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51. 发明授权

US09908093B2 Process for converting a carbonaceous material to methane, methanol and/or dimethyl ether using microchannel process technology 有权
公开(公告)号：US09908093B2
公开(公告)日：2018-03-06
申请号：US12420942
申请日：2009-04-09
申请人： Wayne W. Simmons , Robert Dwayne Litt , Terry Mazanec , Anna Lee Tonkovich
发明人： Wayne W. Simmons , Robert Dwayne Litt , Terry Mazanec , Anna Lee Tonkovich
IPC分类号： B01J19/00 , C01B3/22 , C01B3/32 , C01B3/50 , C01B3/52 , C01B3/56 , C07C1/04 , C07C1/20 , C07C2/84 , C07C9/06 , C07C11/04 , C07C29/152 , C10J3/00
CPC分类号： B01J19/0093 , B01J2219/00835 , B01J2219/00846 , B01J2219/0086 , B01J2219/00873 , B01J2219/00918 , B01J2219/00921 , B01J2219/00984 , C01B3/22 , C01B3/32 , C01B3/501 , C01B3/52 , C01B3/56 , C01B2203/0205 , C01B2203/0266 , C01B2203/0405 , C01B2203/0415 , C01B2203/042 , C01B2203/043 , C01B2203/0465 , C01B2203/0475 , C01B2203/0485 , C01B2203/06 , C01B2203/061 , C01B2203/062 , C01B2203/0838 , C01B2203/0883 , C01B2203/1217 , C01B2203/84 , C07C1/04 , C07C1/20 , C07C2/84 , C07C9/06 , C07C11/04 , C07C29/152 , C07C2529/85 , C10J3/00 , C10J2300/1662 , C10J2300/1665 , Y02E50/18 , Y02E50/32 , Y02E50/346 , Y02P30/42 , C07C9/04 , C07C11/02 , C07C31/04
摘要： This invention relates to a process for converting a carbonaceous material to a desired product comprising methane, methanol and/or dimethyl ether, the process comprising: gasifying the carbonaceous material at a temperature in excess of about 700° C. to form synthesis gas; and flowing the synthesis gas through two or more reaction zones in a microchannel reactor to convert the synthesis gas to the desired product.

52. 发明授权

US09695368B2 Process and apparatus employing microchannel process technology 有权
公开(公告)号：US09695368B2
公开(公告)日：2017-07-04
申请号：US15041119
申请日：2016-02-11
申请人： Velocys, Inc.
发明人： Anna Lee Tonkovich , Ravi Arora , John Brophy , Francis P. Daly , Soumitra Deshmukh , Maddalena Fanelli , Kai Tod Paul Jarosch , Timothy J. LaPlante , Richard Q. Long , Terry Mazanec , Daniel Francis Ryan , Laura J. Silva , Wayne W. Simmons , Bruce Stangeland , Yong Wang , Thomas Yuschak , Steven T. Perry , Jeffrey Dale Marco , Michael Alan Marchiando , Robert Lewis Litt
IPC分类号： C10G47/00 , C10G45/02 , C10G47/02 , C10G47/14 , B01J19/00 , B01J23/42 , B01J23/75 , B01J23/96 , B01J35/02 , C10G2/00 , B01J21/12
CPC分类号： C10G47/14 , B01J19/0093 , B01J21/12 , B01J23/42 , B01J23/75 , B01J23/96 , B01J35/023 , B01J2219/00783 , B01J2219/00788 , B01J2219/00835 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00984 , C10G2/32 , C10G45/02 , C10G47/00 , C10G47/02 , C10G2300/202 , C10G2300/4018 , Y02P20/582
摘要： This invention relates to a process for conducting a hydrocracking or a hydrotreating process in a microchannel reactor. This invention also relates to a process and apparatus for flowing a vapor and liquid into a plurality of microchannels in a microchannel processing unit.

