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1. 发明申请

US20140216649A1 THIOL-ENE CURED OIL-RESISTANT POLYACRYLATE SEALANTS FOR IN-PLACE GASKETING APPLICATIONS 有权
标题翻译： THIOL-ENE固化耐油聚丙烯酸酯密封剂，用于内部气体应用
公开(公告)号：US20140216649A1
公开(公告)日：2014-08-07
申请号：US12062090
申请日：2008-04-03
申请人： John G. Woods , Richard O. Angus, JR. , Joel D. Schall
发明人： John G. Woods , Richard O. Angus, JR. , Joel D. Schall
IPC分类号： B32B37/12 , C08F8/34 , C08F2/46
CPC分类号： C08F8/02 , C08F8/14 , C08F8/32 , C08F8/34 , C08K5/0025 , C08K5/372 , C09J133/14 , G02F2202/023 , G02F2202/28 , C08F220/28 , C08F220/18 , C08F20/18
摘要： The present invention relates to thiol-ene curing compositions, which cure upon exposure to ultraviolet (UV) light and/or heat. The compositions include components having alkenyl (or “ene”) functionality and components having thiol functionality, which undergo thiol-ene curing. The compositions also include a cure system. More specifically, in some embodiments, the curable compositions include a vinyl polymer bearing alkenyl or thiol terminal functional group(s) and a cross-linking agent having the opposing functionality, i.e., thiol cross-linking agents with alkenyl-terminated vinyl polymers and vinyl cross-linking agents with thiol-terminated vinyl polymers. Also provided are methods of making and using the compositions, such as for sealants for in-place gasketing applications.
摘要翻译：本发明涉及硫醇烯固化组合物，其在暴露于紫外线（UV）光和/或热时固化。组合物包括具有烯基（或“烯”）官能团的组分和具有硫醇官能团的组分，其经历硫醇烯固化。组合物还包括固化体系。更具体地，在一些实施方案中，可固化组合物包括带有烯基或硫醇末端官能团的乙烯基聚合物和具有相反官能团的交联剂，即具有链烯基封端的乙烯基聚合物和乙烯基的硫醇交联剂交联剂与硫醇封端的乙烯基聚合物。还提供了制备和使用组合物的方法，例如用于就地垫片应用的密封剂。

2. 发明授权

US07960445B2 Dual cure compositions employing free radical and RTV cure 有权
标题翻译：使用自由基和RTV固化的双重固化组合物
公开(公告)号：US07960445B2
公开(公告)日：2011-06-14
申请号：US11572738
申请日：2005-07-22
申请人： Anthony F. Jacobine , John G. Woods , Steven T. Nakos , Thomas Fay-Oy Lim
发明人： Anthony F. Jacobine , John G. Woods , Steven T. Nakos , Thomas Fay-Oy Lim
IPC分类号： C03C25/10 , C08L83/00 , C08F8/30
CPC分类号： C08J3/243 , C08G18/10 , C08G18/672 , C08G18/755 , C08G63/6854 , C08G63/6954 , C08G63/914 , C08G2190/00 , C09J167/07 , C08G18/48 , C08G18/718
摘要： The present invention relates to dual curing compositions, which cure with moisture and photo radiation, such as UV light, and methods for preparing and using same. In particular, the compositions of the present invention contain a polyether or polyester backbone, photocurable portion(s) and moisture curable portion(s). The photo curable portion is a urethane or carbamate linkage terminated with a (meth)acryloxyalkyl group. The moisture curable portion is either: (1) a portion terminated with a polyalkoxysilyl group; or (2) a portion having a urea linkage terminated with an alkylpolyalkoxysilyl group.
摘要翻译：本发明涉及用水分和光辐射固化的双重固化组合物，例如UV光，以及制备和使用它们的方法。特别地，本发明的组合物含有聚醚或聚酯骨架，可光固化部分和湿气可固化部分。光固化部分是用（甲基）丙烯酰氧基烷基封端的氨基甲酸酯或氨基甲酸酯键。湿气固化部分是：（1）以多烷氧基甲硅烷基封端的部分; 或（2）具有用烷基聚烷氧基甲硅烷基封端的脲键的部分。

