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1. 发明授权

US08901360B2 Process for cis 1,1,1,4,4,4-hexafluoro-2-butene 有权
标题翻译：顺式1,1,1,4,4,4-六氟-2-丁烯的方法
公开(公告)号：US08901360B2
公开(公告)日：2014-12-02
申请号：US13110979
申请日：2011-05-19
申请人： Andrew Joseph Poss , David Nalewajek , Haridasan K. Nair , Michael Van Der Puy
发明人： Andrew Joseph Poss , David Nalewajek , Haridasan K. Nair , Michael Van Der Puy
IPC分类号： C07C21/18 , C07C17/278 , C07C17/04 , C07C17/20 , C07C17/23 , C07C17/25 , C07C17/354
CPC分类号： C07C17/278 , C07C17/04 , C07C17/206 , C07C17/23 , C07C17/25 , C07C17/354 , C07C19/10 , C07C21/22 , C07C21/18
摘要： Disclosed is a process for preparing cis-1,1,1,4,4,4-hexafluorobutene comprising the steps of (a) reacting CCl4 with a compound having the formula CF3CX═CXH, where each X is independently halogen or hydrogen, to form a compound having the formula CF3CXClCXHCCl3; (b) fluorinating the compound formed in step (a) to form a compound having the formula CF3CXHCXHCF3; (c) converting the compound formed in step (b) by a reaction selected from the group consisting of dehydrohalogenation, dehalogenation and both reactions, to form a compound having the formula CF3C≡CCF3; and (d) catalytically reducing the compound formed in step (c) with hydrogen to form the compound having the formula:
摘要翻译：公开了一种制备顺式-1,1,1,4,4,4-六氟丁烯的方法，包括以下步骤：（a）使CCl4与具有式CF 3 C X = C X H的化合物反应，其中每个X独立地为卤素或氢，形成式CF3CXClCXHCCl3的化合物; （b）氟化步骤（a）中形成的化合物以形成具有式CF 3 C XHCXHCF 3的化合物; （c）通过选自脱卤化氢，脱卤和两种反应的反应转化步骤（b）中形成的化合物，以形成具有式CF 3C≡CCF3的化合物; 和（d）用氢气将步骤（c）中形成的化合物催化还原以形成具有下式的化合物：

2. 发明申请

US20100210883A1 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 有权
标题翻译：生产氟化有机化合物的方法
公开(公告)号：US20100210883A1
公开(公告)日：2010-08-19
申请号：US12702135
申请日：2010-02-08
申请人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Daniel C. Merkel , Rajesh K. Dubey , Jing Ji Ma
发明人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Daniel C. Merkel , Rajesh K. Dubey , Jing Ji Ma
IPC分类号： C07C17/23 , C07C17/357
CPC分类号： C07C17/04 , C07C17/00 , C07C17/06 , C07C17/206 , C07C17/25 , C07C17/26 , C07C17/269 , C07C17/272 , C07C17/278 , C07C21/18 , C07C19/08 , C07C19/10
摘要： Disclosed are methods for producing fluorinated organic compounds, including hydrofluoropropenes, which preferably comprises converting at least one compound of formula (I): CF3CHXCH2X (I) to at least one compound of formula (II) CF3CZCHZ (II). where X is independently Cl, Br, I or F, and Z independently is H or F. In certain preferred embodiments, each Z is different.
摘要翻译：公开了生产氟化有机化合物的方法，包括氢氟丙烯，其优选包括将至少一种式（I）化合物：CF 3 CHXCH 2 X（I）转化为至少一种式（II）CF 3 CZCHZ（II）化合物。其中X独立地为Cl，Br，I或F，Z独立地为H或F.在某些优选实施方案中，每个Z不同。

