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1. 发明授权

US08580978B2 Process for preparing a hydroxyacid or hydroxyester 有权
标题翻译：制备羟基酸或羟基酯的方法
公开(公告)号：US08580978B2
公开(公告)日：2013-11-12
申请号：US12851468
申请日：2010-08-05
申请人： Rene Johan Haan , Jean-Paul Lange
发明人： Rene Johan Haan , Jean-Paul Lange
IPC分类号： C07D307/00
CPC分类号： C07C51/377 , C07C67/03 , C07D307/33 , Y02P20/127 , C07C59/01 , C07C69/533
摘要： A process for preparing a hydroxyacid or hydroxyester from a reactant selected from (a) a carboxylic acid having an aldehyde or keto group; and (b) an ester of a carboxylic acid having an aldehyde or keto group; by contacting the reactant with a metal catalyst in the presence of hydrogen, wherein the metal catalyst is supported on a titanium dioxide or zirconium dioxide support.
摘要翻译：从选自（a）具有醛或酮基的羧酸的反应物制备羟基酸或羟基酯的方法; 和（b）具有醛或酮基的羧酸酯; 通过在氢的存在下使反应物与金属催化剂接触，其中金属催化剂负载在二氧化钛或二氧化锆载体上。

2. 发明授权

US08003818B2 Process for the hydrogenation of a lactone or of a carboxylic acid or an ester having a gamma-carbonyl group 有权
标题翻译：内酯或具有γ-羰基的羧酸或酯的氢化方法
公开(公告)号：US08003818B2
公开(公告)日：2011-08-23
申请号：US11314404
申请日：2005-12-21
申请人： Peter John Van Den Brink , Klaas Lambertus Von Hebel , Jean-Paul Lange , Leonardus Petrus
发明人： Peter John Van Den Brink , Klaas Lambertus Von Hebel , Jean-Paul Lange , Leonardus Petrus
IPC分类号： C07C69/34 , C07C69/52
CPC分类号： C07C51/377 , C07C53/126
摘要： The invention provides a process for the hydrogenation of a reactant selected from the group consisting of: at the ring-closing carbon atom and has a proton at a (a) a 5- or 6-membered lactone that is substituted carbon atom adjacent to the ring-closing carbon atom; (b) an ester of a carboxylic acid having a gamma-carbonyl group and a proton at a carbon atom adjacent to the carbon atom of the carbonyl group; and (c) a carboxylic acid having a gamma-carbonyl group and a proton at a carbon atom adjacent to the carbon atom of the carbonyl group, wherein the reactant is contacted with a strongly acidic heterogeneous catalyst comprising a hydrogenating metal, in the presence of hydrogen, at a temperature in the range of from 100 to 350° C. and a pressure in the range of from 1 to 150 bar (absolute). The invention further provides a fuel composition, preferably a diesel composition, comprising di-alkyl 4-methylnonanedioate or di-alkyl 3-ethyl-4-methylheptanedioate.
摘要翻译：本发明提供了一种用于氢化反应物的方法，所述反应物选自：在闭环碳原子处，并且在（a）5-或6-元内酯上具有质子，该内酯是与闭环碳原子; （b）在与羰基的碳原子相邻的碳原子处具有γ-羰基和质子的羧酸的酯; 和（c）在与羰基的碳原子相邻的碳原子处具有γ-羰基和质子的羧酸，其中反应物与包含氢化金属的强酸性多相催化剂在存在下，氢气，温度范围为100至350℃，压力范围为1至150巴（绝对）。本发明还提供一种燃料组合物，优选含有4-甲基壬二酸二烷基酯或3-乙基-4-甲基庚二酸二烷基酯的柴油组合物。

3. 发明申请

US20110112326A1 PROCESS FOR HYDROGENATION 审中-公开
标题翻译：加氢方法
公开(公告)号：US20110112326A1
公开(公告)日：2011-05-12
申请号：US12851462
申请日：2010-08-05
申请人： Jean-Paul Lange
发明人： Jean-Paul Lange
IPC分类号： C07C51/09
CPC分类号： C07C51/377 , C07C53/126
摘要： A process for the hydrogenation of a reactant selected from: (a) a 5- or 6-membered lactone that is substituted at the ring-closing carbon atom and has a proton at a carbon atom adjacent to the ring-closing carbon atom; (b) an ester of a carboxylic acid having a gamma-carbonyl group and a proton at a carbon atom adjacent to the carbon atom of the carbonyl group; and (c) a carboxylic acid having a gamma-carbonyl group and a proton at a carbon atom adjacent to the carbon atom of the carbonyl group, which process involves contacting the reactant with a catalyst in the presence of hydrogen, at a temperature from 100 to 350° C. and a pressure from 1 to 150 bar (absolute), provided the pressure is low enough to avoid condensation of the heaviest feed component at the temperature chosen, and wherein the catalyst is a weakly acidic heterogeneous catalyst comprising a hydrogenating metal.
摘要翻译：一种选自以下的反应物的氢化方法：（a）在闭环碳原子上被取代并在与闭环碳原子相邻的碳原子处具有质子的5或6元内酯; （b）在与羰基的碳原子相邻的碳原子处具有γ-羰基和质子的羧酸的酯; 和（c）在与羰基碳原子相邻的碳原子处具有γ-羰基和质子的羧酸，该方法包括在氢气存在下使反应物与催化剂接触，温度为100℃ 至350℃，压力为1至150巴（绝对值），条件是压力足够低以避免在所选择的温度下最重的进料组分冷凝，并且其中催化剂是弱酸性非均相催化剂，其包含氢化金属。

