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71. 发明授权

US09352968B2 Graphene materials having randomly distributed two-dimensional structural defects 有权
公开(公告)号：US09352968B2
公开(公告)日：2016-05-31
申请号：US14025572
申请日：2013-09-12
申请人： Northwestern University
发明人： Harold H. Kung , Xin Zhao , Cary M. Hayner , Mayfair C. Kung
IPC分类号： C01B31/04 , H01B1/04 , B82Y30/00 , B82Y40/00 , H01M4/134 , H01M4/38 , H01M4/62 , H01M4/36 , H01M10/052
CPC分类号： C01B31/0446 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/23 , H01B1/04 , H01M4/134 , H01M4/386 , H01M4/625 , H01M10/052 , Y02P70/54
摘要： Graphene-based storage materials for high-power battery applications are provided. The storage materials are composed of vertical stacks of graphene sheets and have reduced resistance for Li ion transport. This reduced resistance is achieved by incorporating a random distribution of structural defects into the stacked graphene sheets, whereby the structural defects facilitate the diffusion of Li ions into the interior of the storage materials.

72. 发明授权

US09327985B2 Graphene oxide sheet, article containing graphene-containing substance produced by reducing the graphene oxide sheet, and process for production of the graphene oxide sheet 有权
标题翻译：石墨烯氧化物片，通过还原石墨烯氧化物片制备的含有含石墨烯的物质的制品，以及石墨烯氧化物片的制造方法
公开(公告)号：US09327985B2
公开(公告)日：2016-05-03
申请号：US13515889
申请日：2009-12-18
申请人： Bunshi Fugetsu
发明人： Bunshi Fugetsu
IPC分类号： C01B31/02 , C01B31/04 , H01B1/04 , B82Y30/00 , B82Y40/00 , F16D69/02
CPC分类号： C01B31/0476 , B82Y30/00 , B82Y40/00 , C01B31/043 , C01B32/192 , C01B32/23 , F16D69/026 , F16D2200/006 , F16D2200/0095
摘要： [Means for solving]A graphene oxide sheet which changes to a substance having a graphene structure when reduced, and which is obtainable by dispersing a graphene-containing carbon substance using a dispersant to reduce the size of the aggregate units of the graphene-containing carbon substance, and then oxidizing the graphene-containing carbon substance.
摘要翻译： [解决方法]在还原时改变为具有石墨烯结构的物质的石墨烯氧化物片材，其可以通过使用分散剂分散含石墨烯的碳物质以减小含石墨烯碳的骨料单元的尺寸而获得物质，然后氧化含石墨烯的碳物质。

73. 发明授权

US09266737B2 Method and apparatus for manufacturing graphite oxide 有权
标题翻译：石墨氧化物的制造方法和装置
公开(公告)号：US09266737B2
公开(公告)日：2016-02-23
申请号：US14581150
申请日：2014-12-23
申请人： IDT INTERNATIONAL CO., LTD.
发明人： Byoung Kyu Ji , Jung Young Choi , Cheol Min Shin , Shi Choon Lee
IPC分类号： C01B31/04 , B01J19/10 , B01J8/20 , B01J19/18 , B82Y40/00
CPC分类号： C01B31/043 , B01J8/20 , B01J19/10 , B01J19/18 , B01J19/1831 , B01J19/1862 , B01J2208/00176 , B01J2219/0004 , B01J2219/00099 , B01J2219/00103 , B01J2219/00263 , B82Y40/00 , C01B32/192 , C01B32/23
摘要： There is provided a method and an apparatus for preparing graphite oxide. In accordance with the present disclosure, when an oxidizer is added by stages into a sequencing batch oxidizer mixer connected in multiple stages at a constantly low temperature, the oxidizer is mixed therein while suppressing an oxidation reaction. During an oxidation reaction of graphite, in a risky range of overheating and explosion, a tube type reactor equipped within a heat exchanger is used to accurately control a local temperature and the oxidizer can permeate between layers of the graphite with increased efficiency under ultrasonication. In an additional reaction range out of the risky range, a continuous stirred tank reactor is used to mature the oxidation reaction, so that a risk of explosion during manufacturing of graphite oxide can be reduced and a great amount of graphite oxide can be mass-produced economically.
摘要翻译：提供了一种制备氧化石墨的方法和装置。根据本公开，当将氧化剂分阶段加入到以恒定低温连续多级连续的间歇式氧化器混合器中时，氧化剂在其中混合，同时抑制氧化反应。在石墨的氧化反应中，在过热和爆炸的危险范围内，使用装在热交换器内的管式反应器来精确地控制局部温度，并且氧化剂可以在超声波处理下以更高的效率在石墨层之间渗透。在危险范围之外的另外的反应范围内，使用连续搅拌釜反应器来使氧化反应成熟，从而可以减少制造氧化石墨过程中爆炸的风险，并可大量生产大量氧化石墨经济上

