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1. 发明申请

US20050204957A1 Modified carbon black dispersion liquid and water base ink containing the same 有权
标题翻译：改性炭黑分散液和含有其的水基油墨
公开(公告)号：US20050204957A1
公开(公告)日：2005-09-22
申请号：US10517951
申请日：2004-04-23
申请人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
发明人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
IPC分类号： C09D17/00 , C09C1/48 , C09C1/56 , C09C3/06 , C09C3/08 , C09D11/00 , C09D11/322 , C09D11/324 , C09D11/326 , C09D11/38 , B41J2/01 , C09D11/02
CPC分类号： C09D11/324 , C01P2004/62 , C01P2006/12 , C01P2006/19 , C09C1/565 , C09D11/17
摘要： The present invention provides a water-based ink that is used in ink jet printer printing, with a writing instrument, or the like, that has a low settling rate and for which clogging is not prone to occurring, that can be stored stably for a long period without the viscosity or the carbon black particle diameter increasing, and for which printing with a deep black color and a high print density is possible, and a modified carbon black dispersion used for preparing this water-based ink. The present invention is a liquid having dispersed therein a modified carbon black obtained by subjecting a carbon black raw material powder to oxidation treatment, wherein the modified carbon black has on the surface thereof (a) carboxyl groups, and (b) lactone groups in a molar amount of at least 500 μmol/g relative to the weight of the modified carbon black and a molar ratio of 0.8 to 1.1 times the amount of the carboxyl groups.
摘要翻译：本发明提供一种水性油墨，其用于喷墨打印机印刷中，具有书写工具等，其具有低沉降速率并且不容易发生堵塞，可以稳定地储存长时间没有粘度或炭黑粒径增加，并且可以进行深黑色和高印刷密度的印刷，以及用于制备该水性油墨的改性炭黑分散体。本发明是分散有炭黑原料粉末进行氧化处理而得到的改性炭黑的液体，其中，改性炭黑在其表面上具有（a）羧基，（b）在摩尔量相对于改性炭黑的重量为至少500mol / g，摩尔比为羧基量的0.8〜1.1倍。

2. 发明授权

US5326866A Liquid azo dye and ink composition containing the same 失效
标题翻译：液体偶氮染料和含有它的油墨组合物
公开(公告)号：US5326866A
公开(公告)日：1994-07-05
申请号：US59666
申请日：1993-05-12
申请人： Takashi Ono , Tatsuya Yagyu , Tetsui Akase
发明人： Takashi Ono , Tatsuya Yagyu , Tetsui Akase
IPC分类号： C09B29/15 , C09B29/28 , C09B29/50 , C09B31/068 , C09B31/08 , C09B31/147 , C09B67/44 , C09D11/02 , C09D11/033 , C09D11/328 , C09D11/36 , C09B29/46 , C09D11/18
CPC分类号： C09D11/17 , C09B29/106 , C09B29/28 , C09B29/366 , C09B31/068 , C09B31/08 , C09B31/147 , C09B67/0083 , C09D11/328 , Y10S8/938
摘要： A liquid azo dye represented by the formula: ##STR1## (wherein, A stands for a phenylene group which may have a substituent, n is o or 1, Cp is a pyrazolone derivative residue or a naphthol derivative residue, X is --NH-- or --COO-- and R is an alkyl group having 3 to 12 carbon atoms).
摘要翻译：由下式表示的液体偶氮染料：其中，A表示可具有取代基的亚苯基，n表示0或1，Cp表示吡唑啉酮衍生物残基或萘酚衍生物残基，X表示-NH- 或-COO-，R为碳原子数3〜12的烷基）。