4. 发明授权

US07265239B2 Process for the conversion of furfuryl alcohol into levulinic acid or alkyl levulinate 失效
标题翻译：将糠醇转化为乙酰丙酸或乙酰丙酸烷基酯的方法
公开(公告)号：US07265239B2
公开(公告)日：2007-09-04
申请号：US11466630
申请日：2006-08-23
申请人： Wouter David Van De Graaf , Jean-Paul Lange
发明人： Wouter David Van De Graaf , Jean-Paul Lange
IPC分类号： C07C69/66 , C07C59/00
CPC分类号： C07C51/00 , C07C67/00 , C07C59/185 , C07C69/716
摘要： A process for the conversion of furfuryl alcohol into levulinic acid or alkyl levulinate comprising contacting furfuryl alcohol and water or an alkyl alcohol with a porous heterogeneous catalyst comprising strong acid ion-exchange resin, wherein the catalyst has pores with an average pore diameter in the range of from 1 to 1000 nm.
摘要翻译：一种将糠醇转化成乙酰丙酸或乙酰丙酸烷基酯的方法，包括使糠醇与水或烷基醇与包含强酸离子交换树脂的多孔非均相催化剂接触，其中催化剂具有平均孔径在该范围内的孔为1〜1000nm。

5. 发明申请

US20050250958A1 Method for the catalytic conversion of alkylene carbonate 失效
公开(公告)号：US20050250958A1
公开(公告)日：2005-11-10
申请号：US11181252
申请日：2005-07-14
申请人： Johannes De Jonge , Jean-Paul Lange , Dennis Pello
发明人： Johannes De Jonge , Jean-Paul Lange , Dennis Pello
IPC分类号： B01J21/10 , B01J21/16 , B01J37/03 , C07B61/00 , C07C27/02 , C07C29/09 , C07C31/20 , C07C68/06 , C07C69/96 , C11D7/18
CPC分类号： C07C29/095 , B01J21/10 , B01J37/03 , C07C68/065 , Y02P20/52 , C07C69/96 , C07C31/202 , C07C31/205
摘要： A method for catalytic conversion of alkylene carbonate, wherein alkylene carbonate is contacted with C1-C5 aliphatic alcohol and/or water in the presence of Mg, Al mixed (hydr) oxide catalyst having a Mg:Al molar ratio in the range of from 4 to 20.

6. 发明申请

US20050014956A1 Process for the preparation of propylene carbonate 有权
标题翻译：碳酸丙烯酯的制备方法
公开(公告)号：US20050014956A1
公开(公告)日：2005-01-20
申请号：US10880079
申请日：2004-06-29
申请人： Jean-Paul Lange
发明人： Jean-Paul Lange
IPC分类号： C07C29/12 , C07D317/08 , C07C69/96
CPC分类号： C07C29/12 , Y02P20/584 , C07C31/205
摘要： The invention relates to a process for the preparation of propylene carbonate, which process involves contacting propylene oxide with carbon dioxide at a temperature of from 150° C. to 250° C. in the presence of a recycled tetraalkylphosphonium bromide catalyst.
摘要翻译：本发明涉及一种制备碳酸丙烯酯的方法，该方法包括在循环的四烷基溴化鏻催化剂存在下，将环氧丙烷与二氧化碳在150℃至250℃的温度下接触。

7. 发明授权

US06762332B2 Process for preparing an alcohol from an olefin 失效
标题翻译：从烯烃制备醇的方法
公开(公告)号：US06762332B2
公开(公告)日：2004-07-13
申请号：US10239100
申请日：2002-11-22
申请人： Jean-Paul Lange
发明人： Jean-Paul Lange
IPC分类号： C07C2916
CPC分类号： C07C29/16 , C07C31/125
摘要： A process for the preparation of an alcohol from an olefin wherein the olefin is reacted with syngas in the presence of a catalyst system having a homogeneous hydroformylation catalyst and a heterogeneous catalyst having copper on a support.
摘要翻译：一种从烯烃制备醇的方法，其中在具有均匀加氢甲酰化催化剂的催化剂体系和在载体上具有铜的多相催化剂存在下，烯烃与合成气反应。