74. 发明申请

US20150360197A1 Spinel-Type Lithium Titanium Oxide/Graphene Composite and Method of Preparing the Same 有权
标题翻译：尖晶石型锂钛/石墨烯复合物及其制备方法
公开(公告)号：US20150360197A1
公开(公告)日：2015-12-17
申请号：US14836045
申请日：2015-08-26
申请人： INDUSTRY-ACADEMIC COOPERATION FOUNDATION, YONSEI UNIVERSITY
发明人： Kwang Bum KIM , Hyun Kyung KIM , Ji Young KIM
IPC分类号： B01J19/12 , H01M4/36 , H01M4/04
CPC分类号： B01J19/126 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01G23/005 , C01P2002/32 , C01P2002/72 , C01P2002/82 , C01P2004/04 , C01P2004/64 , C01P2006/40 , H01B1/18 , H01M4/04 , H01M4/364 , H01M4/485 , H01M4/587 , H01M10/052
摘要： A spinel-type lithium titanium oxide/graphene composite and a method of preparing the same are provided. The method can be useful in simplifying a manufacturing process and shortening a manufacturing time using microwave associated solvothermal reaction and post heat treatment, and the spinel-type lithium titanium oxide/graphene composite may have high electrochemical performances due to its excellent capacity and rate capability and long lifespan, and thus be used as an electrode material of the lithium secondary battery.
摘要翻译：提供尖晶石型锂钛/石墨烯复合物及其制备方法。该方法在简化制造工艺和缩短使用微波相关溶剂热反应和后热处理的制造时间方面是有用的，并且由于其优异的容量和速率能力，尖晶石型锂钛/石墨烯复合材料可能具有高电化学性能，寿命长，因此用作锂二次电池的电极材料。

75. 发明授权

US09177688B2 Carbon nanotube-graphene hybrid transparent conductor and field effect transistor 有权
标题翻译：碳纳米管 - 石墨烯混合透明导体和场效应晶体管
公开(公告)号：US09177688B2
公开(公告)日：2015-11-03
申请号：US13301943
申请日：2011-11-22
申请人： Ageeth A. Bol , Bhupesh Chandra , Amal Kasry , Ahmed Maarouf , Glenn J. Martyna , George S. Tulevski
发明人： Ageeth A. Bol , Bhupesh Chandra , Amal Kasry , Ahmed Maarouf , Glenn J. Martyna , George S. Tulevski
IPC分类号： B32B9/00 , H01B1/04 , C01B31/02 , C01B31/04 , C23C16/26 , H01L51/10 , H01L29/16 , H01L29/778 , H01L29/66 , H01L29/786 , B82Y10/00 , B82Y30/00 , B82Y40/00 , H01L51/00 , H01L51/05 , H01L29/06
CPC分类号： H01L51/0048 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/158 , C01B32/182 , C01B32/186 , C01B32/192 , C01B2202/00 , C01B2204/00 , C23C16/26 , H01B1/04 , H01L29/0673 , H01L29/1606 , H01L29/66742 , H01L29/778 , H01L29/78618 , H01L29/78684 , H01L29/78696 , H01L51/0025 , H01L51/0545 , H01L51/0562 , H01L51/0566 , H01L51/102 , H01L51/105 , Y10S977/742 , Y10S977/75 , Y10S977/938 , Y10T428/30
摘要： A nanotube-graphene hybrid film and method for forming a cleaned nanotube-graphene hybrid film. The method includes depositing nanotube film over a substrate to produce a layer of nanotube film, removing impurities from a surface of the layer of nanotube film not contacting the substrate to produce a cleaned layer of nanotube film, depositing a layer of graphene over the cleaned layer of nanotube film to produce a nanotube-graphene hybrid film, and removing impurities from a surface of the nanotube-graphene hybrid film to produce a cleaned nanotube-graphene hybrid film, wherein the hybrid film has improved electrical performance. Another method includes depositing nanotube film over a metal foil to produce a layer of nanotube film, placing the metal foil with as-deposited nanotube film in a chemical vapor deposition furnace to grow graphene on the nanotube film to form a nanotube-graphene hybrid film, and transferring the nanotube-graphene hybrid film over a substrate.
摘要翻译：一种纳米管 - 石墨烯复合膜及其形成清洁的纳米管 - 石墨烯混合膜的方法。该方法包括在衬底上沉积纳米管膜以产生纳米管膜层，从不接触衬底的纳米管膜的表面去除杂质以产生清洁的纳米管膜层，在清洁层上沉积一层石墨烯的纳米管膜以制造纳米管 - 石墨烯混合膜，并从纳米管 - 石墨烯混合膜的表面除去杂质，以制造清洁的纳米管 - 石墨烯混合膜，其中混合膜具有改善的电性能。另一种方法包括在金属箔上沉积纳米管膜以产生纳米管膜层，将具有沉积纳米管膜的金属箔放置在化学气相沉积炉中以在纳米管膜上生长石墨烯以形成纳米管 - 石墨烯混合膜，并将纳米管 - 石墨烯混合膜转移到衬底上。

