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51. 发明授权

US07569721B2 Process for conducting equilibrium-limited reactions 有权
标题翻译：进行平衡限制反应的方法
公开(公告)号：US07569721B2
公开(公告)日：2009-08-04
申请号：US10544817
申请日：2004-02-19
申请人： Leah A. Patterson , Fungau Nmn Ho
发明人： Leah A. Patterson , Fungau Nmn Ho
IPC分类号： C07C69/52 , C07C67/48
CPC分类号： C07B41/12 , C07C67/08 , C07C67/327 , Y02P20/582 , C07C69/54
摘要： This invention relates to a process for conducting equilibrium-limited reactions, such as esterification and alcoholysis reactions, that uses two reaction zones. The first reaction zone operates under reaction conditions that retain at least a portion of the product in a liquid phase, and at least a portion of the liquid from the first reaction zone is introduced into a second reaction zone which operates under conditions sufficient to crack heavies, for example, Michael-addition heavies, formed in or introduced into said second reaction zone and to vaporize at least a portion of the product upon production thereof. Such a process allows for removal of product from the reaction system while catalyst desirably remains in the reaction system.
摘要翻译：本发明涉及一种使用两个反应区进行平衡有限反应的方法，如酯化和醇解反应。第一反应区在反应条件下操作，该反应条件保留产物在液相中的至少一部分，并且来自第一反应区的至少一部分液体被引入第二反应区，其在足以破裂重质的条件下操作例如，形成或引入所述第二反应区的迈克尔加成物重质物，并在其生产时汽化至少一部分产物。这种方法允许从反应体系中除去产物，同时催化剂理想地保留在反应体系中。

52. 发明授权

US07507846B2 Method and apparatus for refining biodiesel 失效
标题翻译：炼制生物柴油的方法和装置
公开(公告)号：US07507846B2
公开(公告)日：2009-03-24
申请号：US10547574
申请日：2004-03-17
申请人： Michael F. Pelly
发明人： Michael F. Pelly
IPC分类号： C11C3/04 , C07C69/52
CPC分类号： C11C3/003 , C07C67/03 , C07C67/08 , C10L1/026 , C11C1/08 , C11C3/10 , Y02E50/13 , Y02P20/582 , Y02P30/20 , C07C69/24 , C07C69/52
摘要： Method and apparatus for producing biodiesel fuel, i.e., alkyl ester, from vegetable and/or animal oil. A transesterification catalyst is prepared in a base catalyst tank by spraying alkyl alcohol under pressure through jets at metal hydroxide pellets until the pellets have fully reacted with the alcohol. The oil is heated and transesterified in the presence of alkyl alcohol and the transesterification catalyst in a closed, recirculating transesterification flow system under slight cavitation to yield product alkyl ester and product glycerol. Cavitation is achieved by permitting air to enter the transesterification flow system through an adjustable air inlet valve. When permitted to stand, product alkyl ester forms an upper layer that is decanted and subjected to purification steps, to remove particulates and alkyl alcohol from the product alkyl ester, and a lower layer of product glycerol is drained away. Purification of the product alkyl ester preferably includes subjecting the product alkyl ester to an overhead water mist in a wash tank with simultaneous infusion of a stream of air bubbles. Alcohol vapor is reclaimed as liquid alcohol within an alcohol condenser and stored for reuse. If the oil contains free fatty acids, prior to transesterification, the oil is heated and the free fatty acids are esterified in the presence of an esterification catalyst and alkyl alcohol. For safety, baffles and explosion damper/flame arrestors are provided in locations where flammable vapors pose a risk.
摘要翻译：用于从植物油和/或动物油生产生物柴油燃料（即烷基酯）的方法和装置。在碱性催化剂罐中通过在压力下喷射烷基醇在金属氢氧化物颗粒中喷射来制备酯交换催化剂，直到颗粒与醇完全反应。将油在烷基醇和酯交换催化剂存在下在密闭的循环酯交换流动体系中加热和酯交换，在轻微气蚀下得到产物烷基酯和产物甘油。通过允许空气通过可调节进气阀进入酯交换流系统来实现空化。产物烷基酯当被允许放置时，形成倾析并经过纯化步骤的上层，从产物烷基酯中除去微粒和烷基醇，并将产物甘油的下层排出。产物烷基酯的纯化优选包括使产物烷基酯在洗涤槽中的顶部水雾下同时输入气泡流。酒精蒸汽在酒精冷凝器内作为液体酒精回收并储存以供重新使用。如果油含有游离脂肪酸，则在酯交换前，加热油，游离脂肪酸在酯化催化剂和烷基醇存在下酯化。为安全起见，挡风玻璃和爆炸阻尼器/阻火器在易燃蒸汽造成风险的地方提供。

