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1. 发明授权

US09905856B1 Flexible and shape-conformal rope-shape alkali metal-sulfur batteries 有权
公开(公告)号：US09905856B1
公开(公告)日：2018-02-27
申请号：US15392213
申请日：2016-12-28
申请人： Aruna Zhamu , Hui He , Baofei Pan , Yu-Sheng Su , Bor Z Jang
发明人： Aruna Zhamu , Hui He , Baofei Pan , Yu-Sheng Su , Bor Z Jang
IPC分类号： H01M2/10 , H01M4/78 , H01M10/0525 , H01M10/054 , H01M10/0568 , H01M10/0569 , H01M10/0587 , H01M4/02
CPC分类号： H01M4/78 , H01M2/1055 , H01M2/1083 , H01M10/0525 , H01M10/054 , H01M10/0568 , H01M10/0569 , H01M10/0587 , H01M2004/025 , H01M2300/0025
摘要： Provided is a rope-shape alkali metal-sulfur battery having (a) a first electrode comprising a conductive porous rod and a mixture of a first electrode active material and a first electrolyte residing in pores of the first porous rod; (b) a porous separator wrapping around the first electrode to form a separator-protected first electrode; (c) a second electrode comprising a conductive porous rod having a mixture of a second electrode active material and a second electrolyte residing in pores of the second porous rod; wherein the separator-protected first electrode and the second electrode are combined to form a braid or a yarn; and (d) a protective sheath encasing the braid or yarn; wherein either the first or the second electrode is a cathode containing sulfur or a sulfur compound as a cathode active material and the battery has a rope shape having a length-to-diameter aspect ratio no less than 5.

2. 发明授权

US09564630B2 Anode active material-coated graphene sheets for lithium batteries and process for producing same 有权
标题翻译：用于锂电池的阳极活性材料涂覆石墨烯片及其制造方法
公开(公告)号：US09564630B2
公开(公告)日：2017-02-07
申请号：US13987566
申请日：2013-08-08
申请人： Yanbo Wang , Bor Z Jang , Hui He , Aruna Zhamu
发明人： Yanbo Wang , Bor Z Jang , Hui He , Aruna Zhamu
IPC分类号： H01M4/26 , H01M4/36 , H01M4/04 , H01M4/38 , H01M4/42 , H01M4/44 , H01M4/46 , H01M4/133 , H01M4/134 , H01M4/1393 , H01M4/1395 , H01M4/587 , H01M10/0525 , H01M4/62 , H01M4/485 , H01M4/02
CPC分类号： H01M4/366 , H01M4/0423 , H01M4/0426 , H01M4/0428 , H01M4/133 , H01M4/134 , H01M4/1393 , H01M4/1395 , H01M4/386 , H01M4/387 , H01M4/42 , H01M4/44 , H01M4/463 , H01M4/485 , H01M4/587 , H01M4/625 , H01M10/0525 , H01M2004/027 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： The present invention provides a process for producing a graphene-enhanced anode active material for use in a lithium battery. The process comprises (a) providing a continuous film of a graphene material into a deposition zone; (b) introducing vapor or atoms of a precursor anode active material into the deposition zone, allowing the vapor or atoms to deposit onto a surface of the graphene material film to form a sheet of an anode active material-coated graphene material; and (c) mechanically breaking this sheet into multiple pieces of anode active material-coated graphene; wherein the graphene material is in an amount of from 0.1% to 99.5% by weight and the anode active material is in an amount of at least 0.5% by weight, all based on the total weight of the graphene material and the anode active material combined.
摘要翻译：本发明提供一种用于生产用于锂电池的石墨烯增强的阳极活性材料的方法。该方法包括（a）将石墨烯材料的连续膜提供到沉积区中; （b）将前体负极活性物质的蒸汽或原子引入沉积区，允许蒸气或原子沉积在石墨烯材料膜的表面上以形成负极活性材料涂覆石墨烯材料的片材; 和（c）将该片材机械地破碎成多片阳极活性材料涂覆的石墨烯; 其中所述石墨烯材料的量为0.1重量％至99.5重量％，并且所述负极活性材料的量为至少0.5重量％，全部基于所述石墨烯材料和所述负极活性材料的总重量。