3. 发明授权

US5095100A Metal complex dyes and preparation thereof 失效
标题翻译：金属络合染料及其制备方法
公开(公告)号：US5095100A
公开(公告)日：1992-03-10
申请号：US537904
申请日：1990-06-12
申请人： Takashi Ono , Tatsuya Yagyu , Katsumi Fukuda , Minako Terasaki
发明人： Takashi Ono , Tatsuya Yagyu , Katsumi Fukuda , Minako Terasaki
IPC分类号： C09B45/24 , C09B45/38 , C09B62/095 , C09B69/00 , D06P3/32
CPC分类号： C09B62/095 , C09B45/24 , C09B45/38 , C09B69/007 , D06P3/3206 , D06P3/326
摘要： Metal complex dyes comprising a metalizable azo compound represented by one of Formulas [I] through [IV]: ##STR1## In Formulas [I] through [IV], Ps represents a phosphono group in the form of a free acid or a salt; Sf represents a sulfo group in the form of a free acid or a salt; m is 0, 1 or 2. R.sup.1 represents a hydrogen atom or an amino group; X represents a hydroxyl group, an alkoxy group having a carbon number of 1 or 2 or a carboxyl group. Y represents a hydroxyl group, an alkoxy group having a carbon number of 1 or 2, a carboxyl group or a methyl group; R.sup.2 represents a hydrogen atom or a hydroxyl group; A represents a phenyl group or naphthyl group selected from the group comprising the following 1 through 4: ##STR2## In the above formulas 1 through 4, Sf has the same definition as above; n is 0, 1 or 2. R.sup.3 represents a hydroxyl group or a carboxyl group; R.sup.4 represents a hydroxyl group, a carboxyl group or an amino group; R.sup.5 and R.sup.6 independently represent a hydroxyl group or a carboxyl group; R.sup.7 and R.sup.8 independently represent a hydrogen atom, a hydroxyl group or an amino group. B has the same definition as A above except that R.sup.3 represents a hydroxyl group, a carboxyl group or an amino group. R.sup.9 represents a hydrogen atom, a methyl group, an alkoxy group having a carbon number of 1 or 2 or a sulfo group in the form of a free acid or a salt; D represents a coupling component residue having a metalizable hydroxyl group at the position adjoining to the azo group.Use of these metal complex dyes makes it possible to dye metal-tanned leather with good permeability and excellent color fastness to rubbing and color fastness to light.
摘要翻译：包含由式[I]至[IV]之一表示的可金属化的偶氮化合物的金属络合物染料：式（I）中的化合物： [I]〜[IV]中，Ps表示游离酸或盐形式的膦酰基; Sf表示游离酸或盐形式的磺基; m为0,1或2.R 1表示氢原子或氨基; X表示羟基，碳数为1或2的烷氧基或羧基。 Y表示羟基，碳数为1或2的烷氧基，羧基或甲基; R2表示氢原子或羟基; A表示选自包括以下+ E，crc / 1 /至+ E，crc / 4 /：图像+ E，CRC / 1 /图像+ E，CRC / 2的苯基或萘基在上述公式+ E中，crc / 1 /至+ E，crc / 4 /，Sf具有与上述相同的定义; n为0,1或2.R 3表示羟基或羧基; R4代表羟基，羧基或氨基; R5和R6独立地表示羟基或羧基; R 7和R 8独立地表示氢原子，羟基或氨基。 B具有与上述相同的定义，只是R3表示羟基，羧基或氨基。 R9表示氢原子，甲基，碳数为1或2的烷氧基或游离酸或盐形式的磺基; D表示在与偶氮基相邻的位置具有可金属化羟基的偶合成分残基。使用这些金属络合染料使得可以染色具有良好透光性和优异的耐色牢度的金属鞣革，并且具有良好的耐光色牢度。

4. 发明授权

US4666519A Aqueous ink composition 失效
标题翻译：水性油墨组合物
公开(公告)号：US4666519A
公开(公告)日：1987-05-19
申请号：US749086
申请日：1985-06-26
申请人： Kazutoshi Akiyama , Takashi Ono , Tatsuya Yagyu
发明人： Kazutoshi Akiyama , Takashi Ono , Tatsuya Yagyu
IPC分类号： C09B69/00 , C09D11/00 , C09D11/16
CPC分类号： C09D11/17 , C09B69/00 , C09D11/00
摘要： The present invention provides an aqueous ink composition having water-resistance in written trace or printed image on or after writing down and having good solution stability; which comprises as a coloring agent a reaction mixture of a dye, an epoxy compound and optionally an amine compound.
摘要翻译：本发明提供一种水性油墨组合物，其在书写或记录之后具有书写痕迹或印刷图像的耐水性并且具有良好的溶液稳定性; 其包括染料，环氧化合物和任选的胺化合物的反应混合物作为着色剂。

