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71. 发明授权

US07497968B2 Dilute solutions of lyotropic liquid crystalline polymers, methods of making same and compositions prepared from same 失效
标题翻译：溶致液晶聚合物的稀释溶液，其制备方法和由其制备的组合物
公开(公告)号：US07497968B2
公开(公告)日：2009-03-03
申请号：US11134583
申请日：2005-05-20
申请人： David Ofer , Bindu R. Nair , John D. Larouco , William A. Stevenson , Leslie S. Rubin
发明人： David Ofer , Bindu R. Nair , John D. Larouco , William A. Stevenson , Leslie S. Rubin
IPC分类号： C09K19/52 , C09K19/54 , C08J3/20 , H01M8/00
CPC分类号： C09K19/54 , C08J3/095 , C08J2379/06 , C09K19/3477 , C09K19/3497 , C09K19/3823 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1072 , H01M2300/0082 , Y02P70/56 , Y10S428/91 , Y10T428/10 , Y10T428/249958
摘要： The invention features dilute solutions of rigid rod or extended rod lyotropic liquid crystalline polymers prepared from high concentration polymerization mixtures. The invention also features methods of preparing such dilute solutions which utilize high mechanical shear to induce mix the high concentration solution with a diluent. The invention further provides articles of manufacture, including films and fibers, having a porous microstructure which are prepared from the dilute homogeneous solutions of the invention.
摘要翻译：本发明具有由高浓度聚合混合物制备的刚性棒或延伸棒溶致液晶聚合物的稀溶液。本发明还涉及制备这种稀溶液的方法，其利用高机械剪切来诱导将高浓度溶液与稀释剂混合。本发明进一步提供了包含薄膜和纤维的制品，其具有由本发明的稀释均匀溶液制备的多孔微结构。

72. 发明申请

US20060065877A1 Dilute solutions of lyotropic liquid crystalline polymers, methods of making same and compositions prepared from same 失效
公开(公告)号：US20060065877A1
公开(公告)日：2006-03-30
申请号：US11134583
申请日：2005-05-20
申请人： David Ofer , Bindu Nair , John Larouco , William Stevenson , Leslie Rubin
发明人： David Ofer , Bindu Nair , John Larouco , William Stevenson , Leslie Rubin
IPC分类号： C09K19/38 , C09K19/52 , C09K19/34 , C09K19/30
CPC分类号： C09K19/54 , C08J3/095 , C08J2379/06 , C09K19/3477 , C09K19/3497 , C09K19/3823 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1072 , H01M2300/0082 , Y02P70/56 , Y10S428/91 , Y10T428/10 , Y10T428/249958
摘要： The invention features dilute solutions of rigid rod or extended rod lyotropic liquid crystalline polymers prepared from high concentration polymerization mixtures. The invention also features methods of preparing such dilute solutions which utilize high mechanical shear to induce mix the high concentration solution with a diluent. The invention further provides articles of manufacture, including films and fibers, having a porous microstructure which are prepared from the dilute homogeneous solutions of the invention.