8. 发明授权

US06307095B1 Process for the preparation of vinylesters 失效
标题翻译：制备乙烯基酯的方法
公开(公告)号：US06307095B1
公开(公告)日：2001-10-23
申请号：US08950427
申请日：1997-10-15
申请人： Johannes Jacobus Keijsper , Jean-Paul Lange , Brendan Dermot Murray
发明人： Johannes Jacobus Keijsper , Jean-Paul Lange , Brendan Dermot Murray
IPC分类号： C07C6704
CPC分类号： C07C67/04 , C07C69/01 , C07C69/24
摘要： A process for the catalytic conversion of carboxylic acids with acetylene to vinylesters. At least one, preferably saturated, secondary carboxylic ester and/or at least one, preferably tertiary carboxylic acid is (are) passed in the gas phase together with acetylene at an elevated temperature, preferably in the range of from 150 to 400° C., over a catalyst comprising zinc and a solid inert oxidic carrier, preferably alumina. The carboxylic acids have advantageously the following formula: in which R1 is H or an alkyl group and R2 and R3 are alkyl groups, the total number of C-atoms of R1+R2+R3 being in the range of from 3 to 18. These vinylesters have a good stability and are particularly useful components in emulsion paints and as modifiers in alkyd and epoxy resin.
摘要翻译：将羧酸与乙炔催化转化成乙烯基酯的方法。在高温下，将至少一种优选饱和的仲羧酸酯和/或至少一种优选叔羧酸与乙炔一起通入气相中温度，优选在150-400℃的范围内，在包含锌和固体惰性氧化载体的催化剂，优选氧化铝中。羧酸有利地具有下式：其中R 1是H或烷基，R 2 并且R 3是烷基，R 1 + R 2 + R 3的C原子总数在3至18的范围内。这些乙烯基酯具有良好的稳定性，并且在乳液漆中和作为醇酸树脂和环氧树脂中的改性剂是特别有用的组分树脂。

9. 发明授权

US06294691B1 Process for the manufacture of carboxylic acids 失效
标题翻译：制备羧酸的方法
公开(公告)号：US06294691B1
公开(公告)日：2001-09-25
申请号：US09102983
申请日：1998-06-22
申请人： Jean-Paul Lange
发明人： Jean-Paul Lange
IPC分类号： C07C5114
CPC分类号： C07C51/14 , C07C53/128
摘要： A process for manufacture of branched carboxylic acids from branched olefins by means of reaction with carbon monoxide and a solid acid catalyst, characterized in that a branched olefin, or a precursor thereof, is reacted in a batch reactor or a plug flow reactor with carbon monoxide and water, in the presence of an acidic ion exchanger, having sufficient acid groups to provide requisite protons for conversion of said olefin or a precursor of it, and carbon monoxide into branched carboxylic acids, and in the presence of a polar non-coordinating organic solvent.
摘要翻译：通过与一氧化碳和固体酸催化剂的反应从支链烯烃制备支链羧酸的方法，其特征在于支化烯烃或其前体在间歇式反应器或活塞式流动反应器中与一氧化碳反应和酸，在酸性离子交换剂存在下，具有足够的酸基以提供用于将所述烯烃或其前体转化的必需质子和一氧化碳转化成支化羧酸，并且在极性非配位有机物存在下溶剂。

10. 发明授权

US09365778B2 Process for liquefying a cellulosic material and its products 有权
标题翻译：液化纤维素材料及其制品的方法
公开(公告)号：US09365778B2
公开(公告)日：2016-06-14
申请号：US13106553
申请日：2011-05-12
申请人： Klaas Lambertus Von Hebel , Jean-Paul Lange
发明人： Klaas Lambertus Von Hebel , Jean-Paul Lange
IPC分类号： C10G1/06 , C08H8/00
CPC分类号： C10G1/002 , C08H8/00 , C10G1/065 , C10G3/50 , C10G2300/1014 , C10G2300/208 , C10G2300/44 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10L1/02 , C10L1/04 , C10L2200/0469 , C10L2290/544 , Y02E50/13 , Y02P30/20
摘要： A process for liquefying a cellulosic material to produce a liquefied product from cellulosic material is provided. Products obtained from such process and use of such products to prepare biofuels is also provided.
摘要翻译：提供了一种用于液化纤维素材料以从纤维素材料生产液化产物的方法。还提供从这种方法获得的产品和使用这些产品来制备生物燃料。

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