53. 发明申请

US20090074709A1 METHODS, DEVICES AND SYSTEMS FOR BIOCIDAL SURFACE ACTIVITY 审中-公开
标题翻译：方法，用于生物表面活性的装置和系统
公开(公告)号：US20090074709A1
公开(公告)日：2009-03-19
申请号：US12209334
申请日：2008-09-12
申请人： RICHARD R. KOEPSEL , ALAN J. RUSSELL , THANGAPPAN RAVIKUMAR
发明人： RICHARD R. KOEPSEL , ALAN J. RUSSELL , THANGAPPAN RAVIKUMAR
IPC分类号： A01N43/40 , A01N37/06 , A01N43/36 , C08F118/02 , C08F226/06 , C08F20/52 , C08F20/44 , C08F22/10 , C07C69/52 , C07D211/20 , C07C255/08 , C07C211/62 , C07C233/01 , C07D213/20 , A01P1/00
CPC分类号： C07D213/20 , A01N33/12 , C07C69/54 , C07C219/08 , C07D295/084 , C08F220/56
摘要： A method of applying a biocidal polymer to a surface including applying a solution of the biocidal polymer to the surface, wherein the biocidal polymer includes biocidal groups and the biocidal polymer is insoluble in water. The biocidal groups can be selected from the group consisting of quaternary salt groups or haloamino groups.
摘要翻译：一种将杀生物聚合物施用于表面的方法，包括将杀生物聚合物的溶液施用于表面，其中杀生物聚合物包括杀生物基团，并且杀生物聚合物不溶于水。杀生物基团可以选自季盐基团或卤代氨基基团。

54. 发明申请

US20090062296A1 Prostaglandin derivatives 失效
标题翻译：前列腺素衍生物
公开(公告)号：US20090062296A1
公开(公告)日：2009-03-05
申请号：US11478129
申请日：2006-06-28
申请人： Francesca Benedini , Valerio Chiroli , Wesley Kwan Mung Chong , Achim Hans-Peter Krauss , Michael Ross Niesman , Ennio Ongini
发明人： Francesca Benedini , Valerio Chiroli , Wesley Kwan Mung Chong , Achim Hans-Peter Krauss , Michael Ross Niesman , Ennio Ongini
IPC分类号： A61K31/495 , C07C233/01 , A61K31/164 , C07C69/52 , A61K31/445 , A61P27/02 , A61P9/12 , C07D211/06 , A61K31/215 , C07D241/04
CPC分类号： C07C405/00 , C07D207/08 , C07D295/12 , C07D295/13
摘要： Nitroderivatives of prostaglandin amides having improved pharmacological activity and enhanced tolerability are described. They can be employed for the treatment of glaucoma and ocular hypertension.
摘要翻译：描述了具有改善的药理活性和增强的耐受性的前列腺素酰胺的硝基衍生物。可用于治疗青光眼和高眼压症。