73. 发明授权

US06939940B2 Liquid crystalline thermosets from ester, ester-imide, and ester-amide oligomers 有权
标题翻译：来自酯，酯 - 酰亚胺和酯 - 酰胺低聚物的液晶热固性材料
公开(公告)号：US06939940B2
公开(公告)日：2005-09-06
申请号：US09757398
申请日：2001-01-05
申请人： Theodorous J. Dingemans , Erik S. Weiser , Terry L. St. Clair
发明人： Theodorous J. Dingemans , Erik S. Weiser , Terry L. St. Clair
IPC分类号： C08L101/12 , C08G63/60 , C08G63/685 , C08G69/44 , C08G73/16 , C09K19/38 , C08G73/06 , C09K19/06
CPC分类号： C09K19/3823 , C08G63/60 , C08G63/6854 , C08G69/44 , C08G73/16 , C09K19/3804
摘要： Main chain thermotropic liquid crystal esters, ester-imides, and ester-amides were prepared from AA, BB, and AB type monomeric materials and were end-capped with phenylacetylene, phenylmaleimide, or nadimide reactive end-groups. The resulting reactive end-capped liquid crystal oligomers exhibit a variety of improved and preferred physical properties. The end-capped liquid crystal oligomers are thermotropic and have, preferably, molecular weights in the range of approximately 1000-15,000 grams per mole. The end-capped liquid crystal oligomers have broad liquid crystalline melting ranges and exhibit high melt stability and very low melt viscosities at accessible temperatures. The end-capped liquid crystal oligomers are stable for up to an hour in the melt phase. These properties make the end-capped liquid crystal oligomers highly processable by a variety of melt process shape forming and blending techniques including film extrusion, fiber spinning, reactive injection molding (RIM), resin transfer molding (RTM), resin film injection (RFI), powder molding, pultrusion, injection molding, blow molding, plasma spraying and thermo-forming. Once processed and shaped, the end-capped liquid crystal oligomers were heated to further polymerize and form liquid crystalline thermosets (LCT). The fully cured products are rubbers above their glass transition temperatures. The resulting thermosets display many properties that are superior to their non-end-capped high molecular weight analogs.
摘要翻译：主链热致液晶酯，酯 - 酰亚胺和酯 - 酰胺由AA，BB和AB型单体材料制成，并用苯乙炔，苯基马来酰亚胺或纳二酰胺反应性端基封端。所得到的反应性封端的液晶低聚物表现出各种改进和优选的物理性质。封端的液晶低聚物是热致变性的，并且优选分子量在约1000-15,000克/摩尔的范围内。封端的液晶低聚物具有宽的液晶熔融范围，并且在可接近的温度下表现出高的熔体稳定性和非常低的熔体粘度。封端的液晶低聚物在熔融相中稳定长达一个小时。这些特性使得封端液晶低聚物可以通过各种熔融加工成型和共混技术加工，包括薄膜挤出，纤维纺丝，反应注射成型（RIM），树脂传递模塑（RTM），树脂薄膜注射（RFI）粉末成型，拉挤成型，注射成型，吹塑成型，等离子喷涂和热成型。一旦加工和成形，加热封端的液晶低聚物进一步聚合并形成液晶热固性塑料（LCT）。完全固化的产品是高于其玻璃化转变温度的橡胶。所得到的热固性材料显示出优于其非末端封端的高分子量类似物的许多性质。

74. 发明授权

US06841677B2 Mono-, oligo- and polydithienopyridine 失效
标题翻译：单 - ，寡 - 和聚二噻吩并吡啶
公开(公告)号：US06841677B2
公开(公告)日：2005-01-11
申请号：US10190622
申请日：2002-07-09
申请人： Martin Heeney , Steven Tierney , Marcus Thompson , Mark Giles , Louise Farrand , Maxim Shkunov , David Sparrowe , Iain McCulloch
发明人： Martin Heeney , Steven Tierney , Marcus Thompson , Mark Giles , Louise Farrand , Maxim Shkunov , David Sparrowe , Iain McCulloch
IPC分类号： H01L51/50 , C07D495/14 , C07D519/00 , C08F246/00 , C08G61/12 , C08J5/18 , C09K19/34 , C09K19/38 , H01L29/786 , H01L51/05 , H01L51/30 , H01B1/12 , C07D505/00 , C08F126/06 , C08F128/06
CPC分类号： C07D495/14 , C08F246/00 , C09K19/3491 , C09K19/3823
摘要： The invention relates to new conjugated mono-, oligo- and polydithienopyridines, their use as semiconductors or charge transport materials in optical, electrooptical or electronic devices including field effect transistors, electroluminescent, photovoltaics, sensors and electrophotographic recording devices, and to a field effect transistor as a component of integrated circuitry, as a thin fim transistor in flat panel display applications or for RFID tags, or a semiconducting component in organic light-emitting diode applications, comprising the new mono-, oligo and polydithienopyridines.
摘要翻译：本发明涉及新的共轭单 - ，寡 - 和聚 - 二烯并吡啶，它们在光学，电光或电子器件中用作半导体或电荷传输材料，包括场效应晶体管，电致发光，光伏，传感器和电子照相记录装置，以及场效应晶体管作为集成电路的组件，作为平板显示器应用中的薄型薄膜晶体管或用于RFID标签的薄型晶体管，或者在有机发光二极管应用中的半导体元件，包括新的单，低聚和多二烯并吡啶类。