76. 发明申请

US20150284253A1 Process for producing highly conducting graphitic films from graphene liquid crystals 有权
标题翻译：由石墨烯液晶生产高导电性石墨膜的方法
公开(公告)号：US20150284253A1
公开(公告)日：2015-10-08
申请号：US13999912
申请日：2014-04-03
申请人： Aruna Zhamu , Bor Z. Jang
发明人： Aruna Zhamu , Bor Z. Jang
IPC分类号： C01B31/04 , B05D3/02 , B05D3/12
CPC分类号： C01B32/182 , C01B32/184 , C01B32/192 , C01B32/198 , C01B32/23 , C01B2204/22 , C01P2006/10 , C01P2006/32 , C01P2006/40 , C09K5/14 , H01B1/04 , H01B1/24
摘要： A process for producing a highly oriented graphitic film, consisting of (a) preparing a dispersion having graphene oxide (GO) or chemically functionalized graphene (CFG) dispersed in a liquid to form a liquid crystal phase (but not in a GO gel state); (b) depositing the dispersion onto a supporting substrate to form a layer of GO or CFG under an orientation-inducing stress; (c) removing the liquid to form a dried GO or CFG layer having an inter-plane spacing d002 of 0.4 nm to 1.2 nm; (d) thermally reducing the dried layer at a first temperature higher than 100° C. to produce a porous layer of reduced GO or CFG; (e) further heat-treating the porous layer at a second temperature to produce a porous graphitic film having an inter-plane spacing d002 less than 0.4 nm; and (f) compressing the porous graphitic film to produce the highly oriented graphitic film.
摘要翻译：一种高取向石墨膜的制造方法，由（a）制备分散在液体中的石墨烯氧化物（GO）或化学官能化石墨烯（CFG）的分散体形成液晶相（但不在GO凝胶状态） ; （b）将分散体沉积在支撑基底上以在取向诱导应力下形成一层GO或CFG; （c）去除液体以形成具有0.4nm至1.2nm的平面间距d002的干GO或CFG层; （d）在高于100℃的第一温度下热干燥干燥层以产生减少的GO或CFG的多孔层; （e）在第二温度下进一步热处理多孔层以产生具有小于0.4nm的平面间距d002的多孔石墨膜; 和（f）压缩多孔石墨膜以产生高取向的石墨膜。