55. 发明申请

US20090053826A1 Electropolymerisable monomers that are soluble in aqueous solution and electroactive probes that can be obtained with such monomers 有权
标题翻译：可溶于水溶液的电聚合单体和可用这些单体获得的电活性探针
公开(公告)号：US20090053826A1
公开(公告)日：2009-02-26
申请号：US11988655
申请日：2006-07-07
申请人： Aurelie Bouchet , Carole Chaix , Bernard Mandrand
发明人： Aurelie Bouchet , Carole Chaix , Bernard Mandrand
IPC分类号： G01N33/53 , C07H21/00 , C07K2/00 , C07K14/00 , C07K16/00 , C08B37/00 , C07D235/02 , C07D207/30 , C07D333/02 , C07D209/04 , C07C211/43 , C07C11/24 , C07C15/02 , C07C15/38 , C07D307/34 , C07D237/02 , C07D209/82 , C07C69/52 , C08F2/16 , C07F15/02
CPC分类号： C08G73/0611 , C07F17/02 , C08F2/10 , C08F2/16 , C08F2/52 , C08G61/124
摘要： The invention relates to an electropolymerizable monomer, intended to be polymerized in aqueous solution, comprising a single electropolymerizable unit and an electron-donating group, characterized in that it also comprises at least one arm ionizable in aqueous solution. The invention also relates to the polymerization process, to the electroactive probe thus obtained and to the method for the detection of a target ligand in a biological sample.
摘要翻译：本发明涉及旨在在水溶液中聚合的电聚合单体，其包含单个可电聚合单元和给电子基团，其特征在于其还包含至少一个可在水溶液中电离的臂。本发明还涉及聚合方法，由此获得的电活性探针和生物样品中靶配体的检测方法。

56. 发明授权

US07473749B2 Preparation of topcoat compositions and methods of use thereof 失效
标题翻译：面漆组合物的制备及其使用方法
公开(公告)号：US07473749B2
公开(公告)日：2009-01-06
申请号：US11159477
申请日：2005-06-23
申请人： Hiroshi Ito , Linda Karin Sundberg
发明人： Hiroshi Ito , Linda Karin Sundberg
IPC分类号： C07C69/52
CPC分类号： G03F7/2041 , G03F7/0046 , G03F7/11
摘要： A topcoat composition that includes a fluorine-containing polymer and a casting solvent selected from an alcohol is provided. Also provided is a method of forming an image on a photoresist that includes forming a photoresist over a substrate; applying a topcoat composition, the topcoat composition comprising at least one fluorine-containing polymer and a casting solvent, onto the photoresist; removing the casting solvent of the topcoat composition resulting in the formation of a topcoat material over the photoresist; exposing the photoresist to radiation, the radiation changing a chemical composition of the regions of the photoresist exposed to the radiation, forming exposed and unexposed regions in the photoresist; and removing i) the topcoat material and ii) the exposed regions of the photoresist or the unexposed regions of the photoresist.
摘要翻译：提供了包含含氟聚合物和选自醇的流延溶剂的面漆组合物。还提供了在光致抗蚀剂上形成图像的方法，其包括在基板上形成光致抗蚀剂; 将面漆组合物，包含至少一种含氟聚合物和浇铸溶剂的面漆组合物涂覆到光致抗蚀剂上; 除去顶涂层组合物的浇铸溶剂，导致在光致抗蚀剂上形成顶涂层材料; 将光致抗蚀剂暴露于辐射，辐射改变暴露于辐射的光刻胶的区域的化学组成，在光致抗蚀剂中形成暴露和未曝光的区域; 并去除i）面漆材料和ii）光致抗蚀剂的曝光区域或光致抗蚀剂的未曝光区域。