3. 发明申请

US20140363746A1 Lithium secondary batteries containing non-flammable quasi-solid electrolyte 有权
标题翻译：锂二次电池含有不易燃的准固体电解质
公开(公告)号：US20140363746A1
公开(公告)日：2014-12-11
申请号：US13986814
申请日：2013-06-10
申请人： Hui He , Bor Z. Jang , Yanbo Wang , Aruna Zhamu
发明人： Hui He , Bor Z. Jang , Yanbo Wang , Aruna Zhamu
IPC分类号： H01M10/056 , H01M10/052
CPC分类号： H01M10/052 , H01M4/136 , H01M4/5825 , H01M10/0525 , H01M10/0568 , H01M10/0569 , H01M12/08 , H01M2004/028 , H01M2300/0028 , Y02E60/122 , Y02E60/128 , Y02T10/7011
摘要： A rechargeable lithium cell comprising a cathode having a cathode active material, an anode having an anode active material, a porous separator electronically separating the anode and the cathode, a non-flammable quasi-solid electrolyte in contact with the cathode and the anode, wherein the electrolyte contains a lithium salt dissolved in a first organic liquid solvent with a concentration sufficiently high so that the electrolyte exhibits a vapor pressure less than 0.01 kPa when measured at 20° C., a flash point at least 20 degrees Celsius higher than the flash point of the first organic liquid solvent alone, a flash point higher than 150° C., or no flash point. This battery cell is non-flammable and safe, has a long cycle life, high capacity, and high energy density.
摘要翻译：一种可再充电锂电池，包括具有阴极活性材料的阴极，具有阳极活性材料的阳极，电子分离阳极和阴极的多孔隔板，与阴极和阳极接触的不可燃的准固体电解质，其中电解质含有溶解在浓度足够高的第一有机液体溶剂中的锂盐，使得当在20℃下测量时，电解质的蒸汽压力低于0.01kPa，闪点高于闪光灯的至少20摄氏度第一有机液体溶剂点，闪点高于150℃，或无闪点。该电池不易燃，安全，循环寿命长，容量大，能量密度高。

4. 发明授权

US09601805B2 Process for producing non-flammable quasi-solid electrolyte and electrolyte-separator for lithium battery applications 有权
公开(公告)号：US09601805B2
公开(公告)日：2017-03-21
申请号：US13987396
申请日：2013-07-22
申请人： Hui He , Bor Z Jang , Yanbo Wang , Aruna Zhamu
发明人： Hui He , Bor Z Jang , Yanbo Wang , Aruna Zhamu
IPC分类号： H01M2/16 , H01M10/056 , H01M10/0566 , H01M2/14 , H01M10/0569 , H01M10/0568
CPC分类号： H01M10/0566 , H01M2/145 , H01M2/162 , H01M10/0568 , H01M10/0569 , H01M2300/0025 , H01M2300/0028
摘要： A process for producing a separator-electrolyte layer for use in a lithium battery, comprising: (a) providing a porous separator; (b) providing a quasi-solid electrolyte containing a lithium salt dissolved in a first liquid solvent up to a first concentration no less than 3 M; and (c) coating or impregnating the separator with the electrolyte to obtain the separator-electrolyte layer with a final concentration≧the first concentration so that the electrolyte exhibits a vapor pressure less than 0.01 kPa when measured at 20° C., a vapor pressure less than 60% of that of the first liquid solvent alone, a flash point at least 20 degrees Celsius higher than a flash point of the first liquid solvent alone, a flash point higher than 150° C., or no detectable flash point. A battery using such a separator-electrolyte is non-flammable and safe, has a long cycle life, high capacity, and high energy density.

5. 发明申请

US20160308208A1 Magnesium-sulfur secondary battery containing a metal polysulfide-preloaded active cathode layer 有权
标题翻译：含有金属多硫化物预负载活性阴极层的镁硫二次电池
公开(公告)号：US20160308208A1
公开(公告)日：2016-10-20
申请号：US14545279
申请日：2015-04-17
申请人： Hui He , Aruna Zhamu , Bor Z Jang
发明人： Hui He , Aruna Zhamu , Bor Z Jang
IPC分类号： H01M4/58 , H01M10/0568 , H01M2/16 , H01M10/054 , H01M4/38 , H01M4/62
CPC分类号： H01M4/5815 , H01M2/1673 , H01M4/136 , H01M4/38 , H01M4/622 , H01M4/625 , H01M4/66 , H01M4/80 , H01M10/054 , H01M10/0568 , H01M2004/021 , H01M2004/028 , H01M2220/20 , H01M2300/0037
摘要： A rechargeable magnesium-sulfur cell comprising an anode layer, an electrolyte, a metal polysulfide-preloaded active cathode layer, wherein the active cathode layer comprises: (a) an integral porous structure having massive surfaces (specific surface area >100 m2/g) or pores with a size from 1.0 nm to 100 nm and wherein multiple particles; and (b) a metal polysulfide, MxSy, preloaded in the pores or deposited on the massive surfaces, wherein x is an integer from 1 to 3 and y is an integer from 1 to 10, and M is a metal element selected from an alkali metal, an alkaline metal, a transition metal, a metal from groups 13 to 17 of the periodic table, or a combination thereof. The metal polysulfide is in a form of solid-state thin coating or small particles with a thickness or diameter less than 50 nm.
摘要翻译：一种可充电的镁硫电池，包括阳极层，电解质，金属多硫化物预加载的活性阴极层，其中所述活性阴极层包括：（a）具有块状表面（比表面积> 100m 2 / g）的整体多孔结构，或尺寸为1.0nm至100nm的孔，并且其中多个颗粒; 和（b）金属多硫化物MxSy，其预载在孔中或沉积在块状表面上，其中x为1至3的整数，y为1至10的整数，M为选自碱金属的金属元素金属，碱金属，过渡金属，元素周期表第13至17族的金属，或其组合。金属多硫化物是固态薄涂层的形式或厚度或直径小于50nm的小颗粒。