5. 发明授权

US07220304B2 Modified carbon black dispersion liquid and water base ink containing the same 有权
标题翻译：改性炭黑分散液和含有其的水基油墨
公开(公告)号：US07220304B2
公开(公告)日：2007-05-22
申请号：US10517951
申请日：2004-04-23
申请人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
发明人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
IPC分类号： C09D11/00
CPC分类号： C09D11/324 , C01P2004/62 , C01P2006/12 , C01P2006/19 , C09C1/565 , C09D11/17
摘要： The present invention provides a water-based ink that is used in ink jet printer printing, with a writing instrument, or the like, that has a low settling rate and for which clogging is not prone to occurring, that can be stored stably for a long period without the viscosity or the carbon black particle diameter increasing, and for which printing with a deep black color and a high print density is possible, and a modified carbon black dispersion used for preparing this water-based ink. The present invention is a liquid having dispersed therein a modified carbon black obtained by subjecting a carbon black raw material powder to oxidation treatment, wherein the modified carbon black has on the surface thereof (a) carboxyl groups, and (b) lactone groups in a molar amount of at least 500 μmol/g relative to the weight of the modified carbon black and a molar ratio of 0.8 to 1.1 times the amount of the carboxyl groups.
摘要翻译：本发明提供一种水性油墨，其用于喷墨打印机印刷中，具有书写工具等，其具有低沉降速率并且不容易发生堵塞，可以稳定地储存长时间没有粘度或炭黑粒径增加，并且可以进行深黑色和高印刷密度的印刷，以及用于制备该水性油墨的改性炭黑分散体。本发明是分散有炭黑原料粉末进行氧化处理而得到的改性炭黑的液体，其中，改性炭黑在其表面上具有（a）羧基，（b）在摩尔量相对于改性炭黑的重量为至少500mol / g，摩尔比为羧基量的0.8〜1.1倍。

6. 发明授权

US5795970A Mixed disazo-dye composition and black aqueous ink composition containing the same that provides high grade image on print 失效
标题翻译：混合的双偶氮染料组合物和含有这种组合物的黑色水性墨水组合物，其在印刷品上提供高等级的图像
公开(公告)号：US5795970A
公开(公告)日：1998-08-18
申请号：US701578
申请日：1996-08-22
申请人： Takashi Ono , Tatsuya Yagyu , Yoshihiro Sawatari , Masaki Sasaki , Miharu Kanaya , Hiroko Hayashi , Akio Owatari , Yasuhiro Ouki
发明人： Takashi Ono , Tatsuya Yagyu , Yoshihiro Sawatari , Masaki Sasaki , Miharu Kanaya , Hiroko Hayashi , Akio Owatari , Yasuhiro Ouki
IPC分类号： C09B67/22 , C09D11/00 , B41J2/01 , C09D11/02
CPC分类号： C09D11/328 , C09B67/0055
摘要： A disazo dye composition comprising at least a disazo dye represented by the formula (I) and a disazo dye represented by the formula (II): ##STR1## (wherein X and Y indicate an alkoxy group having 1 to 4 carbon atoms, and M indicates hydrogen or a cation selected from the group consisting of, alkaline metal, NH.sub.4, alkyl-substituted ammonium, alkanolammonium, morpholinium and piperidinium), wherein, when the disazo dye composition is analyzed by liquid chromatography, the area ratio of the peak area (Sp) of the disazo dye represented by the formula (I) to the peak area (Sc) of the disazo dye represented by the formula (II), that is Sp:Sc is from 1:0.4 to 1:2.4. This disazo dye composition provides a high quality image, rapid ink fixing and the like even on the plain paper.
摘要翻译：包含至少一种由式（I）表示的双偶氮染料和由式（II）表示的双偶氮染料的双偶氮染料组合物：其中X和Y表示烷氧基具有1至4个碳原子，M表示氢或选自碱金属，NH 4，烷基取代的铵，链烷醇铵，吗啉鎓和哌啶鎓的阳离子），其中当通过液相色谱分析双偶氮染料组合物时由式（I）表示的双偶氮染料的峰面积（Sp）与式（II）表示的双偶氮染料的峰面积（Sc）的面积比为Sp：Sc为1： 0.4〜1：2.4。这种双偶氮染料组合物即使在普通纸上也提供高质量的图像，快速的墨水固定等。

