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    • 7. 发明申请
    • APPARATUS AND PROCESS FOR THE PREPARATION OF ACETYLENE AND SYNTHESIS GAS
    • US20180170829A1
    • 2018-06-21
    • US15129094
    • 2015-03-25
    • BASF SE
    • Maximilian VICARISusanne BRITZIUSLilian KARA-HIPPENMichael RUSSMatthias KERNChristian WEICHERT
    • C07C2/78C01B3/36C07C11/24B01D3/14C07D207/267
    • C07C2/78B01D3/14B01J2219/00006C01B3/36C07C9/04C07C9/06C07C9/14C07C11/04C07C11/24C07C15/04C07C15/06C07C15/073C07C15/08C07C15/58C07D207/267
    • An apparatus (10) for the preparation of acetylene and synthesis gas by partial oxidation of hydrocarbons with oxygen is proposed. The apparatus (10) comprises a reactor (12), wherein the reactor (12) comprises a burner block (14) with a furnace chamber for the preparation of a composition C1 comprising at least acetylene and substituted acetylene, a first scrubber (22) which is constructed for adding a solvent to the composition C1 to obtain a composition C2, a second scrubber (26) which is constructed for adding the solvent to the composition C2 to obtain a composition C3, a first stripper (36) which is constructed for stripping the composition C3 to obtain a composition C4 comprising the substituted acetylene, acetylene and the solvent and for separating off the acetylene, a first column (46) which is constructed for partial degassing of the composition C4 under a pressure of from 1.0 bar to 1.5 bar to obtain a composition C5 and a first amount A1 of the solvent, a second stripper (56) to which the composition C5 can be fed for stripping a composition C9 to obtain a second amount A2 of the solvent and a composition C6, a third stripper (68) which is constructed for stripping the solvent from the first scrubber (22) to obtain a composition C9, wherein the third striper (68) is connected to the second stripper (56) for feeding the composition C9 to the second stripper (56), an apparatus (72) for adding a diluting gas to the composition C5, which is arranged between the first column (46) and the second stripper (56), a second column (76) which is constructed for adding water to the composition C6 to obtain a composition C7 comprising a third amount A3 of the solvent and water and to obtain a composition C8 comprising the substituted acetylene, and a mixing condenser (82) which is constructed for adding water to the composition C8 to obtain a composition C11 comprising the substituted acetylene.A process for the preparation of acetylene and synthesis gas by partial oxidation of hydrocarbons with oxygen is further proposed.