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1. 发明授权

US09902670B2 Production method for composition containing 1,2-dichloro-3,3,3-trifluoropropene (HCFO-1223xd) and/or 1,1,2-trichloro-3,3,3-trifluoropropene (CFO-1213xa) 有权
公开(公告)号：US09902670B2
公开(公告)日：2018-02-27
申请号：US15307956
申请日：2015-05-14
申请人： DAIKIN INDUSTRIES, LTD.
发明人： Daisuke Karube , Shun Ohkubo , Tatsuya Takakuwa
IPC分类号： C07C17/06 , C07C21/18 , C07C17/25 , C07C17/15 , C07C19/10 , C07B61/00 , C07C17/383
CPC分类号： C07C17/06 , C07B61/00 , C07C17/15 , C07C17/25 , C07C17/383 , C07C19/10 , C07C21/18 , Y02P20/582
摘要： The present invention provides a method that produces a composition containing 1223xd and/or 1213xa by a gas-phase reaction, and that achieves production efficiency higher than known methods. The present invention provides a method for producing a composition containing at least one fluorine-containing olefin selected from 1,2-dichloro-3,3,3-trifluoropropene (HCFO-1223xd) and 1,1,2-trichloro-3,3,3-trifluoropropene (CFO-1213xa), the method comprising subjecting at least one starting compound selected from a chlorine-containing alkane represented by Formula (1-1): CF3CHXCHX2, wherein each X is independently H or Cl, with the proviso that at least one X represents Cl, and a chlorine-containing alkene represented by Formula (1-2): CF3CX═CX2, wherein each X is independently H or Cl, with the proviso that at least one X represents Cl, to a gas-phase oxychlorination reaction in a temperature range of 380° C. or lower in the presence of oxidative gas and hydrogen chloride gas.

2. 发明申请

US20170057891A1 PRODUCTION METHOD FOR COMPOSITION CONTAINING 1,2-DICHLORO-3,3,3-TRIFLUOROPROPENE (HCFO-1223xd) AND/OR 1,1,2-TRICHLORO-3,3,3-TRIFLUOROPROPENE (CFO-1213xa) 有权
标题翻译：含有1,2-二氯-3,3,3-三氟丙烯（HCFO-1223xd）和/或1,1,2-三氯-3,3,3-三氟丙烯（CFO-1213xa）的组合物的制备方法
公开(公告)号：US20170057891A1
公开(公告)日：2017-03-02
申请号：US15307956
申请日：2015-05-14
申请人： DAIKIN INDUSTRIES, LTD.
发明人： Daisuke KARUBE , Shun OHKUBO , Tatsuya TAKAKUWA
IPC分类号： C07C17/06 , C07C17/383
CPC分类号： C07C17/06 , C07B61/00 , C07C17/15 , C07C17/25 , C07C17/383 , C07C19/10 , C07C21/18 , Y02P20/582
摘要： The present invention provides a method that produces a composition containing 1223xd and/or 1213xa by a gas-phase reaction, and that achieves production efficiency higher than known methods. The present invention provides a method for producing a composition containing at least one fluorine-containing olefin selected from 1,2-dichloro-3,3,3-trifluoropropene (HCFO-1223xd) and 1,1,2-trichloro-3,3,3-trifluoropropene (CFO-1213xa), the method comprising subjecting at least one starting compound selected from a chlorine-containing alkane represented by Formula (1-1): CF3CHXCHX2, wherein each X is independently H or Cl, with the proviso that at least one X represents Cl, and a chlorine-containing alkene represented by Formula (1-2): CF3CX═CX2, wherein each X is independently H or Cl, with the proviso that at least one X represents Cl, to a gas-phase oxychlorination reaction in a temperature range of 380° C. or lower in the presence of oxidative gas and hydrogen chloride gas.
摘要翻译：本发明提供了一种通过气相反应产生含有1223xd和/或1213xa的组合物的方法，其实现了比已知方法更高的生产效率。本发明提供一种制备含有至少一种选自1,2-二氯-3,3,3-三氟丙烯（HCFO-1223xd）和1,1,2-三氯-3,3,3-三氟丙烯的含氟烯烃的组合物的方法，3-三氟丙烯（CFO-1213xa），该方法包括使至少一种选自式（1-1）表示的含氯烷烃的起始化合物：CF 3 CHXCHX 2，其中每个X独立地为H或Cl，条件是至少一个X表示Cl，和由式（1-2）表示的含氯烯烃：CF 3 C X = C X 2，其中每个X独立地为H或Cl，条件是至少一个X表示Cl，在氧化性气体和氯化氢气体存在下，在380℃以下的温度范围内进行三相氧氯化反应。

