorinated carbon nanostructure material with a polyol in the presence of a base. A water soluble carbon nanostructure comprises a fluorinated carbon nanostructure covalently bound to a polyol. Exemplary uses of water soluble carbon nanostructures include use in polymer composites, biosensors and drug delivery vehicles.
摘要翻译：制备水溶性碳纳米结构的方法包括在碱的存在下用多元醇处理氟化碳纳米结构材料。水溶性碳纳米结构包括与多元醇共价结合的氟化碳纳米结构。水溶性碳纳米结构的示例性用途包括用于聚合物复合材料，生物传感器和药物递送载体。

47. 发明授权

US08343581B2 Synthesis of pure nanotubes from nanotubes 有权
标题翻译：从纳米管合成纯纳米管
公开(公告)号：US08343581B2
公开(公告)日：2013-01-01
申请号：US11742032
申请日：2007-04-30
申请人： Peter J. Burke , Zhen Yu
发明人： Peter J. Burke , Zhen Yu
IPC分类号： C23C16/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/16 , C01B32/168 , C01B2202/02 , C01B2202/34 , C01B2202/36
摘要： An improved method of synthesizing nanotubes that avoids the slow process and the impurities or defects that are usually encountered with regard to as-grown carbon nanotubes. In a preferred embodiment, nanotubes are synthesized from nanotubes providing a novel catalyst-free growth method for direct growth of single- or multi-walled, metallic or semiconducting nanotubes.
摘要翻译：一种合成纳米管的改进方法，其避免了慢生成方法以及通常在生长的碳纳米管方面遇到的杂质或缺陷。在优选的实施方案中，从纳米管合成纳米管，提供用于直接生长单层或多壁金属或半导体纳米管的新型无催化剂生长方法。

48. 发明授权

US08333900B1 Selective etching of single walled carbon nanotubes 失效
标题翻译：单壁碳纳米管的选择性蚀刻
公开(公告)号：US08333900B1
公开(公告)日：2012-12-18
申请号：US12493459
申请日：2009-06-29
申请人： Salah Boussaad , Frank M. Pellicone , Joseph Menezes
发明人： Salah Boussaad , Frank M. Pellicone , Joseph Menezes
IPC分类号： C23F3/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/172 , C01B2202/02
摘要： Described is a method for the selective etching of single walled carbon nanotubes with CO2 where nanotubes of small diameters are removed.
摘要翻译：描述了用CO 2选择性蚀刻单壁碳纳米管的方法，其中除去小直径的纳米管。

49. 发明申请

US20120308471A1 SELECTIVE ETCHING OF SINGLE WALLED CARBON NANOTUBES 失效
标题翻译：单壁碳纳米管的选择性蚀刻
公开(公告)号：US20120308471A1
公开(公告)日：2012-12-06
申请号：US12493459
申请日：2009-06-29
申请人： Salah Boussaad , Frank M. Pellicone , Joseph Menezes
发明人： Salah Boussaad , Frank M. Pellicone , Joseph Menezes
IPC分类号： D01F9/12 , B82Y30/00 , B82Y40/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/172 , C01B2202/02
摘要： Described is a method for the selective etching of single walled carbon nanotubes with CO2 where nanotubes of small diameters are removed.
摘要翻译：描述了用CO 2选择性蚀刻单壁碳纳米管的方法，其中除去小直径的纳米管。

50. 发明申请

US20120295091A1 PROCESSES FOR FABRICATING FILMS OF GRAPHENE, CARBON NANOTUBES, AND OTHER CARBON NANOSTRUCTURES ON VARIOUS TYPES OF SUBSTRATES 审中-公开
标题翻译：在不同类型的基底上制作石墨，碳纳米管和其他碳纳米管的薄膜的方法
公开(公告)号：US20120295091A1
公开(公告)日：2012-11-22
申请号：US13508780
申请日：2010-11-09
申请人： Matteo Pasquali , Robert H. Hauge , Budhadipta Dan , Natnael Behabtu , Cary Pint
发明人： Matteo Pasquali , Robert H. Hauge , Budhadipta Dan , Natnael Behabtu , Cary Pint
IPC分类号： C01B31/00 , B32B9/00 , B32B37/24 , C01B31/02 , D01F9/12 , B82Y40/00 , B82Y30/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/15 , C01B32/168 , C01B32/174 , C01B32/194 , C01B2202/02 , C01B2202/04 , C01B2202/06 , Y10T428/30
摘要： Methods for producing carbon films are disclosed herein. The methods include treating a carbon nanostructure with one or more dispersing agents, filtering the solution through a filter membrane to form the carbon film, releasing the carbon film from the filter membrane, and transferring the film onto a desired substrate without the use of sonication. Carbon films formed by said methods are also disclosed herein.
摘要翻译：本文公开了生产碳膜的方法。所述方法包括用一种或多种分散剂处理碳纳米结构，通过过滤膜过滤溶液以形成碳膜，从过滤膜释放碳膜，并将膜转移到所需的基材上而不使用超声处理。通过所述方法形成的碳膜也在本文中公开。

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