3. 发明申请

US20080312392A1 PROCESS FOR PREPARING A POLYMER FROM ALLYLOXYTRIFLUOROPROPENES 审中-公开
标题翻译：从聚乙烯吡咯烷酮制备聚合物的方法
公开(公告)号：US20080312392A1
公开(公告)日：2008-12-18
申请号：US12196721
申请日：2008-08-22
申请人： HARIDASAN K. NAIR , Rajiv R. Singh , Gregory J. Shafer
发明人： HARIDASAN K. NAIR , Rajiv R. Singh , Gregory J. Shafer
IPC分类号： C08F4/42 , C08F16/12
CPC分类号： C08F14/18 , C07C41/06 , C08F2/00 , C07C43/17
摘要： A process for preparing a polymer comprising the step of: polymerizing: (i) an allyloxytrifluoropropene derivative selected from the group consisting of compounds represented by the formula: CF3CH═CH(OCH2CR═CH2); CF3CH═C(OCH2CR═CH2)2; CF3CH═CF(OCH2CR═CH2); and any mixtures thereof; wherein R is selected from the group consisting of: hydrogen and methyl; and optionally (ii) an ethylenically unsaturated comonomer; wherein the copolymerizing step is carried out in the presence of a catalyst, under conditions sufficient to produce the copolymer.
摘要翻译：一种制备聚合物的方法，包括以下步骤：聚合：（i）选自由下式表示的化合物的烯丙氧基三氟丙烯衍生物：<？in-line-formula description =“In-line Formulas”end =“lead “> CF 3 CH-CH（OCH 2 CR-CH 2）; <？在线公式描述=”在线公式“end =”tail“？> <？in-line-formula description =”In-line Formulas“end =“lead”→CF 3 CH-C（OCH 2 CR-CH 2）2; <βin-line-formula description =“In-line Formulas”end =“tail”？> <？in-line-formula description = CF 3 CH-CF（OCH 2 CR-CH 2）; 和<？in-line-formula description =“In-line Formulas”end =“tail”？>它们的任何混合物; 其中R选自：氢和甲基; 和任选的（ⅱ）烯属不饱和共聚单体; 其中所述共聚步骤在催化剂存在下，在足以产生所述共聚物的条件下进行。

4. 发明申请

US20080242901A1 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 有权
标题翻译：生产氟化有机化合物的方法
公开(公告)号：US20080242901A1
公开(公告)日：2008-10-02
申请号：US12134629
申请日：2008-06-06
申请人： Sudip Mukhopadhyay , Hsueh Sung Tung , Haridasan K. Nair , Jingji Ma
发明人： Sudip Mukhopadhyay , Hsueh Sung Tung , Haridasan K. Nair , Jingji Ma
IPC分类号： C07C17/00
CPC分类号： B01J27/125 , B01J27/10 , B01J27/12 , C07C17/00 , C07C17/278 , C07C21/18 , C07C19/08
摘要： A method for preparing fluorinated organic compounds wherein at least one fluorinated olefin is reacted with methyl fluoride in the gas-phase and in the presence of a Lewis Acid catalyst to form at least one product having at least 3 carbon atoms.
摘要翻译：一种制备氟化有机化合物的方法，其中至少一种氟化烯烃在气相和路易斯酸催化剂存在下与甲基氟反应形成至少一种具有至少3个碳原子的产物。

5. 发明授权

US06551469B1 Photochlorination of 1,1,1,3,3-pentafluoropropane 有权
标题翻译： 1,1,1,3,3-五氟丙烷的光氯化
公开(公告)号：US06551469B1
公开(公告)日：2003-04-22
申请号：US09994438
申请日：2001-11-27
申请人： Haridasan K. Nair , Michael Van Der Puy , David Nalewajek , Timothy R. Demmin , Andrew J. Poss , David E. Bradley , Ian R. Shankland , Martin E. Cheney
发明人： Haridasan K. Nair , Michael Van Der Puy , David Nalewajek , Timothy R. Demmin , Andrew J. Poss , David E. Bradley , Ian R. Shankland , Martin E. Cheney
IPC分类号： C07C1700
CPC分类号： C07C17/10 , C07C19/10
摘要： A process for preparing 1-chloro-1,1,3,3,3-pentafluoropropane, CF3CH2CF2Cl, comprising contacting in a reaction zone in the substantial absence of oxygen, reactants comprising chlorine and 1,1,1,3,3-pentafluoropropane, CF3CH2CHF2 (also referred to as HFC-245fa), and subjecting the reactants to actinic radiation, such as UV light at about 2,000 to 4,000 Angstroms, wherein: (1) inert gas is present at a concentration equal to or less than about 5 wt. % of the total weight of reactants; (2) the molar ratio of chlorine to CF3CH2CHF2 is from about 0.2:1 to about 1.5:1; and (3) the concentration of chlorinated product produced having greater than one chlorine present in the molecule is less than or equal to about 10 wt. %.
摘要翻译：制备1-氯-1,1,3,3,3-五氟丙烷CF 3 CH 2 CF 2 Cl的方法，包括在基本不存在氧的反应区中接触，包含氯的反应物和1,1,1,3,3-五氟丙烷，CF 3 CH 2 CHF 2（也称为HFC-245fa），并使反应物进行光化辐射，例如约2,000至4,000埃的紫外光，其中：（1）惰性气体的存在浓度等于或小于约5 重量反应物总重量的百分比; （2）氯与CF 3 CH 2 CHF 2的摩尔比为约0.2:1至约1.5:1; 和（3）分子中存在的具有大于一个氯的氯化产物的浓度小于或等于约10wt。％。