3. 发明申请

US20170029361A1 HALOGENATED ANILINE AND METHOD FOR PRODUCING SAME 审中-公开
标题翻译：氢化苯胺及其生产方法
公开(公告)号：US20170029361A1
公开(公告)日：2017-02-02
申请号：US15293507
申请日：2016-10-14
申请人： Nippon Soda Co., Ltd.
发明人： Hiroki Inoue , Yuzuru Sakata , Shinichi Kobayashi , Yoshikazu Ito , Takashi Kitayama
IPC分类号： C07C205/12 , C07C17/06 , C07C201/08
CPC分类号： C07C209/74 , C07C17/00 , C07C17/06 , C07C17/12 , C07C201/08 , C07C201/14 , C07C205/12 , C07C209/32 , C07C211/52 , C07C25/13
摘要： The present invention provides a halogenated aniline represented by formula (I) (wherein each of X1 and X2 independently represents a chlorine atom, a bromine atom or an iodine atom), a method for producing the halogenated aniline, and other aspects.
摘要翻译：本发明提供由式（I）表示的卤代苯胺（其中，X 1和X 2各自独立地表示氯原子，溴原子或碘原子），卤代苯胺的制造方法等。

4. 发明授权

US08912368B2 Method for producing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf) 有权
标题翻译： 2-氯-3,3,3-三氟丙烯（HCFC-1233xf）的制备方法
公开(公告)号：US08912368B2
公开(公告)日：2014-12-16
申请号：US13742792
申请日：2013-01-16
申请人： Honeywell International Inc.
发明人： Daniel C. Merkel , Hsueh S. Tung
IPC分类号： C07C19/08 , C07C17/42 , C07C21/18 , C07C17/20 , C07C17/25
CPC分类号： C07C17/206 , C07C17/06 , C07C17/087 , C07C17/20 , C07C17/25 , C07C17/42 , C07C21/18
摘要： The present invention relates to an improved method for manufacturing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf) by reacting 1,1,2,3-tetrachloropropene, 1,1,1,2,3-pentachloropropane, and/or 2,3,3,3-tetrachloropropene with hydrogen fluoride, in a vapor phase reaction vessel in the presence of a vapor phase fluorination catalyst and stabilizer. HCFC-1233xf is an intermediate in the production of 2,3,3,3-tetrafluoropropene (HFO-1234yf) which is a refrigerant with low global warming potential.
摘要翻译：本发明涉及一种通过使1,1,2,3-四氯丙烯，1,1,1,2,3-五氯丙烷与1,1,3,3-四氯丙烯反应制备2-氯-3,3,3-三氟丙烯（HCFC-1233xf）的改进方法，和/或2,3,3,3-四氯丙烯与氟化氢在气相反应容器中在气相氟化催化剂和稳定剂存在下反应。 HCFC-1233xf是生产2,3,3,3-四氟丙烯（HFO-1234yf）的中间体，它是具有低全球变暖潜能的制冷剂。

5. 发明申请

US20130197282A1 METHOD FOR PRODUCING 2-CHLORO-3,3,3,-TRIFLUOROPROPENE (HCFC-1233xf) 有权
公开(公告)号：US20130197282A1
公开(公告)日：2013-08-01
申请号：US13742792
申请日：2013-01-16
申请人： HONEYWELL INTERNATIONAL INC.
发明人： Daniel C. Markel , Hsueh S. Tung
IPC分类号： C07C17/20
CPC分类号： C07C17/206 , C07C17/06 , C07C17/087 , C07C17/20 , C07C17/25 , C07C17/42 , C07C21/18
摘要： The present invention relates to an improved method for manufacturing 2-chloro-3,3,3,-trifluoropropene (HCFC-1233xf) by reacting 1,1,2,3-tetrachloropropene, 1,1,1,2,3-pentachloropropane, and/or 2,3,3,3-tetrachloropropene with hydrogen fluoride, in a vapor phase reaction vessel in the presence of a vapor phase fluorination catalyst and stabilizer. HCFC-1233xf is an intermediate in the production of 2,3,3,3-tetrafluoropropene (HFO-1234yf) which is a refrigerant with low global warming potential.