75. 发明申请

US20030047719A1 Mono-, oligo- and polydithienopyridines 失效
标题翻译：单 - ，寡 - 和聚二噻吩并吡啶
公开(公告)号：US20030047719A1
公开(公告)日：2003-03-13
申请号：US10190622
申请日：2002-07-09
申请人： Merck Patent GmbH
发明人： Martin Heeney , Steven Tierney , Marcus Thompson , Mark Giles , Louise Farrand , Maxim Shkunov , David Sparrowe , Iain McCulloch
IPC分类号： H01B001/00
CPC分类号： C07D495/14 , C08F246/00 , C09K19/3491 , C09K19/3823
摘要： The invention relates to new conjugated mono-, oligo- and polydithienopyridines, their use as semiconductors or charge transport materials in optical, electrooptical or electronic devices including field effect transistors, electroluminescent, photovoltaics, sensors and electrophotographic recording devices, and to a field effect transistor as a component of integrated circuitry, as a thin fim transistor in flat panel display applications or for RFID tags, or a semiconducting component in organic light-emitting diode applications, comprising the new mono-, oligo and polydithienopyridines.
摘要翻译：本发明涉及新的共轭单 - ，寡 - 和聚 - 二烯并吡啶，它们在光学，电光或电子器件中用作半导体或电荷传输材料，包括场效应晶体管，电致发光，光伏，传感器和电子照相记录装置，以及场效应晶体管作为集成电路的组件，作为平板显示器应用中的薄型薄膜晶体管或用于RFID标签的薄型晶体管，或者在有机发光二极管应用中的半导体元件，包括新的单，低聚和多二烯并吡啶类。

76. 发明授权

US5602211A Adducts of epoxy resins and active hydrogen containing compounds containing mesogenic moieties 失效
标题翻译：环氧树脂和含有介晶部分的含活性氢化合物的加合物
公开(公告)号：US5602211A
公开(公告)日：1997-02-11
申请号：US374281
申请日：1995-01-18
申请人： Robert E. Hefner, Jr. , Jimmy D. Earls
发明人： Robert E. Hefner, Jr. , Jimmy D. Earls
IPC分类号： C08G59/14 , C08G59/02 , C08G59/18 , C08G59/20 , C08G59/28 , C08G59/30 , C09K19/38 , C08L63/00 , C08G59/06
CPC分类号： C08G59/20 , C08G59/02 , C09K19/3814 , C09K19/3823
摘要： Adducts containing mesogenic or rodlike moieties are prepared by reacting (1) at least one compound containing an average of more than one vicinal epoxide group per molecule with (2) at least one compound containing an average of more than one reactive hydrogen atom per molecule; with the proviso that at least one member of components (1) and (2) contains a mesogenic or rodlike moiety. These compounds are useful as curing agents for epoxy resins.
摘要翻译：含有介晶或棒状部分的加合物通过使（1）至少一种每分子含有多于一个邻位环氧基团的化合物与（2）至少一种每分子平均含有多于一个反应性氢原子的化合物反应而制备; 条件是组分（1）和（2）的至少一个成员含有介晶或棒状部分。这些化合物可用作环氧树脂的固化剂。

77. 发明授权

US5569727A Antistrospic polymers and method of producing them 失效
标题翻译：防雾聚合物及其制备方法
公开(公告)号：US5569727A
公开(公告)日：1996-10-29
申请号：US433344
申请日：1995-05-08
申请人： Werner Mormann , Christoph Irle
发明人： Werner Mormann , Christoph Irle
IPC分类号： C08G18/58 , C08G18/00 , C08G18/77 , C08G18/81 , C08G59/40 , C09K19/38
CPC分类号： C08G18/771 , C08G18/003 , C08G18/8125 , C09K19/3804 , C09K19/3823
摘要： The invention describes anisotropic polymers of diepoxide A having the formula (I) ##STR1## and anisotropic polymers of diisocyanate B having the formulas (II) to (VII) ##STR2## where as defined in the specification.
摘要翻译： PCT No.PCT / EP94 / 02979第 371日期1995年5月8日 102（e）日期1995年5月8日PCT 1994年9月7日PCT公布。公开号WO95 / 07308 日期：1995年3月16日本发明描述了具有式（I）的二环氧化物A和具有式（II）至（VII）的二异氰酸酯B的各向异性聚合物的各向异性聚合物。（III）其中如说明书中所定义的那样，（iii）图像（IV）<图像>（V）（VI）（VII）