6. 发明授权

US06466730B2 Radiation curable fluorinated vinyl ethers derived from hexafluoropene 失效
标题翻译：衍生自六氟丙烯的可辐射固化氟化乙烯基醚
公开(公告)号：US06466730B2
公开(公告)日：2002-10-15
申请号：US09919015
申请日：2001-07-31
申请人： Haridasan K. Nair , David Nalewajek , David E. Bradley
发明人： Haridasan K. Nair , David Nalewajek , David E. Bradley
IPC分类号： G02B600
CPC分类号： C07C43/17 , C07C43/172 , C07C43/176 , C07C2601/14 , C08F16/26 , C09D11/101 , G02B6/1221 , G02B6/13
摘要： Vinyl ether compounds having the formula: R—O—X—O—CH═CH2 wherein R is a radical having the formula: R1—CFH—CF2— or R1—CF═CF2—, wherein R1 is an unsubstituted or substituted aliphatic radical, an unsubstituted or substituted cyclic aliphatic radical, an unsubstituted or substituted aromatic radical, an unsubstituted or substituted araliphatic radical, or an unsubstituted or substituted heterocyclic radical, and X is an unsubstituted or substituted aliphatic radical, an un-substituted or substituted cyclic aliphatic radical, an unsubstituted or substituted aromatic radical, an unsubstituted or substituted araliphatic radical, or an unsubstituted or substituted heterocyclic radical. Curable compositions containing the vinyl ether compounds and methods in which substrate coating layers of the vinyl ether compositions are cured, particularly on optical devices, are also disclosed, as well as polymers polymerized from the vinyl ether compounds.
摘要翻译：具有下式的乙烯基醚化合物：其中R是具有下式的基团：R1-CFH-CF2-或R1-CF = CF2-，其中R1是未取代或取代的脂族基团，未取代或取代的环状脂族基团，未取代的或取代的芳族基团，未取代或取代的芳脂族基团，或未取代或取代的杂环基，X是未取代或取代的脂族基团，未取代或取代的环状脂族基团，未取代或取代的芳族基团，未取代或取代的芳族基团，取代的芳脂族基团，或未取代或取代的杂环基团。还公开了包含乙烯基醚化合物的可固化组合物和其中乙烯基醚组合物的基底涂层被固化的方法，特别是在光学器件上，以及由乙烯基醚化合物聚合的聚合物。

7. 发明授权

US5661138A (o-Acyl-p-N-acylamino-phenyl)-O-phosphoethanolamines 失效
标题翻译：（邻 - 酰基对-N-酰基氨基 - 苯基）-O-磷酸乙醇胺
公开(公告)号：US5661138A
公开(公告)日：1997-08-26
申请号：US726059
申请日：1996-10-03
申请人： Andrew C. Peterson , Rudolf Franzmair , Haridasan K. Nair
发明人： Andrew C. Peterson , Rudolf Franzmair , Haridasan K. Nair
IPC分类号： A61K31/685 , A61K31/167 , A61K31/216 , A61P29/00 , C07C233/31 , C07C233/33 , C07F9/02 , C07F9/12 , C07F9/10
CPC分类号： C07C233/31 , C07F9/12
摘要： Novel (o-acyl-p-N-acylamino-phenyl)-O-phosphoethanolamines and pharmaceutically acceptable salts thereof having anti-inflammatory activity, and pharmaceutical compositions containing same are disclosed. Certain novel intermediates are also disclosed.
摘要翻译：公开了具有抗炎活性的新型（邻酰基对N-酰基氨基 - 苯基）-O-磷酸乙醇胺及其药学上可接受的盐，以及含有它们的药物组合物。还公开了某些新颖的中间体。