6. 发明申请

US20110218370A1 PROCESS FOR THE MANUFACTURE OF HYDROCHLOROFLUOROOLEFINS 有权
标题翻译：氢氯酚制备方法
公开(公告)号：US20110218370A1
公开(公告)日：2011-09-08
申请号：US13127817
申请日：2009-11-12
申请人： Maher Y. Elsheikh , Philippe Bonnet , John A. Wismer
发明人： Maher Y. Elsheikh , Philippe Bonnet , John A. Wismer
IPC分类号： C07C17/358 , C07C17/38
CPC分类号： C07C21/18 , C07C17/06 , C07C17/10 , C07C17/206 , C07C17/25 , C07C17/358 , C07C17/383
摘要： The present invention provides a process for the manufacture of trans 1-chloro-3,3,3-trifluoropropene (E-1233zd). The first step of the process comprises the fluorination of 1,1,3,3-tetrachlororopropene (1230za, CCh═CH—CHCh) and/or 1,1,1,3,3-pentaachloropropane (240fa) to a mixture of cis 1233zd (Z-1233zd) and trans 1233zd (E-1233zd). The second step of the process comprises a separation of the mixture formed in the first step to isolate cis 1233zd (Z-1233zd) from the mixture. The third step of the process comprises isomerization of cis 1233zd (Z-1233zd) to trans 1233zd (E-1233zd).
摘要翻译：本发明提供了制备反式1-氯-3,3,3-三氟丙烯（E-1233zd）的方法。该方法的第一步包括将1,1,3,3-四氯丙烯（1230za，CCh = CH-CHCH）和/或1,1,1,3,3-五氯丙烷（240fa）氟化为顺式 1233zd（Z-1233zd）和反式1233zd（E-1233zd）。该方法的第二步包括将第一步中形成的混合物分离以从混合物中分离顺式1233zd（Z-1233zd）。该方法的第三步包括顺式1233zd（Z-1233zd）异构化为反式1233zd（E-1233zd）。

7. 发明申请

US20100099930A1 Continuous Process for Converting Natural Gas to Liquid Hydrocarbons 有权
标题翻译：将天然气转化为液态碳氢化合物的连续工艺
公开(公告)号：US20100099930A1
公开(公告)日：2010-04-22
申请号：US12504894
申请日：2009-07-17
申请人： Peter Stoimenov , Charles Ian Cutier , Jihong Cheng , Charles J. Coronelia , Krishna Janmanchi , Zachary J.A. Komon , Saydul Amin Sardar , Vivek Julka , Sagar Gadewar , Philip Grosso , Daniel J. Auerbach , Jean Wheeler
发明人： Peter Stoimenov , Charles Ian Cutier , Jihong Cheng , Charles J. Coronelia , Krishna Janmanchi , Zachary J.A. Komon , Saydul Amin Sardar , Vivek Julka , Sagar Gadewar , Philip Grosso , Daniel J. Auerbach , Jean Wheeler
IPC分类号： C07C1/00 , C01B7/00 , B01J8/04 , B01J8/18 , C07C17/00
CPC分类号： B01J8/00 , B01J8/18 , C01B7/01 , C01B7/093 , C01B7/096 , C01B7/13 , C01B7/19 , C07C17/06 , C07C17/10 , C07C17/23 , C07C17/26 , Y02C20/30 , C07C19/075 , C07C25/02
摘要： A method comprising: providing an alkyl halide stream; contacting at least some of the alkyl halides with a coupling catalyst to form a product stream comprising higher hydrocarbons and hydrogen halide; contacting the product stream with a solid reactant to remove at least a portion of the hydrogen halide from the product stream; and reacting the solid reactant with a source of oxygen to generate a corresponding halogen.
摘要翻译：一种方法，包括：提供烷基卤流; 使至少一些烷基卤与偶联催化剂接触以形成包含高级烃和卤化氢的产物流; 使产物流与固体反应物接触以从产物流中除去至少一部分卤化氢; 并使固体反应物与氧源反应以产生相应的卤素。