78. 发明授权

US5464912A Amines from nitro group terminated mesogenic epoxy resin adducts with reduced hydroxyl group functionality 失效
标题翻译：来自硝基的胺封端的中等环氧树脂加合物具有降低的羟基官能度
公开(公告)号：US5464912A
公开(公告)日：1995-11-07
申请号：US377070
申请日：1995-01-23
申请人： Robert E. Hefner, Jr. , Jimmy D. Earls
发明人： Robert E. Hefner, Jr. , Jimmy D. Earls
IPC分类号： C08G59/14 , C08G59/20 , C08G59/22 , C08G59/28 , C09K19/38 , C08F283/00
CPC分类号： C08G59/1477 , C08G59/20 , C08G59/22 , C09K19/3814 , C09K19/3823
摘要： Adducts containing terminating nitro (nitroso) groups and one or more mesogenic moleties are prepared by reacting (A) at least one compound containing an average of more than one vicinal epoxide group per molecule with (B) at least one compound containing one or more nitro (nitroso) groups and an average of one reactive hydrogen atom per molecule; with the proviso that at least one member of components (A) and (B) contains a mesogenic moiety. Reaction of part or all of the aliphatic hydroxyl backbone groups by etherification, conversion to a halide, urethanation, oxidation to a ketone, or reduction of said ketone to an alkane, decreases the amount of hydroxyl group functionality. Reduction of these adducts provides amines which are useful as curing agents for epoxy resins.
摘要翻译：含有终止硝基（亚硝基）基团和一种或多种介晶摩尔的加合物通过使（A）至少一种含有平均每分子多个邻位环氧基团的化合物与（B）至少一种含有一个或多个硝基（亚硝基）基团，每个分子平均有一个反应性氢原子; 条件是组分（A）和（B）的至少一个成员含有介晶部分。通过醚化，转化成卤化物，氨基甲酸酯化，氧化成酮或将所述酮还原成烷烃，部分或全部脂族羟基骨架基团的反应减少羟基官能度的量。这些加合物的还原提供了可用作环氧树脂固化剂的胺。

79. 发明授权

US5463091A Diglycidyl ether of 4,4'-dihydroxy-.alpha.-methylstilbene 失效
标题翻译： 4,4'-二羟基-α-甲基芪的二缩水甘油醚
公开(公告)号：US5463091A
公开(公告)日：1995-10-31
申请号：US252811
申请日：1994-06-02
申请人： Jimmy D. Earls , Robert E. Hefner, Jr. , Paul M. Puckett
发明人： Jimmy D. Earls , Robert E. Hefner, Jr. , Paul M. Puckett
IPC分类号： C07D303/22 , C07D303/24 , C08G59/02 , C08G59/22 , C08G59/32 , C08G59/38 , C08G59/62 , C09K19/38 , C07D303/18
CPC分类号： C07D303/22 , C07D303/24 , C08G59/02 , C08G59/22 , C08G59/32 , C08G59/38 , C08G59/621 , C09K19/3814 , C09K19/3823
摘要： The diglycidyl ether of 4,4'-dihydroxy-.alpha.-methylstilbene is prepared.
摘要翻译：制备4,4'-二羟基-α-甲基芪的二缩水甘油醚。

80. 发明授权

US5344898A Oriented compositions derived from nitro group terminated mesogenic epoxy resin adducts 失效
标题翻译：衍生自硝基封端的中间环氧树脂加合物的定向组合物
公开(公告)号：US5344898A
公开(公告)日：1994-09-06
申请号：US154805
申请日：1993-11-18
申请人： Robert E. Hefner, Jr. , Jimmy D. Earls
发明人： Robert E. Hefner, Jr. , Jimmy D. Earls
IPC分类号： C08G59/14 , C08G59/20 , C08G59/22 , C08G59/28 , C09K19/38 , C08G59/50 , C08G75/32
CPC分类号： C08G59/1477 , C08G59/20 , C08G59/22 , C09K19/3814 , C09K19/3823
摘要： Adducts containing terminating nitro (nitroso) groups and one or more mesogenic moieties are prepared by reacting (A) at least one compound containing an average of more than one vicinal epoxide group per molecule with (B) at least one compound containing one or more nitro (nitroso) groups and an average of one reactive hydrogen atom per molecule; with the proviso that at least one member of components (A) and (B) contains a mesogenic moiety. Reduction of these adducts provides amines which are useful as curing agents for epoxy resins. Curable compositions comprising an epoxy resin and the adducts can be oriented before, during or prior to curing.
摘要翻译：含有末端硝基（亚硝基）基团和一个或多个介晶部分的加合物通过使（A）至少一种每分子含有多于一个邻位环氧基团的化合物与（B）至少一种含有一个或多个硝基（亚硝基）基团，每个分子平均有一个反应性氢原子; 条件是组分（A）和（B）的至少一个成员含有介晶部分。这些加合物的还原提供了可用作环氧树脂固化剂的胺。包含环氧树脂和加合物的可固化组合物可以在固化之前，期间或之前取向。

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