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1. 发明授权

US08163899B2 Process for producing laurolactam 有权
标题翻译：生产月桂内酰胺的方法
公开(公告)号：US08163899B2
公开(公告)日：2012-04-24
申请号：US12526494
申请日：2008-02-08
申请人： Kazuaki Ishihara , Junichi Kugimoto , Joji Kawai
发明人： Kazuaki Ishihara , Junichi Kugimoto , Joji Kawai
IPC分类号： C07D201/04
CPC分类号： C07D201/04 , C07D225/02 , Y02P20/582
摘要： Disclosed is a method for producing laurolactam from cyclododecanone and hydroxylamine in a simple process and with high efficiency. The method comprises the following steps (a) to (e): (a) reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an excess amount of cyclododecanone or a solvent to produce cyclododecanone oxime; (b) separating the reaction mixture obtained after the oxime-forming step into an oil and an aqueous phases and collecting a solution of cyclododecanone oxime of the oil phase as; (c) removing dissolved water from the solution of cyclododecanone oxime which is collected as an oily phase in the oil/aqueous phase separation step; (d) producing laurolactam from cyclododecanone oxime by rearrangement reaction using an aromatic-ring containing compound as a rearrangement catalyst; and (e) separating the produced laurolactam from the reaction mixture after the rearrangement step and purifying the laurolactam.
摘要翻译：公开了一种以简单的工艺和高效率从环十二酮和羟胺制备月桂内酰胺的方法。该方法包括以下步骤（a）至（e）：（a）在过量的环十二烷酮或溶剂的存在下，使环十二酮与羟胺在水溶液中反应，生成环十二酮肟; （b）将在肟形成步骤后获得的反应混合物分离成油和水相，并收集油相的环十二酮肟溶液; （c）从在油/水相分离步骤中以油相收集的环十二酮肟溶液中除去溶解的水; （d）使用含芳环的化合物作为重排催化剂，通过重排反应从环十二酮肟生产月桂内酰胺; 和（e）在重排步骤之后将所生产的月桂内酰胺与反应混合物分离并纯化十二内酰胺。

2. 发明申请

US20110065913A1 PROCESS FOR PRODUCING LAUROLACTAM 有权
标题翻译：生产乳酸菌的方法
公开(公告)号：US20110065913A1
公开(公告)日：2011-03-17
申请号：US12993451
申请日：2009-05-19
申请人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
发明人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention relates to a process for producing laurolactam from cyclododecanone oxime by liquid-phase rearrangement reaction using trichlorotriazine as a rearrangement catalyst. The present invention can provide a process which can solve the problem of termination of the reaction at a certain conversion, can prevent an inactive precipitate generated from trichlorotriazine from precipitating in the course of the reaction process, and can remove an inactive precipitate, an active intermediate and a residual catalyst.
摘要翻译：本发明涉及使用三氯三嗪作为重排催化剂通过液相重排反应从环十二酮肟生产十二内酰胺的方法。本发明可以提供能够解决在一定转化时终止反应的问题的方法，可以防止三氯三嗪在反应过程中产生的不活泼的沉淀物沉淀，并且可以除去无活性的沉淀物，活性中间体和残留催化剂。

3. 发明授权

US5091842A Device for removing D.C. components from output of multi-phase inverter 失效
标题翻译：用于从多相逆变器的输出中去除直流元件的装置
公开(公告)号：US5091842A
公开(公告)日：1992-02-25
申请号：US515457
申请日：1990-04-26
申请人： Joji Kawai
发明人： Joji Kawai
IPC分类号： H02M7/539 , H02M7/537
CPC分类号： H02M7/53875 , H02M2007/4803
摘要： A device for removing D.C. components from output voltages of a multi-phase inverter which converts a D.C. voltage into first to N-th phases of A.C. voltages comprises first to (N-1)th detectors connected between the first-phase output line of the multi-phase inverter and the second- to N-th-phase output lines of the multi-phase inverter, respectively. The device also comprises controllers for respectively controlling the second- to N-th-phase output voltages of the inverter in such a manner that the D.C. components detected by the first to (N-1)th detectors are nullified.
摘要翻译：用于从DC电压转换为第一至第N相的电压的多相逆变器的输出电压中去除DC分量的装置包括：第一至第（N-1）个检测器，连接在第一相输出线多相逆变器和多相逆变器的二相到N相输出线。该装置还包括用于分别控制逆变器的第二至第N相输出电压的控制器，使得由第一至第（N-1）个检测器检测到的直流分量无效。