57. 发明授权

US07411086B2 Process for the production of n-alkylaminoalkyl (meth)acrylates 有权
标题翻译：（甲基）丙烯酸正烷基氨基烷基酯的制备方法
公开(公告)号：US07411086B2
公开(公告)日：2008-08-12
申请号：US10558193
申请日：2004-05-27
申请人： Shuhei Otsuka , Akira Ogawa , Tohru Endoh , Shingo Tanaka
发明人： Shuhei Otsuka , Akira Ogawa , Tohru Endoh , Shingo Tanaka
IPC分类号： C07C69/52
CPC分类号： C07C213/06 , C07C219/08
摘要： The present invention is to provide a method of producing an N-alkylaminoalkyl (meth)acrylate containing a small amount of low boiling components, especially, containing a small amount of raw components, without any complicated operations or special apparatuses. The method of producing an N-alkylaminoalkyl (meth)acrylate comprising the steps of: (A) performing the reaction between the (meth)acrylic acid ester and the N-alkylaminoalkyl alcohol in a presence of a catalyst to obtain a reaction solution containing the N-alkylaminoalkyl (meth)acrylate; (B) distilling out components which have lower boiling points than the N-alkylaminoalkyl (meth)acrylate from the reaction solution obtained by the step (A); and (C) distilling the N-alkylaminoalkyl (meth)acrylate; and further comprising the step of: (D) adjusting water concentration at a range from 0.01 to 1 wt %. in the reaction solution which is located after the step (A) and before the step (C).
摘要翻译：本发明提供一种含有少量低沸点成分的（甲基）丙烯酸N-烷基氨基烷基酯（特别是含有少量原料成分）的方法，无需任何复杂的操作或特殊设备。（甲基）丙烯酸N-烷基氨基烷基酯的制造方法，其特征在于：（A）在催化剂存在下进行（甲基）丙烯酸酯与N-烷基氨基烷基醇的反应，得到含有（甲基）丙烯酸N-烷基氨基烷基酯; （B）从步骤（A）获得的反应溶液中蒸馏沸点低于（甲基）丙烯酸N-烷基氨基烷基酯的组分; 和（C）蒸馏（甲基）丙烯酸N-烷基氨基烷基酯; 并且还包括以下步骤：（D）将水浓度调节在0.01至1重量％的范围内。在步骤（A）之后和步骤（C）之前的反应溶液中。

58. 发明申请

US20080167332A1 Novel Compounds 243 审中-公开
标题翻译：新型化合物243
公开(公告)号：US20080167332A1
公开(公告)日：2008-07-10
申请号：US11779700
申请日：2007-07-18
申请人： Scott Gibson , Barry Elkins , Mike Rogers , Ian Hassall , Hong Gu , Zhenyu Wang , Vinod Kumar , Synthana Suresh Kumar , Santosh Kavitake , Sidda Lingesha , Eric Merifield , David Ennis , John Pavey , Austen Pimm , James Reuberson , Bo-Goran Josefsson , Martin Hemmerling , Svetlana Ivanova , Marguerite Mensonides-Harsema , Hakan Schulz , John Mo , Tomas Eriksson , Per Strandberg
发明人： Scott Gibson , Barry Elkins , Mike Rogers , Ian Hassall , Hong Gu , Zhenyu Wang , Vinod Kumar , Synthana Suresh Kumar , Santosh Kavitake , Sidda Lingesha , Eric Merifield , David Ennis , John Pavey , Austen Pimm , James Reuberson , Bo-Goran Josefsson , Martin Hemmerling , Svetlana Ivanova , Marguerite Mensonides-Harsema , Hakan Schulz , John Mo , Tomas Eriksson , Per Strandberg
IPC分类号： A61K31/438 , A61P11/00 , C07D491/107 , C07C275/32 , C07D211/52 , C07C69/76 , C07C69/52 , C07C233/81 , C07C233/00 , C07D303/46 , A61P29/00
CPC分类号： C07C233/25 , C07C69/92 , C07C235/60 , C07D211/48 , C07D303/23 , C07D491/107
摘要： Compounds of formula (I) wherein R1, R3, R4, R5, R6, R7, and R10 are as defined in the specification, are described. The present invention also relates to pharmaceutical composition comprising said compounds and to the use of said compounds in therapy. The present invention further relates to processes for the preparation of said compounds and to new intermediates useful in the preparation thereof. Beside, the invention relates to salts and polymorphic forms of the new compounds as well as the preparation thereof.
摘要翻译：式（I）的化合物，其中R 1，R 3，R 4，R 5，R SUP > 6 ，R＆lt; 7＆gt;和＆lt; 10＆gt;如说明书中所定义。本发明还涉及包含所述化合物的药物组合物和所述化合物在治疗中的用途。本发明还涉及制备所述化合物的方法和可用于其制备的新中间体。除此之外，本发明涉及新化合物的盐和多晶型物及其制备。