77. 发明申请

US20150270548A1 STABLE DISPERSIONS OF SINGLE AND MULTIPLE GRAPHENE LAYERS IN SOLUTION 有权
标题翻译：单个和多个石墨层在溶液中的稳定分散
公开(公告)号：US20150270548A1
公开(公告)日：2015-09-24
申请号：US14666692
申请日：2015-03-24
申请人： BELENOS CLEAN POWER HOLDING AG
发明人： Reinhard Nesper , Tommy Kaspar
IPC分类号： H01M4/587 , H01B13/32 , H01B1/04
CPC分类号： H01M4/587 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B2204/02 , C01B2204/28 , C01B2204/30 , H01B1/04 , H01B13/32 , H01M10/052 , Y02E60/324 , Y02P70/54 , Y10T428/30
摘要： A method for producing colloidal graphene dispersions comprises the steps of: (i) stirring graphite oxide in an aqueous dispersion medium to form a dispersion; (ii) determining if the dispersion is optically clear in a light microscope at 1000 fold magnification after 1 to 5 hours of stirring, and, if not clear, removing any undissolved impurities in the dispersion, in order to form a colloidal graphene oxide dispersion, or a multi-graphene oxide dispersion, that is optically clear in a light microscope at 1000 fold magnification; and (iii) thermally reducing the graphene oxide, or multi-graphene oxide, in dispersion in the aqueous dispersion medium at a temperature between 120° C. and 170° C. under pressure in order to ensure that the dispersion medium is not evaporated to form a stable colloidal graphene dispersion or a stable multi-graphene dispersion. Using the method used for the preparation of the starting dispersion a graphene or a multi-graphene dispersion is obtained that can be further processed to multi-graphene with larger inter-planar distances than graphite. Such dispersions and multi-graphenes are suitable materials in the manufacturing of rechargeable lithium ion batteries.
摘要翻译：制备胶体石墨烯分散体的方法包括以下步骤：（i）在水性分散介质中搅拌石墨氧化物以形成分散体; （ii）在1〜5小时的搅拌后，在光学显微镜中以1000倍放大率确定分散体是否光学透明，如果不清楚，则除去分散体中的任何未溶解的杂质，以形成胶态石墨烯氧化物分散体，或多石墨烯氧化物分散体，其在1000倍放大倍数的光学显微镜中是光学透明的; 和（iii）在120℃和170℃之间的温度下在压力下将氧化石墨烯或氧化石墨烯在热分解中热分解，以确保分散介质不被蒸发形成稳定的胶体石墨烯分散体或稳定的多石墨烯分散体。使用用于制备起始分散体的方法，获得石墨烯或多石墨烯分散体，其可以进一步加工成具有比石墨更大的平面间距离的多石墨烯。这种分散体和多石墨烯是可再生锂离子电池制造中的合适材料。

78. 发明申请

US20150248972A1 LINKED STACKS OF PARTLY REDUCED GRAPHENE, METHOD FOR PRODUCING LINKED STACKS OF PARTLY REDUCED GRAPHENE, POWDER COMPRISING LINKED STACKS OF PARTLY REDUCED GRAPHENE, FILM COMPRISING LINKED STACKS OF PARTLY REDUCED GRAPHENE, GRAPHENE ELECTRODE FILM, METHOD FOR PRODUCING GRAPHENE ELECTRODE FILM, AND GRAPHENE CAPACITOR 有权
标题翻译：一部分减少的石墨的连接堆叠，一部分减少的石墨的连接堆叠的方法，包含部分减少的石墨的链接堆的粉末，包含部分还原的石墨的连接堆的膜，石墨电极膜，用于生产石墨电极膜的方法和石墨电容器
公开(公告)号：US20150248972A1
公开(公告)日：2015-09-03
申请号：US14425436
申请日：2013-09-04
申请人： NATIONAL INSTITUTE FOR MATERIALS SCIENCE
发明人： Jie Tang , Feifei Zhang , Norio Shinya , Qian Cheng , Luchang Qin
IPC分类号： H01G11/36 , B32B7/04 , B32B9/04 , H01G11/80 , H01B1/04 , C01B31/04 , H01G11/86 , B32B9/00 , H01B1/12
CPC分类号： H01G11/36 , B32B7/045 , B32B9/007 , B32B9/04 , B32B2307/202 , B32B2313/04 , B32B2457/16 , B32B2605/00 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/194 , C01B2204/22 , H01B1/04 , H01B1/12 , H01G11/80 , H01G11/86 , Y02E60/13 , Y02T10/7022
摘要： The object of the present invention is to provide linked stacks of reduced graphene, in which excellent electrical property on the surface of graphene may be utilized, a method for producing the same, powder comprising the same, and film comprising the same. The object may be solved by using linked stacks of partly reduced graphene 11 comprising two or more stacks of partly reduced graphene 21 to 24 linked together, in which the stack of partly reduced graphene 21 has two or more sheets of partly reduced graphene 31 and a nanosubstance 32 held between the sheets of partly reduced graphene 31, the partly reduced graphene 31 has no carbonyl groups and has carboxyl groups 31a and hydroxyl groups 31b, and different stacks of partly reduced graphene 21 to 24 are linked to each other by an ester bond 34.
摘要翻译：本发明的目的是提供可以利用石墨烯表面上优异电性能的还原石墨烯的连接叠层，其制造方法，包含该石墨烯的粉末和包含它们的薄膜。该目的可以通过使用部分还原的石墨烯11的连接堆叠来解决，该组合包括连接在一起的部分还原的石墨烯21至24的两个或多个堆叠，其中部分还原的石墨烯21的堆叠具有两个或更多个部分还原的石墨烯31和保留在部分还原的石墨烯31的片之间的纳米级32，部分还原的石墨烯31没有羰基并具有羧基31a和羟基31b，并且部分还原的石墨烯21-24的不同的叠层通过酯键彼此连接 34。