4. 发明授权

US4969079A Corrective device for inverter output voltage error 失效
标题翻译：变频器输出电压误差校正装置
公开(公告)号：US4969079A
公开(公告)日：1990-11-06
申请号：US472297
申请日：1990-01-30
申请人： Mitsuo Kiriyama , Joji Kawai
发明人： Mitsuo Kiriyama , Joji Kawai
IPC分类号： H02M7/48 , H02M7/537 , H02M7/5395
CPC分类号： H02M7/5395
摘要： A corrective device for an inverter output voltage error in which a current sensor is connected in series with the output of an inverter, the polarity of current detected by the current sensor is discriminated by a polarity decision current, a value corresponding to an input D.C. voltage is found by a D.C. voltage sensor, a signal with the polarity of the value inverted according to the discriminated result delivered from the polarity decision current is generted by a polarity inverter circuit, and the signal is applied as a correction signal to the PWM (pulse-width modulation) circuit of the inverter so as to correct the output voltage error.
摘要翻译：用于逆变器输出电压误差的校正装置，其中电流传感器与逆变器的输出串联，电流传感器检测到的电流的极性由极性判定电流来区分，对应于输入直流电压由直流电压传感器发现，极性反转电路产生根据极性判定电流输出的鉴别结果反转的极性值的信号，并将该信号作为校正信号施加到PWM（脉冲宽带调制）电路，以纠正输出电压误差。

5. 发明授权

US4667297A Running speed detector 失效
标题翻译：运行速度检测器
公开(公告)号：US4667297A
公开(公告)日：1987-05-19
申请号：US683583
申请日：1984-12-19
申请人： Joji Kawai
发明人： Joji Kawai
IPC分类号： G01P3/489 , G01P3/42 , G01P3/48 , G06F15/20 , G06G7/00
CPC分类号： G01P3/489
摘要： The present invention relates to a running speed detector comprising:a pulse encoder which generates pulses of a frequency proportional to the running speed of a rotary member;pulse period counting device for counting the periods of pulses having said frequency relying upon clock signals;memory for storing ounted values of periods counted by said pulse period counting means; andand a calculating device which receives pulses having said frequency, which calculates the sum of n latest counted values that have been counted already after the arrival of each of said pulses or after the arrival of a predetermined number of pulses, and which calculates the running speed that varies in proportion to a ratio of the number n of counted values of periods to said sum of counted values of periods.
摘要翻译：运行速度检测器技术领域本发明涉及一种运行速度检测器，包括：脉冲编码器，其生成与旋转部件的运行速度成比例的频率的脉冲; 脉冲周期计数装置，用于根据时钟信号计数具有所述频率的脉冲的周期; 用于存储由所述脉冲周期计数装置计数的周期值的存储器; 以及计算装置，其接收具有所述频率的脉冲，其计算在每个所述脉冲到达之后或在预定脉冲数到达之后已经计数的n个最近计数值的和，并且计算运行速度与周期的计数值的数量n与周期的计数值的总和的比率成比例地变化。

6. 发明授权

US08338589B2 Process for producing laurolactam 有权
标题翻译：生产月桂内酰胺的方法
公开(公告)号：US08338589B2
公开(公告)日：2012-12-25
申请号：US12993451
申请日：2009-05-19
申请人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
发明人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
IPC分类号： C07D201/04 , C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention relates to a process for producing laurolactam from cyclododecanone oxime by liquid-phase rearrangement reaction using trichlorotriazine as a rearrangement catalyst. The present invention can provide a process which can solve the problem of termination of the reaction at a certain conversion, can prevent an inactive precipitate generated from trichlorotriazine from precipitating in the course of the reaction process, and can remove an inactive precipitate, an active intermediate and a residual catalyst.
摘要翻译：本发明涉及使用三氯三嗪作为重排催化剂通过液相重排反应从环十二酮肟生产十二内酰胺的方法。本发明可以提供能够解决在一定转化时终止反应的问题的方法，可以防止三氯三嗪在反应过程中产生的不活泼的沉淀物沉淀，并且可以除去无活性的沉淀物，活性中间体和残留催化剂。

7. 发明申请

US20100267944A1 PROCESS FOR PRODUCING LAUROLACTAM 有权
标题翻译：生产乳酸菌的方法
公开(公告)号：US20100267944A1
公开(公告)日：2010-10-21
申请号：US12744675
申请日：2008-11-19
申请人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro II
发明人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro II
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02 , Y02P20/582
摘要： Provided is a process for efficiently producing laurolactam by simple steps from cyclododecanone and hydroxylamine. This production process comprises the steps of: (a) reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an oxime-formation solvent to produce cyclododecanone oxime; (b) separating the reaction mixture obtained after the oxime-forming step into an oil and an aqueous phases and collecting a solution of cyclododecanone oxime of the oil phase; (c) removing a part or all of the oxime-formation solvent and dissolved water from the solution of cyclododecanone oxime which is collected as an oil phase in the oil/aqueous phase separation step, whereby preparing a solution containing a rearrangement solvent to be used in a rearrangement reaction in a later step and the cyclododecanone oxime; (d) producing laurolactam from cyclododecanone oxime by rearrangement reaction using an aromatic-ring containing compound as a rearrangement catalyst; and (e) separating and removing the rearrangement solvent and the rearrangement catalyst from the reaction mixture after the rearrangement step, and purifying the laurolactam.
摘要翻译：提供一种通过简单的步骤从环十二酮和羟胺有效地生产十二内酰胺的方法。该制备方法包括以下步骤：（a）在肟形成溶剂存在下，使环十二酮与羟胺在水溶液中反应，生成环十二酮肟; （b）将在肟形成步骤后获得的反应混合物分离成油相和水相，并收集油相的环十二烷酮肟溶液; （c）从油/水相分离步骤中以油相收集的环十二酮肟溶液中除去部分或全部肟形成溶剂和溶解的水，由此制备含有使用的重排溶剂的溶液在后续步骤中的重排反应和环十二酮肟; （d）使用含芳环的化合物作为重排催化剂，通过重排反应从环十二酮肟生产月桂内酰胺; 和（e）在重排步骤之后从反应混合物中分离和除去重排溶剂和重排催化剂，并纯化月桂内酰胺。