53. 发明授权

US09527057B2 Laminated, leak-resistant chemical processors; methods of making, and methods of operating 有权
标题翻译：层压，防漏化学处理器; 制作方法和操作方法
公开(公告)号：US09527057B2
公开(公告)日：2016-12-27
申请号：US13276311
申请日：2011-10-18
申请人： Anna Lee Tonkovich , Thomas Yuschak , Paul W. Neagle , Jennifer L. Marco , Jeffrey D. Marco , Michael A. Marchiando , Lane W. Keyes , Soumitra Deshmukh , Robert J. Luzenski
发明人： Anna Lee Tonkovich , Thomas Yuschak , Paul W. Neagle , Jennifer L. Marco , Jeffrey D. Marco , Michael A. Marchiando , Lane W. Keyes , Soumitra Deshmukh , Robert J. Luzenski
IPC分类号： B32B37/00 , B32B37/02 , B01J19/00 , B23K1/00 , B23K26/00 , B23K26/20 , B23K26/21 , B23K26/24
CPC分类号： B01J19/0093 , B01J2219/00783 , B01J2219/00806 , B01J2219/00808 , B01J2219/00817 , B01J2219/00822 , B01J2219/00835 , B01J2219/00898 , B01J2219/00988 , B01J2219/0099 , B23K1/00 , B23K1/0012 , B23K26/24 , B23K2101/14 , B23K2103/02 , C10G2/341 , Y10T137/0396 , Y10T156/10 , Y10T428/24562 , Y10T428/24802
摘要： The invention provides methods of making laminated devices (especially microchannel devices) in which plates are assembled and welded together. Unlike conventional microchannel devices, the inventive laminated devices can be made without brazing or diffusion bonding; thus providing significant advantages for manufacturing. Features such as expansion joints and external welded supports are also described. Laminated devices and methods of conducting unit operations in laminated devices are also described.
摘要翻译：本发明提供制造其中板被组装和焊接在一起的层压装置（特别是微通道装置）的方法。不同于传统的微通道器件，本发明的层压器件可以不用钎焊或扩散接合而制成; 从而为制造提供了显着的优势。还描述了诸如膨胀节和外部焊接支撑件的特征。还描述了在层压装置中进行单元操作的层叠装置和方法。

54. 发明授权

US09453165B2 Fischer-tropsch synthesis using microchannel technology and novel catalyst and microchannel reactor 有权
标题翻译：使用微通道技术的费 - 托合成和新型催化剂和微通道反应器
公开(公告)号：US09453165B2
公开(公告)日：2016-09-27
申请号：US14700197
申请日：2015-04-30
申请人： Velocys, Inc.
发明人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
IPC分类号： C10G2/00 , B01J23/75 , B01J19/00 , B01J37/03 , B01J38/48 , B01J35/04 , C10G45/58 , C10G47/00 , B01J23/94 , B01J37/02 , B01J23/755 , B01J23/83 , B01J23/889 , B01J23/89 , B01J35/00 , B01J35/10 , C10G21/00 , C10L1/08 , C10M105/04 , B01J38/58
CPC分类号： C10G2/332 , B01J19/0093 , B01J23/75 , B01J23/755 , B01J23/83 , B01J23/8896 , B01J23/8913 , B01J23/892 , B01J23/894 , B01J23/8986 , B01J23/94 , B01J35/0066 , B01J35/04 , B01J35/1019 , B01J35/1038 , B01J37/0201 , B01J37/0205 , B01J37/038 , B01J38/48 , B01J38/58 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00831 , B01J2219/00835 , B01J2219/00855 , B01J2219/0086 , B01J2219/00873 , C10G2/331 , C10G2/334 , C10G2/34 , C10G2/341 , C10G21/00 , C10G45/58 , C10G47/00 , C10G2300/1022 , C10G2400/04 , C10G2400/10 , C10L1/08 , C10L2200/0492 , C10L2270/026 , C10L2290/42 , C10L2290/544 , C10M105/04 , Y02P20/582
摘要： A process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms comprises: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. A supported catalyst comprises Co, and a microchannel reactor comprises at least one process microchannel and at least one adjacent heat exchange zone.
摘要翻译：将包含H 2和CO的反应物组合物转化为包含至少一种具有至少约5个碳原子的脂族烃的产物的方法包括：使反应物组合物流过与费 - 托催化剂接触的微通道反应器，以将反应物组合物所述微通道反应器包括含有所述催化剂的多个工艺微通道; 将热量从工艺微通道传递到热交换器; 并从微通道反应器中除去产物; 该方法每小时产生至少约0.5克具有至少约5个碳原子的每克催化剂的脂族烃; 产品中甲烷的选择性小于约25％。载体催化剂包括Co，微通道反应器包括至少一个工艺微通道和至少一个相邻的热交换区域。