79. 发明授权

US09096938B2 Graphite oxide and/or graphene preparation method 有权
标题翻译：石墨氧化物和/或石墨烯制备方法
公开(公告)号：US09096938B2
公开(公告)日：2015-08-04
申请号：US13960028
申请日：2013-08-06
申请人： NATIONAL CHIAO TUNG UNIVERSITY
发明人： Kung-Hwa Wei , Van Thanh Dang
IPC分类号： C25B1/00
CPC分类号： C25B1/00 , C01B32/192 , C01B32/23 , C25D11/026
摘要： A graphite oxide or graphene preparation method includes providing a plasma electrolytic apparatus, where an electrolytic solution is provided and a graphite electrode is configured as a cathode of the plasma electrolytic apparatus; and providing a cathodic current so as to initiate a plasma electrolytic process at the graphite cathode to obtain graphite oxide or graphene. The graphite oxide can be synthesized through plasma electrolytic processing at relatively low temperature under atmospheric pressure within a very short period of time, without the need for concentrated acids or strong oxidizing agents. The present invention may prepare graphite oxide with plasma electrolytic process directly from graphite, without requiring any prior purification. This plasma electrolytic process of the present invention is quite promising and provided with advantages such as low cost, simple setup, high efficiency, and environmental friendliness.
摘要翻译：石墨烯或石墨烯制备方法包括提供一种等离子体电解设备，其中提供电解溶液，并且石墨电极被构造为等离子体电解设备的阴极; 并提供阴极电流，以便在石墨阴极处引发等离子体电解工艺以获得石墨氧化物或石墨烯。石墨氧化物可以在非常短的时间内在大气压下在相对低的温度下通过等离子体电解处理而合成，而不需要浓缩酸或强氧化剂。本发明可以直接从石墨制备具有等离子体电解法的氧化石墨，而不需要任何预先的纯化。本发明的等离子体电解方法是非常有希望的，具有成本低，设置简单，效率高，环境友好等优点。

80. 发明授权

US09082613B2 Graphene nanoelectronic device fabrication 有权
标题翻译：石墨烯纳米电子器件制造
公开(公告)号：US09082613B2
公开(公告)日：2015-07-14
申请号：US13847433
申请日：2013-03-19
申请人： Lockheed Martin Corporation
发明人： Jonathan W. Ward , Michael J. O'Connor
IPC分类号： H01L29/16 , H01L21/02 , H01L21/311 , B82Y30/00 , B82Y40/00 , C01B31/04
CPC分类号： H01L21/02282 , B82Y30/00 , B82Y40/00 , C01B31/043 , C01B31/0446 , C01B31/0476 , C01B31/0484 , C01B32/184 , C01B32/192 , C01B32/194 , C01B32/23 , C01B2204/02 , C01B2204/04 , C01B2204/22 , H01L21/02491 , H01L21/02527 , H01L21/0262 , H01L21/02628 , H01L21/31127 , H01L29/1606
摘要： Methods for fabricating graphene nanoelectronic devices with semiconductor compatible processes, which allow wafer scale fabrication of graphene nanoelectronic devices, is provided. One method includes the steps of preparing a dispersion of functionalized graphene in a solvent; and applying a coating of said dispersion onto a substrate and evaporating the solvent to form a layer of functionalized graphene; and defunctionalizing the graphene to form a graphene layer on the substrate.
摘要翻译：提供了用于制造具有半导体兼容工艺的石墨烯纳米电子器件的方法，其允许石墨烯纳米电子器件的晶片规模制造。一种方法包括制备官能化石墨烯在溶剂中的分散体的步骤; 并将所述分散体的涂层施加到基底上并蒸发溶剂以形成功能化的石墨烯层; 并使石墨烯去官能化以在基底上形成石墨烯层。

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