3. 发明申请

US20080139687A1 Vinyl Ether/Acrylate Block Resins, Compositions and Methods of Making Same 审中-公开
标题翻译：乙烯基醚/丙烯酸酯嵌段树脂，组合物和制备方法
公开(公告)号：US20080139687A1
公开(公告)日：2008-06-12
申请号：US11814584
申请日：2005-11-10
申请人： John G. Woods , Joel D. Schall , Steven T. Nakos , Anthony F. Jacobine
发明人： John G. Woods , Joel D. Schall , Steven T. Nakos , Anthony F. Jacobine
IPC分类号： C08G18/63
CPC分类号： C08G18/3212 , C08G18/227 , C08G18/4854 , C08G18/6715 , C08G18/672 , C09J175/16 , C08G18/48
摘要： The present invention relates to vinyl ether or acrylate terminated block resins, compositions incorporating same and methods for preparing same. In particular, the compositions of the present invention may contain a vinyl ether or acrylate terminated block resin, such as a polyurethane block copolymer, a reactive diluent having vinyl ether or 1-alkenyl ether and (meth)acrylate functionality and a curing initiator. The compositions may be exposed to an energy source, e.g., photoradiation, to impart tack-free surface cure.
摘要翻译：本发明涉及乙烯基醚或丙烯酸酯封端的嵌段树脂，其组合物及其制备方法。特别地，本发明的组合物可以含有乙烯基醚或丙烯酸酯封端的嵌段树脂，如聚氨酯嵌段共聚物，具有乙烯基醚或1-链烯基醚和（甲基）丙烯酸酯官能团的反应性稀释剂和固化引发剂。组合物可以暴露于能量源，例如光辐射，以赋予无粘性表面固化。

4. 发明授权

US07087304B1 Polysulfide-based toughening agents, compositions containing same and methods for the use thereof 有权
标题翻译：聚硫醚系增韧剂，含有它们的组合物及其使用方法
公开(公告)号：US07087304B1
公开(公告)日：2006-08-08
申请号：US10367759
申请日：2003-02-19
申请人： John G. Woods , Yuhshi Luh , Mark M. Konarski
发明人： John G. Woods , Yuhshi Luh , Mark M. Konarski
IPC分类号： B32B27/38 , B32B7/12 , C08L63/00 , C09J163/00 , H01L21/56
CPC分类号： C08G59/302 , C08L63/00 , H01L23/293 , H01L2924/0002 , Y10T428/31511 , Y10T428/31515 , C08L81/00 , H01L2924/00
摘要： In accordance with the present invention, there are provided toughening agents which are useful for improving the performance properties of epoxy-based adhesive formulations. For example, epoxidized polysulfides have been found to be useful toughening agents of component level underfill adhesive compositions. Invention materials are liquid rubbers which provide improved fracture toughness while maintaining satisfactory capillary flow properties. Invention materials can be synthesized in neat (solventless) reactions from readily available low-cost raw materials and isolated in high yields. They have linear and branched telechelic structures with terminal epoxide functional groups, and are prepared without substantially increasing the molecular weight of the starting polysulfide materials. Invention materials are compatible with common epoxy formulations and may be used without purification. At low levels of incorporation, they provide adhesives that meet the minimum fracture toughness (Gq>2.0 lb/in) and capillary flow specifications (flow time
摘要翻译：根据本发明，提供了可用于改善环氧基粘合剂制剂的性能的增韧剂。例如，已经发现环氧化多硫化物是组分级底部填充粘合剂组合物的有用的增韧剂。发明材料是提供改善的断裂韧性同时保持令人满意的毛细管流动特性的液体橡胶。本发明材料可以从易于获得的低成本原料的纯（无溶剂）反应中合成并以高收率分离。它们具有带末端环氧官能团的直链和支链遥爪结构，并且在不显着增加起始多硫化物材料的分子量的情况下制备。本发明材料与普通的环氧配方相容，可以不经纯化地使用。在低掺量下，它们提供了许多商业底层填充应用的粘合剂，其满足最小断裂韧性（Gq> 2.0lb / in）和毛细管流动规格（流动时间<180秒）。根据本发明的另一个实施方案，提供了包含本发明化合物的粘合剂组合物及其使用方法。在本发明的另外的实施方案中，提供了制备本发明增韧剂的方法，用于将装置粘附到基底上的方法以及包括附着到第二制品上的第一制品的组件。