8. 发明授权

US5714655A Process of manufacturing 1,1,1,3,3-pentafluoropropane, process of manufacturing 2,2,3-trichloro 1,1,1,3,3-pentafluoropropane and process of manufacturing 2,3,3-trichloro-1,1,1-trifluoropropene 失效
标题翻译：制备1,1,1,3,3-五氟丙烷的方法，制备2,2,3-三氯1,1,1,3,3-五氟丙烷的方法和制备2,3,3-三氯-1,1- 1,1-三氟丙烯
公开(公告)号：US5714655A
公开(公告)日：1998-02-03
申请号：US549815
申请日：1995-12-08
申请人： Akinori Yamamoto , Eiji Seki , Hirokazu Aoyama , Seiji Takubo , Tatsuo Nakada
发明人： Akinori Yamamoto , Eiji Seki , Hirokazu Aoyama , Seiji Takubo , Tatsuo Nakada
IPC分类号： B01J23/44 , C07C17/06 , C07C17/10 , C07C17/20 , C07C17/21 , C07C17/23 , C07C19/08 , C07C17/087
CPC分类号： C07C19/08 , B01J23/44 , C07C17/06 , C07C17/10 , C07C17/206 , C07C17/21 , C07C17/23
摘要： 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane is used as a raw material, to which not less than 4.5 equivalent parts of hydrogen are added to effect a hydrogenation reaction in the presence of a noble metal catalyst, particularly a palladium catalyst, by the vapor phase method to manufacture 1,1,1,3,3-pentafluoropropane. Further, propane, propene, and hexachloropropene, etc. are chlorofluorinated in the presence of a metal catalyst to produce 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane, then this compound is reduced with hydrogen in the presence of a noble metal catalyst to produce 1,1,1,3,3-pentafluoropropane. 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane and 1,1,1,3,3-pentafluoropropane can thus be efficiently and economically produced.
摘要翻译： PCT No.PCT / JP94 / 00867 Sec。 371 1995年12月8日第 102（e）日期1995年12月8日PCT 1994年5月30日PCT PCT。出版物WO94 / 29252 日本1992年12月22日2,2,3-三氯-1,1,1,3,3-五氟丙烷作为原料，向其中加入不少于4.5当量氢的氢化反应存在贵金属催化剂，特别是钯催化剂，通过气相法制造1,1,1,3,3-五氟丙烷。此外，丙烷，丙烯和六氯丙烯等在金属催化剂的存在下被氯氟化，得到2,2,3-三氯-1,1,1,3,3-五氟丙烷，然后将该化合物用氢气还原存在贵金属催化剂以制备1,1,1,3,3-五氟丙烷。因此可以有效且经济地制备2,2,3-三氯-1,1,1,3,3-五氟丙烷和1,1,1,3,3-五氟丙烷。

9. 发明授权

US5674949A Liquid-phase fluorination 失效
标题翻译：液相氟化
公开(公告)号：US5674949A
公开(公告)日：1997-10-07
申请号：US466798
申请日：1995-06-06
申请人： Thomas R. Bierschenk , Timothy Juhlke , Hajimu Kawa , Richard J. Lagow
发明人： Thomas R. Bierschenk , Timothy Juhlke , Hajimu Kawa , Richard J. Lagow
IPC分类号： C07B39/00 , C07C17/02 , C07C17/06 , C07C17/12 , C07C31/40 , C07C41/22 , C07C41/48 , C07C43/12 , C07C43/313 , C07C43/315 , C07C43/32 , C07C45/54 , C07C49/167 , C07C67/307 , C07C209/74 , C07C211/15 , C08G65/00 , C08G65/323 , C08G65/337 , C07C17/04 , C07C19/00
CPC分类号： C08G65/337 , C07B39/00 , C07C17/02 , C07C17/06 , C07C17/12 , C07C209/74 , C07C211/15 , C07C31/40 , C07C41/22 , C07C41/48 , C07C41/60 , C07C45/54 , C07C49/167 , C07C67/307 , C08G65/00 , C08G65/007 , C08G65/3236 , C07C2101/14 , C07C2103/26
摘要： This invention pertains to a method for liquid-phase fluorination for perfluorination of a wide variety of hydrogen-containing compounds.
摘要翻译：本发明涉及用于各种含氢化合物的全氟化的液相氟化方法。

10. 发明授权

US5461117A Liquid phase fluorination 失效
公开(公告)号：US5461117A
公开(公告)日：1995-10-24
申请号：US258708
申请日：1994-06-13
申请人： Thomas R. Bierschenk , Timothy J. Juhlke , Hajimu Kawa , Richard J. Lagow
发明人： Thomas R. Bierschenk , Timothy J. Juhlke , Hajimu Kawa , Richard J. Lagow
IPC分类号： C07B39/00 , C07C17/02 , C07C17/06 , C07C17/12 , C07C29/62 , C07C31/40 , C07C41/22 , C07C41/48 , C07C43/12 , C07C43/313 , C07C43/315 , C07C43/32 , C07C45/54 , C07C49/167 , C07C67/307 , C07C209/74 , C07C211/15 , C08G65/00 , C08G65/323 , C08G65/337 , C07C19/00
CPC分类号： C08G65/337 , C07B39/00 , C07C17/02 , C07C17/06 , C07C17/12 , C07C209/74 , C07C211/15 , C07C29/62 , C07C31/40 , C07C41/22 , C07C41/26 , C07C41/48 , C07C41/60 , C07C45/54 , C07C49/167 , C07C67/307 , C08G65/00 , C08G65/007 , C08G65/3236 , C07C2101/14 , C07C2103/26
摘要： This invention pertains to a method for liquid phase fluorination for perfluorination of a wide variety of hydrogen-containing compounds.

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