8. 发明授权

US08404907B2 Process for cis-1-chloro-3,3,3-trifluoropropene 有权
标题翻译：顺式-1-氯-3,3,3-三氟丙烯的方法
公开(公告)号：US08404907B2
公开(公告)日：2013-03-26
申请号：US13030789
申请日：2011-02-18
申请人： Haridasan K. Nair , Andrew Joseph Poss , Rajiv Ratna Singh , Michael Van Der Puy , Ryan J. Hulse
发明人： Haridasan K. Nair , Andrew Joseph Poss , Rajiv Ratna Singh , Michael Van Der Puy , Ryan J. Hulse
IPC分类号： C07C21/00 , C07C17/00 , C07C19/08 , C07C21/18 , C07C23/00 , C07C25/13
CPC分类号： C07C17/25 , C07B2200/09 , C07C17/354 , C07C21/22 , C07C21/18
摘要： Disclosed is a process for making one isomer of CF3CH═CHCl. More particularly, the invention comprises the production of CF3C≡CCl and its selective reduction to cis-1-chloro-3,3,3-trifluoropropene (CF3CH═CHCl).
摘要翻译：公开了制备CF 3 CH = CHCl的一种异构体的方法。更具体地说，本发明包括生产CF 3C≡CCl及其对顺式-1-氯-3,3,3-三氟丙烯（CF 3 CH = CHCl）的选择性还原。

9. 发明授权

US08395000B2 Method for producing fluorinated organic compounds 有权
标题翻译：氟化有机化合物的制备方法
公开(公告)号：US08395000B2
公开(公告)日：2013-03-12
申请号：US12702135
申请日：2010-02-08
申请人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Daniel C. Merkel , Rajesh K. Dubey , Jing Ji Ma
发明人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Daniel C. Merkel , Rajesh K. Dubey , Jing Ji Ma
IPC分类号： C07C17/25 , C07C21/185 , C07C21/18
CPC分类号： C07C17/04 , C07C17/00 , C07C17/06 , C07C17/206 , C07C17/25 , C07C17/26 , C07C17/269 , C07C17/272 , C07C17/278 , C07C21/18 , C07C19/08 , C07C19/10
摘要： Disclosed are methods for producing fluorinated organic compounds, including hydrofluoropropenes, which preferably comprises converting at least one compound of formula (I): CF3CHXCH2X (I) to at least one compound of formula (II) CF3CZCHZ (II). where X is independently Cl, Br, I or F, and Z independently is H or F. In certain preferred embodiments, each Z is different.
摘要翻译：公开了生产氟化有机化合物的方法，包括氢氟丙烯，其优选包括将至少一种式（I）化合物：CF 3 CHXCH 2 X（I）转化为至少一种式（II）CF 3 CZCHZ（II）化合物。其中X独立地为Cl，Br，I或F，Z独立地为H或F.在某些优选实施方案中，每个Z不同。

10. 发明申请

US20110288350A1 PROCESS FOR THE PREPARATION OF FLUORINATED CIS-ALKENE 有权
标题翻译：制备氟化苯乙烯的方法
公开(公告)号：US20110288350A1
公开(公告)日：2011-11-24
申请号：US13110998
申请日：2011-05-19
申请人： Andrew Joseph Poss , Michael Van Der Puy , Rajiv Ratna Singh , David Nalewajek , Haridasan K. Nair
发明人： Andrew Joseph Poss , Michael Van Der Puy , Rajiv Ratna Singh , David Nalewajek , Haridasan K. Nair
IPC分类号： C07C17/281
CPC分类号： C07C17/23 , C07B2200/09 , C07C17/10 , C07C17/206 , C07C17/278 , C07C21/18 , C07C19/10
摘要： Disclosed is a process for the preparation of fluorine-containing olefins comprising contacting a chlorofluoroalkane with hydrogen in the presence of a catalyst at a temperature sufficient to cause replacement of the chlorine substituents of the chlorofluoroalkane with hydrogen to produce a fluorine-containing olefin. Also disclosed are catalyst compositions for the hydrodechlorination of chlorofluoroalkanes comprising copper metal deposited on a support, and comprising palladium deposited on calcium fluoride, poisoned with lead and reducing the in the presence or absence of a dehydrochlorination catalyst under conditions effective to form a product stream comprising cis-1,1,1,4,4,4-hexafluoro-2-butene (HFO-1336).
摘要翻译：公开了一种制备含氟烯烃的方法，包括在催化剂存在下，使氯氟烷烃与氢气在足以使氯氟烷烃的氯取代基被氢取代以产生含氟烯烃的温度下接触。还公开了用于加氢脱氯氯氟烷烃的催化剂组合物，其包含沉积在载体上的铜金属，并且包含沉积在氟化钙上的钯，由铅中毒并在有效形成产物流的条件下在脱氯化氢催化剂存在或不存在下还原，包含顺式-1,1,1,4,4,4-六氟-2-丁烯（HFO-1336）。

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