55. 发明授权

US09108904B2 Process for converting a hydrocarbon to an oxygenate or a nitrile 有权
标题翻译：将烃转化为含氧化合物或腈的方法
公开(公告)号：US09108904B2
公开(公告)日：2015-08-18
申请号：US11836811
申请日：2007-08-10
申请人： John H. Brophy , Frederick A. Pesa , Anna Lee Tonkovich , Jeffrey S. McDaniel , Kai Tod Paul Jarosch
发明人： John H. Brophy , Frederick A. Pesa , Anna Lee Tonkovich , Jeffrey S. McDaniel , Kai Tod Paul Jarosch
IPC分类号： B01J19/00 , C07C253/26 , C07B41/00 , C07B43/08 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C51/25 , C07C51/265 , C07C67/05 , C07C253/24
CPC分类号： C07C253/26 , B01J19/0093 , B01J2219/00783 , B01J2219/00804 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , C07B41/00 , C07B43/08 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C51/252 , C07C51/265 , C07C67/05 , C07C253/24 , C07C47/22 , C07C57/04 , C07C63/16 , C07C69/01 , C07C255/08 , C07C69/15 , C07C69/155
摘要： This invention relates to a process for converting a hydrocarbon reactant to a product comprising an oxygenate or a nitrile, the process comprising: (A) flowing a reactant composition comprising the hydrocarbon reactant, and oxygen or a source of oxygen, and optionally ammonia, through a microchannel reactor in contact with a catalyst to convert the hydrocarbon reactant to the product, the hydrocarbon reactant undergoing an exothermic reaction in the microchannel reactor; (B) transferring heat from the microchannel reactor to a heat exchanger during step (A); and (C) quenching the product from step (A).
摘要翻译：本发明涉及一种将烃反应物转化为含有氧化合物或腈的产物的方法，该方法包括：（A）使包含烃反应物的反应物组合物和氧气或氧源和任选的氨通过与催化剂接触以将烃反应物转化成产物的微通道反应器，在微通道反应器中经历放热反应的烃反应物; （B）在步骤（A）期间将热量从微通道反应器传递到热交换器; 和（C）淬灭步骤（A）的产物。

56. 发明授权

US08802039B2 Microchannel technology having structures with reduced material and enhanced volumetric productivity 有权
标题翻译：微通道技术具有减少材料和增强体积生产率的结构
公开(公告)号：US08802039B2
公开(公告)日：2014-08-12
申请号：US12642766
申请日：2009-12-18
申请人： Paul W. Neagle , Anna Lee Tonkovich , Soumitra Deshmukh , Ravi Arora
发明人： Paul W. Neagle , Anna Lee Tonkovich , Soumitra Deshmukh , Ravi Arora
IPC分类号： B01J8/00 , B01J19/00
CPC分类号： B01J19/0093 , B01F5/061 , B01F13/0059 , B01F2005/0636 , B01J2219/00783 , B01J2219/00786 , B01J2219/00822 , B01J2219/00824 , B01J2219/00831 , B01J2219/00833 , B01J2219/00835 , B01J2219/00855 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00997 , C01B3/384 , C01B2203/0233 , C01B2203/0283 , C01B2203/1064 , F28F7/02 , F28F2260/02
摘要： Novel designs for microchannel apparatus are described in which microchannels are shaped to reduce the amount of material needed to build an apparatus. In these designs, some microchannels are shaped, in cross-section, to provide relatively more structural material in areas of greatest stress, while leaving greater area for unit operations in areas of the apparatus that are subjected to relatively less stress.
摘要翻译：描述了用于微通道装置的新颖设计，其中微通道成形为减少构建装置所需的材料的量。在这些设计中，一些微通道成形为横截面，以在应力最大的区域提供相对更多的结构材料，同时在经受相对较小应力的设备的区域中为单元操作留下更大的面积。