59. 发明授权

US07390917B2 Method for producing mixture of fluoroalkyl iodide telomers and method for producing mixture of fluorine-containing (meth)acrylate esters 有权
标题翻译：氟烷基碘调节剂混合物的制备方法和含氟（甲基）丙烯酸酯的混合物的制造方法
公开(公告)号：US07390917B2
公开(公告)日：2008-06-24
申请号：US11074707
申请日：2005-03-09
申请人： Yukio Homoto , Kunitada Tanaka
发明人： Yukio Homoto , Kunitada Tanaka
IPC分类号： C07C69/52
CPC分类号： C07C19/16 , C07C17/275 , C07C17/278 , C07C67/10 , C07C69/653
摘要： A method of producing a mixture of fluorine-containing (meth)acrylate esters, the method including: (A) a telomerization step of obtaining the mixture of the fluoroalkyl iodide telomers; (B) an ethylene addition step of adding ethylene to the mixture of the fluoroalkyl iodide telomers obtained in the step (A) to give a mixture of ethylene adducts; and (C) an esterification step of reacting the mixture of the ethylene adducts obtained in the step (B) with a (meth)acrylate compound to obtain fluorine-containing (meth)acrylate esters.
摘要翻译：一种制备含氟（甲基）丙烯酸酯混合物的方法，该方法包括：（A）得到氟代烷基碘调节剂的混合物的调聚步骤; （B）乙烯加成步骤，在步骤（A）得到的氟烷基碘调节剂的混合物中加入乙烯，得到乙烯加成物的混合物; 和（C）使步骤（B）中获得的乙烯加成物的混合物与（甲基）丙烯酸酯化合物反应得到含氟（甲基）丙烯酸酯的酯化步骤。

60. 发明申请

US20070265423A1 Bifunctional phenylene ether oligomer, its derivatives, its use and process for the production thereof 有权
标题翻译：双官能亚苯基醚低聚物，其衍生物，其用途及其制备方法
公开(公告)号：US20070265423A1
公开(公告)日：2007-11-15
申请号：US11812892
申请日：2007-06-22
申请人： Akikazu Amagai , Kenzi Ishii , Kiyonari Hiramatsu , Makoto Miyamoto , Daisuke Ohno , Katsutoshi Yamazaki , Yasumasa Norisue
发明人： Akikazu Amagai , Kenzi Ishii , Kiyonari Hiramatsu , Makoto Miyamoto , Daisuke Ohno , Katsutoshi Yamazaki , Yasumasa Norisue
IPC分类号： C08G63/66 , C07C69/52 , C07C69/62
CPC分类号： C08G59/063 , C08G65/44 , C08G65/485 , C08G2650/20 , C08L2312/00 , H05K1/0326 , Y10T428/24994 , Y10T428/31511
摘要： A bifunctional phenylene ether oligomer of the formula (1), obtained by oxidation polymerization of a bivalent phenol of the formula (2) and a monovalent phenol of the formula (3), wherein —X— is represented by the formula (2′), and Y—O— is represented by the formula (3), R2, R3, R4, R8, R9, R10 and R11 in the formula (2′) and the formula (3′) being required not to be a hydrogen atom, and its use.
摘要翻译：通过式（2）的二价苯酚和式（3）的一价苯酚的氧化聚合获得的式（1）的双功能亚苯基醚低聚物，其中-X-由式（2'）表示，，YO-由式（3）表示，式（2'）和式（3'）中的R2，R3，R4，R8，R9，R10和R11不为氢原子，其使用。

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