5. 发明授权

US07067601B2 Multi-functional alpha-alkoxyalkyl acrylate and methacrylate ester compositions and reworkable polymers formed therefrom 失效
标题翻译：多官能α-烷氧基烷基丙烯酸酯和甲基丙烯酸酯组合物和由其形成的可再加工聚合物
公开(公告)号：US07067601B2
公开(公告)日：2006-06-27
申请号：US10415904
申请日：2001-11-15
申请人： John G. Woods , Susanne D. Morrill
发明人： John G. Woods , Susanne D. Morrill
IPC分类号： C08F116/34
CPC分类号： C08F20/28 , C08F265/06 , C08F290/061 , C08L2666/02 , C09D133/14 , C09J151/003
摘要： Adhesive compositions are disclosed which include acrylates, their polymers, and free radical initiators. The compositions include a multi-functional alpha-alkoxyalkyl (meth)acrylate compound and a free radical initiator. The multi-functional alpha-alkoxyalkyl (meth)acrylate compound is the reaction product of: (a) a (meth)acrylic acid or a (meth)acrylate ester having a free carboxylic acid group; and (b) a compound including two or more 1-alkenyl ether groups and free of acetal and ketal groups, or a compound free of acetal and ketal groups and including one or more 1-alkenyl ether groups and a (meth)acrylate group. The compositions are easier and less expensive to prepare than conventional acrylate compositions and degrade when contacted with an acid medium or when heated. The compositions are useful in a wide range of applications and are compatible with conventional adhesive additives.
摘要翻译：公开了包括丙烯酸酯，它们的聚合物和自由基引发剂的粘合剂组合物。组合物包括多官能α-烷氧基烷基（甲基）丙烯酸酯化合物和自由基引发剂。多官能α-烷氧基烷基（甲基）丙烯酸酯化合物是：（a）（甲基）丙烯酸或具有游离羧酸基的（甲基）丙烯酸酯的反应产物; 和（b）包含两个或更多个1-链烯基醚基并且不含缩醛和缩酮基团的化合物或不含缩醛和缩酮基团的化合物并包括一个或多个1-烯基醚基团和（甲基）丙烯酸酯基团的化合物。组合物比常规丙烯酸酯组合物更容易制备并且更便宜，并且当与酸性介质接触或加热时降解。该组合物可用于广泛的应用，并且与常规粘合剂添加剂相容。

6. 发明授权

US06936664B2 Reworkable epoxidized 1-(cyclo) alkenyl ether/polycarboxylic acid product 失效
标题翻译：可再生的环氧化1-（环）烯基醚/多元羧酸产物
公开(公告)号：US06936664B2
公开(公告)日：2005-08-30
申请号：US10344944
申请日：2001-10-04
申请人： John G. Woods , Susanne D. Morrill , Jianzhao Wang , Brendan J. Kneafsey
发明人： John G. Woods , Susanne D. Morrill , Jianzhao Wang , Brendan J. Kneafsey
IPC分类号： C07D303/22 , C07D303/24 , C07D303/44 , C08G59/12 , C08G59/18 , C08G59/34 , C08G59/42 , C08G59/50 , C09J163/00 , C09J163/02 , C07D303/12 , C08L63/02 , H01L21/56 , H01L23/29
CPC分类号： C07D303/22 , C07D303/24 , C07D303/44 , C08G59/027 , C08G59/12 , C08G59/18 , C08G59/42 , C08G59/5026 , C09J163/00
摘要： The present invention discloses reworkable epoxy compositions suitable for encapsulation of and underfill for electronic components comprising (a) a curable epoxy component which is the reaction product of an epoxidized 1-alkenyl ether or 1-cycloalkenyl ether and a polycarboxylic acid, the reaction product being substantially free of unreacted acid or acid impurities; and (b) a curing agent for the epoxy component, wherein the reaction products of the epoxy composition are reworkable. The cured epoxy compositions of this invention contain thermally labile weak α-alkoxy ester linkages which provide for the reworkable aspect of the invention.
摘要翻译：本发明公开了适用于电子部件的包封和底部填充的可再加工的环氧组合物，其包含（a）作为环氧化的1-链烯基醚或1-环烯基醚与多元羧酸的反应产物的可固化环氧组分，反应产物为基本上不含未反应的酸或酸性杂质; 和（b）环氧组分的固化剂，其中环氧组合物的反应产物是可再加工的。本发明的固化环氧组合物含有热不稳定的弱α-烷氧基酯键，其提供本发明的可再加工方面。