57. 发明申请

US20140109976A1 Multi-Stream Multi-Channel Process and Apparatus 有权
标题翻译：多流多通道过程和装置
公开(公告)号：US20140109976A1
公开(公告)日：2014-04-24
申请号：US14145623
申请日：2013-12-31
申请人： Velocys, Inc.
发明人： James A. Mathias , G. Bradley Chadwell , Dongming Qui , Anna Lee Y. Tonkovich , Steven T. Perry , Matthew B. Schmidt , Sean P. Fitzgerald , David J. Hesse , Thomas D. Yuschak , Bin Yang
IPC分类号： F16L41/02
CPC分类号： F16L41/02 , B01J19/0093 , B01J35/04 , B01J2219/00869 , B01J2219/00891 , C01B3/384 , C01B2203/0233 , C01B2203/0811 , C01B2203/0822 , F28D7/0066 , F28D9/0093 , F28F3/12 , F28F7/02 , F28F2260/02 , Y02P20/128 , Y02P20/52 , Y10T137/0318 , Y10T137/6579 , Y10T137/87153 , Y10T137/87249
摘要： Provided is a process and apparatus for exchanging heat energy between three or more streams in a millichannel apparatus, which millichannel apparatus may comprise a heat exchanger which may be integrated with a millichannel reactor to form an integrated millichannel processing unit. The combining of a plurality of integrated millichannel apparatus to provide the benefits of large-scale operation is enabled. In particular, the millichannel heat exchanger enables flexible heat transfer between multiple streams and total heat transfer rates of about 1 Watt or more per core unit volume expressed as W/cc.
摘要翻译：提供了一种用于在毫通道装置中在三个或更多个流之间交换热能的方法和装置，该通道装置可以包括热交换器，其可与毫通反应器集成以形成集成的毫通道处理单元。能够组合多个集成的毫通道装置以提供大规模操作的优点。特别地，毫通道热交换器使得能够在多个流之间实现柔性热传递，并且以W / cc表示的每单位体积的约1瓦或更高的总传热速率。

58. 发明申请

US20140045954A1 FISCHER-TROPSCH PROCESS 有权
标题翻译： FISCHER-TROPSCH过程
公开(公告)号：US20140045954A1
公开(公告)日：2014-02-13
申请号：US13802921
申请日：2013-03-14
申请人： VELOCYS, INC.
发明人： Stephen Claude LeViness , Francis Daly , Laura Richard , Sreekala Rugmini
IPC分类号： C07C1/04
CPC分类号： C07C1/043 , B01J8/00 , B01J19/0093 , B01J21/08 , B01J23/26 , B01J23/34 , B01J23/8913 , B01J23/8986 , B01J23/8993 , B01J35/0046 , B01J35/0053 , B01J35/006 , B01J35/0066 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J37/0203 , B01J37/0205 , B01J37/0207 , B01J37/0213 , B01J37/08 , B01J37/088 , B01J37/16 , B01J37/18 , B01J2208/00796 , B01J2219/00781 , B01J2219/00835 , B01J2219/00873 , C10G2/33 , C10G2/333 , C10G2/34
摘要： The disclosed invention relates to a process for conducting a Fischer-Tropsch reaction, comprising flowing a reactant mixture comprising fresh synthesis gas and tail gas in a microchannel reactor in contact with a catalyst to form at least one hydrocarbon product, the catalyst being derived from a catalyst precursor comprising cobalt and a surface modified catalyst support.
摘要翻译：所公开的发明涉及进行费 - 托反应的方法，包括使包含新鲜合成气和尾气的反应物混合物在与催化剂接触的微通道反应器中流动以形成至少一种烃产物，所述催化剂衍生自包含钴和表面改性的催化剂载体的催化剂前体。