7. 发明授权

US5486601A Trisazo dye, and aqueous ink composition containing the same 失效
标题翻译：三唑并染料和含有它们的水性油墨组合物
公开(公告)号：US5486601A
公开(公告)日：1996-01-23
申请号：US314001
申请日：1994-09-28
申请人： Tatsuya Yagyu , Takashi Ono
发明人： Tatsuya Yagyu , Takashi Ono
IPC分类号： C09B35/46 , C09D11/00 , C09D11/02 , C09D11/033 , C09D11/328
CPC分类号： C09D11/17 , C09B35/46 , C09D11/328
摘要： Disclosed is a trisazo dye represented by the formula: ##STR1## wherein R.sup.1 and R.sup.2 independently represent a substituted amino group which is substituted with hydrogen, a hydroxyl group, a carboxyl group, an amino group, an alkyl group having 1 to 4 carbon atoms, a hydroxyalkyl group or an acyl group, or an alkyl group having 1 to 4 carbon atoms or an alkoxy group having 1 to 4 carbon atoms; and R.sup.3 is hydrogen, an alkyl or alkoxy group having 1 to 6 carbon atoms; provided that R.sup.1 and R.sup.2 are not amino groups or substituted amino groups simultaneously.A process for producing the trisazo dye and an aqueous ink composition containing the trisazo dye are also disclosed.
摘要翻译：公开了由下式表示的三偶氮染料：其中R 1和R 2独立地表示被氢取代的取代氨基，羟基，羧基，氨基，烷基具有1至4个碳原子，羟基烷基或酰基，或具有1至4个碳原子的烷基或具有1至4个碳原子的烷氧基; 并且R 3是氢，具有1至6个碳原子的烷基或烷氧基; 条件是R1和R2不同时为氨基或取代氨基。还公开了制备三偶氮染料的方法和含有三偶氮染料的含水墨水组合物。

8. 发明授权

US5160504A Method of dyeing leather with metal complex dyes comprised of metalizable azo compounds 失效
标题翻译：用金属化偶氮化合物组成的金属络合染料染色皮革的方法
公开(公告)号：US5160504A
公开(公告)日：1992-11-03
申请号：US783414
申请日：1991-10-28
申请人： Takashi Ono , Tatsuya Yagyu , Katsumi Fukuda , Minako Terasaki
发明人： Takashi Ono , Tatsuya Yagyu , Katsumi Fukuda , Minako Terasaki
IPC分类号： C09B45/24 , C09B45/38 , C09B62/095 , C09B69/00 , D06P3/32
CPC分类号： C09B62/095 , C09B45/24 , C09B45/38 , C09B69/007 , D06P3/3206 , D06P3/326
摘要： Use of metal complex dyes comprised of metalizable azo compounds to dye metal-tanned leather which makes possible good permeability and excellent color fastness to rubbing and color fastness to light.
摘要翻译：使用由可金属化偶氮化合物组成的金属络合染料来染色金属鞣革，这使得可能具有良好的透气性和优异的耐摩擦色牢度和耐光色牢度。

9. 发明授权

US07232480B2 Modified carbon black carbon black dispersion liquid and water base ink 有权
标题翻译：改性炭黑炭黑分散液和水基油墨
公开(公告)号：US07232480B2
公开(公告)日：2007-06-19
申请号：US10504218
申请日：2003-12-26
申请人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
发明人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
IPC分类号： C09D11/00
CPC分类号： B82Y30/00 , C01P2004/64 , C01P2006/12 , C01P2006/19 , C09C1/565 , C09D11/17 , C09D11/18 , C09D11/324 , Y10T428/24802
摘要： There are provided a carbon black according to which long-term stable storage is possible, clogging is not prone to occurring, and the OD value is high and hence printing with a deep black color is possible, or a carbon black that can be used in a water-based ink that is used in ink jet printer printing, that has low settleability and can thus be stored stably for a long period, for which clogging is not prone to occurring, and for which the reflection density is high and hence printing with a high printing density and a deep black color is possible, a carbon black dispersion having the carbon black dispersed therein, and a water-based ink containing the carbon black. An embodiment of a modified carbon black of the present invention is a modified carbon black obtained by carrying out oxidation treatment on a carbon black having a primary particle diameter of 11 to 18 nm, a BET specific surface area of at least 180 m2/g, a DBP oil absorption of at least 180 mL/100 g, and a value of the BET specific surface area (m2/g) divided by the DBP oil absorption (mL/100 g) of 0.75 to 1.3, and is characterized in that at least lactone groups and carboxyl groups are introduced onto the surface thereof, and the ratio of the mean particle diameter to the primary particle diameter is at least 8.5. Moreover, a carbon black dispersion and a water-based ink of the present invention contain this modified carbon black.
摘要翻译：提供了炭黑，根据该炭黑长期稳定的储存是可能的，堵塞不容易发生，并且OD值高，因此可以深黑色印刷，或可以用于黑色的炭黑用于喷墨打印机印刷中的水性油墨，其具有低沉降性并且因此可以长期稳定地储存，其中不易发生堵塞，并且反射密度高，因此用可以具有高的印刷密度和深黑色，分散有炭黑的炭黑分散体和含有炭黑的水性油墨。本发明的改性炭黑的一个实施方案是通过对一次粒径为11〜18nm，BET比表面积为180μm以上的炭黑进行氧化处理得到的改性炭黑， 2μg/ g，DBP吸油量至少为180mL / 100g，BET比表面积值（m 2 SUP / g / g）除以DBP吸油量（ mL / 100g）为0.75〜1.3，其特征在于，至少将内酯基和羧基引入其表面，平均粒径与一次粒径的比例为8.5以上。此外，本发明的炭黑分散体和水性油墨含有该改性炭黑。