7. 发明授权

US06627762B1 Acetal and hemiacetal ester linked propylene carbonate functional (meth)acrylic esters and method of making same 失效
标题翻译：乙缩醛和半缩醛酯连接的丙烯碳酸酯官能（甲基）丙烯酸酯及其制备方法
公开(公告)号：US06627762B1
公开(公告)日：2003-09-30
申请号：US10277988
申请日：2002-10-23
申请人： John G. Woods , Susanne D. Morrill
发明人： John G. Woods , Susanne D. Morrill
IPC分类号： C07D31736
CPC分类号： C08F220/28 , C07D317/36 , C08F216/1416
摘要： Compounds of the formula: wherein R1 is H or methyl, R2 is H or alkyl, R3 is C2-C4 alkylene, n is 0-4, n′ is 1-4, x is one or more, y is one or more, x+y=z, and A is a z-valent organic group linked to the group or groups on the left thereof through a carbon atom and is linked to the group or groups on the right thereof through an ether or ester oxygen atom, or, provided that x and y are both 1, a direct bond.
摘要翻译：下式的化合物：其中R 1是H或甲基，R 2是H或烷基，R 3是C 2 -C 4亚烷基，n是0-4，n'是1-4，x是1或更多的是，y是一个或多个，x + y = z，A是通过碳原子与其左侧的基团连接的z价有机基团，并且通过碳原子连接到其右侧的基团醚或酯氧原子，或者如果x和y均为1，则直接键合。

8. 发明授权

US5113003A Silicon-containing phenoxy ethers, polymers thereof, and use of such polymers 失效
标题翻译：含硅的苯氧基醚，其聚合物和这种聚合物的使用
公开(公告)号：US5113003A
公开(公告)日：1992-05-12
申请号：US672221
申请日：1991-03-20
申请人： John G. Woods , Pauline Coakley
发明人： John G. Woods , Pauline Coakley
IPC分类号： C07F7/18 , C08G8/04 , C08G61/00 , C08G77/48 , C09D183/14 , G03F7/075
CPC分类号： C07F7/1844 , C07F7/1868 , C08G61/00 , C08G77/48 , C08G8/04 , C09D183/14 , G03F7/0757
摘要： The silicon-containing phenoxy ethers are of the formula III: ##STR1## wherein R.sup.1 and R.sup.2 which may be the same or different are selected from H, --R.sup.3 --X, aliphatic hydrocarbyl having 1-6 carbon atoms or aryl, or substituted derivatives thereof, provided that not more than one of R.sup.1 and R.sup.2 is H;R.sup.3 is a divalent C.sub.1 -C.sub.30 aliphatic and/or aromatic hydrocarbyl group which may optionally be substituted, or interrupted, by a hetero atom;R.sup.4 and R.sup.5 which may be the same or different are H, ##STR2## or an ortho para directing activating group for aromatic electrophilic substitution, other than an amine;and X is a reactive functional group capable of undergoing an acid-catalyzed electrophilic aromatic substitution reaction with a phenol, for example an aldehyde group. They can be polymerized to produce silicone-modified polymers of the phenol-aldehyde type without the use of free aldehyde. One-part compositions containing a compound of the formula III and a latent acid catalyst (e.g. for photoinitiation or thermal initiation of polymerization) are described. The compositions are intended for use as coatings, sealants, adhesives, potting compositions or photoresists.Exemplified compounds are of the formula VII: ##STR3##