8. 发明申请

US20130005960A1 METHOD FOR PRODUCING AMIDE COMPOUND 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：US20130005960A1
公开(公告)日：2013-01-03
申请号：US13635092
申请日：2011-03-15
申请人： Junichi Kugimoto , Joji Kawai , Kazuo Yamato , Masahide Okada , Tsunemi Sugimoto , Hiroshi Matsumoto
发明人： Junichi Kugimoto , Joji Kawai , Kazuo Yamato , Masahide Okada , Tsunemi Sugimoto , Hiroshi Matsumoto
IPC分类号： C07D225/02
CPC分类号： C07D201/06 , C07D201/04 , C07D225/02
摘要： The present invention relates to a method for producing a high purity, high quality amide compound, particularly, lactam. A first embodiment of the present invention is characterized in that an amount of each of a halide, an aldehyde compound, an alcohol compound and a nitrile compound contained in a solution recycled into an oxime-forming step is controlled to an amount of 0.4 mol % or less based on the ketone as a starting material. A second embodiment of the present invention is characterized in that one or more compounds selected from the group consisting of a ketone, an oxime and an amide compound are purified by hydrogenation and/or crystallization for eliminating impurities containing a double bond. A third embodiment of the present invention is characterized in that a content of impurities having a cyclic bridge structure is controlled by using a cycloalkanone purified by recrystallization.
摘要翻译：本发明涉及一种生产高纯度，优质酰胺化合物，特别是内酰胺的方法。本发明的第一实施方案的特征在于，将再循环到肟形成步骤的溶液中所含的卤化物，醛化合物，醇化合物和腈化合物中的每一种的量控制为0.4mol％基于酮作为原料。本发明的第二个实施方案的特征在于，通过氢化和/或结晶纯化一种或多种选自酮，肟和酰胺化合物的化合物，以消除含有双键的杂质。本发明的第三实施方案的特征在于通过使用通过重结晶纯化的环烷酮来控制具有环状桥结构的杂质的含量。

9. 发明授权

US06649757B2 Process for producing laurolactam from cyclododecanone 有权
标题翻译：从环十二酮生产十二内酰胺的方法
公开(公告)号：US06649757B2
公开(公告)日：2003-11-18
申请号：US10345548
申请日：2003-01-16
申请人： Nobuyuki Kuroda , Joji Kawai , Hideo Shimomura
发明人： Nobuyuki Kuroda , Joji Kawai , Hideo Shimomura
IPC分类号： C07D22502
CPC分类号： C07D201/06 , C07D201/04
摘要： Laurolactam having high quality is produced by reacting cyclododecanone with a hydroxylamine salt of a mineral acid, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction, wherein a content of each of oxygen atom-containing C12 organic compounds, for example, cyclododecenone or epoxycyclododecane, and cycloaliphatic unsaturated C12 hydrocarbon compounds, contained, as an impurity, in the staring cyclododecanone material, is controlled to 1,000 ppm or less.
摘要翻译：通过使环十二酮与无机酸的羟胺盐反应，通过贝克曼重排反应将所得的环十二烷酮肟转化为十二内酰胺，生成具有高品质的月桂内酰胺，其中各含氧原子的C12有机化合物，例如环十二酮或环氧环十二烷和环脂肪族不饱和C12烃化合物被控制在1000ppm以下，作为杂质，在起始环十二烷酮材料中。

10. 发明授权

US5212630A Parallel inverter system 失效
标题翻译：并行逆变器系统
公开(公告)号：US5212630A
公开(公告)日：1993-05-18
申请号：US809572
申请日：1991-12-18
申请人： Yushin Yamamoto , Joji Kawai
发明人： Yushin Yamamoto , Joji Kawai
IPC分类号： H02J3/38 , H02M7/48 , H02M7/493
CPC分类号： H02M7/493
摘要： A parallel inverter system has a plurality of AC output inverters of an instantaneous voltage control type, a bus for connecting outputs of the inverters to a load so as to share the load current, a detection circuit for detecting a cross current component in a current flowing among the inverters, and an instantaneous voltage control circuit for controlling the output voltages of the inverters. In response to a signal in accordance with the detected cross current component from the detection circuit, the voltage control circuit inserts a virtual impedance between the inverters so as to suppress cross current.

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