59. 发明授权

US08497308B2 Integrated microchannel synthesis and separation 有权
标题翻译：集成微通道的合成和分离
公开(公告)号：US08497308B2
公开(公告)日：2013-07-30
申请号：US12439872
申请日：2007-09-05
申请人： Anna Lee Y. Tonkovich , Robert D. Litt , Timothy M. Werner , Bin Yang
发明人： Anna Lee Y. Tonkovich , Robert D. Litt , Timothy M. Werner , Bin Yang
IPC分类号： C07C27/00
CPC分类号： B01J19/0093 , B01J19/1831 , B01J2219/00783 , B01J2219/00835 , B01J2219/00873 , B01J2219/00984 , C07C29/152 , C10G2/341 , C07C31/04
摘要： A process for carrying out at least two unit operations in series, the process comprising the step of: (a) directing a feed stream into an integrated assembly which comprises a first microchannel unit operation upon at least one chemical of the feed stream to generate a distributed output stream that exits the first microchannel unit operation in a first set of discrete microchannels isolating flow through the discrete microchannels; and (b) directing the distributed output stream of the first microchannel unit operation into a second microchannel unit operation as a distributed input stream, to continue isolating flow between the first set of discrete microchannels, and conducting at least one operation upon at least one chemical of the input stream to generate a product stream that exits the second microchannel unit operation, where the first microchannel unit operation and the second unit operation share a housing.
摘要翻译：一种用于串联进行至少两个单元操作的方法，该方法包括以下步骤：（a）将进料流引导到集成组件中，其包括在进料流的至少一种化学品上的第一微通道单元操作以产生在第一组离散微通道中离开第一微通道单元操作的分布式输出流，其隔离通过离散微通道的流动; 和（b）将第一微通道单元操作的分布式输出流引导到作为分布式输入流的第二微通道单元操作中，以继续隔离第一组离散微通道之间的流动，并且至少一种化学物质进行至少一种操作以产生离开第二微通道单元操作的产品流，其中第一微通道单元操作和第二单元操作共享外壳。

60. 发明授权

US08206597B2 Protected alloy surfaces in microchannel apparatus and catalysts, alumina supported catalysts, catalyst intermediates, and methods of forming catalysts and microchannel apparatus 有权
标题翻译：微通道设备和催化剂中受保护的合金表面，氧化铝负载催化剂，催化剂中间体以及形成催化剂和微通道设备的方法
公开(公告)号：US08206597B2
公开(公告)日：2012-06-26
申请号：US13012797
申请日：2011-01-24
申请人： Barry L. Yang , Anna Lee Tonkovich , Junko M. Watson , Francis P. Daly , Sean P. Fitzgerald , Chunshe Cao , Xiaohong Li , Terry Mazanec , Bradley R. Johnson , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang , Richard Long , Ya-Huei Chin
发明人： Barry L. Yang , Anna Lee Tonkovich , Junko M. Watson , Francis P. Daly , Sean P. Fitzgerald , Chunshe Cao , Xiaohong Li , Terry Mazanec , Bradley R. Johnson , Ravi Arora , David J. Hesse , Dongming Qiu , Rachid Taha , Jeffrey J. Ramler , Yong Wang , Richard Long , Ya-Huei Chin
IPC分类号： B01D37/00 , B01D39/00 , B01J8/00
CPC分类号： C01B3/384 , B01J19/0093 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/0236 , C01B2203/0233 , C01B2203/0811 , C23C8/10 , C23C16/12 , C23C16/56 , H01M2008/1293 , Y02P20/52 , Y10S585/92 , Y10S585/924
摘要： The invention describes microchannel apparatus and catalysts that contain a layer of a metal aluminide or are made in a process in which a metal aluminide layer is formed as an intermediate. Certain processing conditions have surprisingly been found to result in superior coatings. The invention includes chemical processes conducted through apparatus described in the specification. Other catalysts and catalyst synthesis techniques are also described.
摘要翻译：本发明描述了包含金属铝化物层的微通道装置和催化剂，或者是在其中形成金属铝化物层作为中间体的方法制造的。令人惊奇地发现某些加工条件导致优异的涂层。本发明包括通过本说明书中描述的设备进行的化学过程。还描述了其它催化剂和催化剂合成技术。

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