9. 发明授权

US4957960A Encapsulating compositions 失效
标题翻译：封装组合物
公开(公告)号：US4957960A
公开(公告)日：1990-09-18
申请号：US472596
申请日：1990-01-30
申请人： Stephen J. Harris , John G. Woods , John M. Rooney , Marueen G. MacManus , John Guthrie
发明人： Stephen J. Harris , John G. Woods , John M. Rooney , Marueen G. MacManus , John Guthrie
IPC分类号： C08G59/00 , C08K5/00 , C08K5/06 , C08K5/07 , C08K5/15 , C08K5/16 , C08K5/20 , C08K5/5419 , C08K5/549 , C08L63/00 , C08L71/00 , C08L83/04 , C08L101/00 , H01B3/40 , H01L23/29 , H01L23/31
CPC分类号： H01B3/40 , C08K5/0008 , C08K5/06 , C08K5/15 , C08K5/20 , C08K5/549
摘要： An encapsulating composition for electronic devices comprises a curable material such as a silicone resin and an ion scavenger compound selected from certain calixarene or oxacalixarene compounds in which at least half of the phenolic groups have been substituted by specific groups and certain silacrown compounds. Exemplary ion scavenger compounds include ##STR1## the tetraethyl acetate of 7, 13, 19, 25-tetra-tertbutyl-27, 28, 29, 30-tetrahydroxy-2,3-dihomo-3-oxacalix-4-arene and 1,1-dimethasila-17-crown-6.

10. 发明授权

US4323875A Method of making temperature sensitive device and device made thereby 失效
标题翻译：制造温敏装置及装置的方法
公开(公告)号：US4323875A
公开(公告)日：1982-04-06
申请号：US226559
申请日：1981-01-21
申请人： Joseph A. Tentarelli , Richard L. Wahlers , John G. Woods
发明人： Joseph A. Tentarelli , Richard L. Wahlers , John G. Woods
IPC分类号： G01K7/16 , H01C7/02 , H01C17/08 , H01C17/30 , H01C3/04 , B05D5/12
CPC分类号： H01C17/08 , H01C17/30 , H01C7/021 , Y10T29/49085
摘要： A method of making a thin nickel film temperature sensitive device with a relatively high positive temperature coefficient of resistance utilizing a film of nickel deposited from a bulk nickel source onto an electrically insulating substrate, and device made thereby including the step of heat treating a resistor element having a thin film of nickel deposited on an electrically insulating substrate by heating in a reducing atmosphere to a peak temperature of at least 550.degree. C., over a heating cycle of at least about 20 minutes. The nickel film of the heat treated resistor element has a selected temperature coefficient of resistance which is at least 60% of the value of the coefficient for the bulk nickel and a sheet resistance of at least one ohm per square which properties are determined by the heat treating temperature and cycle time, and the thickness of the nickel film. The resistor element can be made by vacuum depositing the nickel film to the desired thickness onto the insulating substrate, and affixing terminations to the ends of the resistor element and applying a protective outer coating to the nickel film after the heat treating of the element.
摘要翻译：一种使用从大块镍源沉积到电绝缘基板上的镍膜形成具有相对高的正温度系数电阻的薄镍膜温度敏感器件的方法，以及由此制成的器件包括对电阻元件进行热处理的步骤具有通过在还原气氛中加热至沉积在电绝缘基板上的镍薄膜至峰值温度至少为550℃的加热循环至少约20分钟。经热处理的电阻器元件的镍膜具有选定的电阻温度系数，其至少为体积镍的系数值的60％，并且每平方厘米至少1欧姆的薄层电阻，其特性由热量确定处理温度和循环时间以及镍膜的厚度。电阻元件可以通过将镍膜真空沉积到所需的厚度到绝缘基板上，并且将端子固定到电阻元件的端部并且在元件的热处理之后向镍膜施加保护性外涂层来制造。

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