10. 发明申请

US20050120914A1 Modified carbon black carbon black dispersion liquid and water base ink 有权
标题翻译：改性炭黑炭黑分散液和水基油墨
公开(公告)号：US20050120914A1
公开(公告)日：2005-06-09
申请号：US10504218
申请日：2003-12-26
申请人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
发明人： Masayuki Momose , Miharu Kanaya , Sohko Itoh , Tatsuya Yagyu
IPC分类号： B41J2/01 , B41M5/00 , B82Y20/00 , B82Y30/00 , C09C1/56 , C09C3/08 , C09D11/00 , C09D11/18 , C09D11/324 , C09D11/326 , C09D11/38 , C09D17/00
CPC分类号： B82Y30/00 , C01P2004/64 , C01P2006/12 , C01P2006/19 , C09C1/565 , C09D11/17 , C09D11/18 , C09D11/324 , Y10T428/24802
摘要： There are provided a carbon black according to which long-term stable storage is possible, clogging is not prone to occurring, and the OD value is high and hence printing with a deep black color is possible, or a carbon black that can be used in a water-based ink that is used in ink jet printer printing, that has low settleability and can thus be stored stably for a long period, for which clogging is not prone to occurring, and for which the reflection density is high and hence printing with a high printing density and a deep black color is possible, a carbon black dispersion having the carbon black dispersed therein, and a water-based ink containing the carbon black. An embodiment of a modified carbon black of the present invention is a modified carbon black obtained by carrying out oxidation treatment on a carbon black having a primary particle diameter of 11 to 18 nm, a BET specific surface area of at least 180 m2/g, a DBP oil absorption of at least 180 mL/100 g, and a value of the BET specific surface area (m2/g) divided by the DBP oil absorption (mL/100 g) of 0.75 to 1.3, and is characterized in that at least lactone groups and carboxyl groups are introduced onto the surface thereof, and the ratio of the mean particle diameter to the primary particle diameter is at least 8.5. Moreover, a carbon black dispersion and a water-based ink of the present invention contain this modified carbon black.
摘要翻译：提供了炭黑，根据该炭黑长期稳定的储存是可能的，堵塞不容易发生，并且OD值高，因此可以深黑色印刷，或可以用于黑色的炭黑用于喷墨打印机印刷中的水性油墨，其具有低沉降性并且因此可以长期稳定地储存，其中不易发生堵塞，并且反射密度高，因此用可以具有高的印刷密度和深黑色，分散有炭黑的炭黑分散体和含有炭黑的水性油墨。本发明的改性炭黑的一个实施方案是通过对一次粒径为11〜18nm，BET比表面积为180μm以上的炭黑进行氧化处理得到的改性炭黑， 2μg/ g，DBP吸油量至少为180mL / 100g，BET比表面积值（m 2 SUP / g / g）除以DBP吸油量（ mL / 100g）为0.75〜1.3，其特征在于，至少将内酯基和羧基引入其表面，平均粒径与一次粒径的比例为8.5以上。此外，本发明的炭黑分散体和水性油墨含有该改性炭黑。

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