6. 发明申请

US20160240841A1 Pre-sulfurized cathode for alkali metal-sulfur secondary battery and production process 审中-公开
标题翻译：碱金属硫二次电池预硫化阴极和生产工艺
公开(公告)号：US20160240841A1
公开(公告)日：2016-08-18
申请号：US14544765
申请日：2015-02-18
申请人： Hui He , Aruna Zhamu , Bor Z. Jang
发明人： Hui He , Aruna Zhamu , Bor Z. Jang
IPC分类号： H01M4/36 , H01M10/0525 , H01M4/04 , H01M4/38 , H01M4/587 , H01M4/1393
CPC分类号： H01M4/366 , H01M4/0447 , H01M4/0452 , H01M4/136 , H01M4/1397 , H01M4/38 , H01M4/625 , H01M10/052 , Y02T10/7011
摘要： A method of producing a pre-sulfurized active cathode layer for a rechargeable alkali metal-sulfur cell; the method comprising: (a) Preparing an integral layer of porous graphene structure having a specific surface area greater than 100 m2/g; (b) Preparing an electrolyte comprising a solvent and a sulfur source; (c) Preparing an anode; and (d) Bringing the integral layer and the anode in ionic contact with the electrolyte and imposing an electric current between the anode and the integral layer (serving as a cathode) to electrochemically deposit nano-scaled sulfur particles or coating on the graphene surfaces. The sulfur particles or coating have a thickness or diameter smaller than 20 nm (preferably 90% or even >95%).
摘要翻译：一种制备用于可再充电碱金属 - 硫电池的预硫化活性阴极层的方法; 该方法包括：（a）制备具有大于100m 2 / g的比表面积的多孔石墨烯结构的整体层; （b）制备包含溶剂和硫源的电解质; （c）制备阳极; 和（d）使整体层和阳极与电解质离子接触并在阳极和整体层（用作阴极）之间施加电流，以电化学沉积在石墨烯表面上的纳米级硫颗粒或涂层。硫颗粒或涂层具有小于20nm（优选<10nm，更优选<5nm或甚至<3nm）的厚度或直径，并且占据至少70％（优选> 90％或甚至> 95）的重量分数％）。

7. 发明授权

US09368831B2 Lithium secondary batteries containing non-flammable quasi-solid electrolyte 有权
标题翻译：锂二次电池含有不易燃的准固体电解质
公开(公告)号：US09368831B2
公开(公告)日：2016-06-14
申请号：US13986814
申请日：2013-06-10
申请人： Hui He , Bor Z Jang , Yanbo Wang , Aruna Zhamu
发明人： Hui He , Bor Z Jang , Yanbo Wang , Aruna Zhamu
IPC分类号： H01M10/056 , H01M10/052 , H01M10/0569 , H01M4/136 , H01M4/58 , H01M10/0525 , H01M10/0568 , H01M12/08 , H01M4/02
CPC分类号： H01M10/052 , H01M4/136 , H01M4/5825 , H01M10/0525 , H01M10/0568 , H01M10/0569 , H01M12/08 , H01M2004/028 , H01M2300/0028 , Y02E60/122 , Y02E60/128 , Y02T10/7011
摘要： A rechargeable lithium cell comprising a cathode having a cathode active material, an anode having an anode active material, a porous separator electronically separating the anode and the cathode, a non-flammable quasi-solid electrolyte in contact with the cathode and the anode, wherein the electrolyte contains a lithium salt dissolved in a first organic liquid solvent with a concentration sufficiently high so that the electrolyte exhibits a vapor pressure less than 0.01 kPa when measured at 20° C., a flash point at least 20 degrees Celsius higher than the flash point of the first organic liquid solvent alone, a flash point higher than 150° C., or no flash point. This battery cell is non-flammable and safe, has a long cycle life, high capacity, and high energy density.
摘要翻译：一种可再充电锂电池，包括具有阴极活性材料的阴极，具有阳极活性材料的阳极，电子分离阳极和阴极的多孔隔板，与阴极和阳极接触的不可燃的准固体电解质，其中电解质含有溶解在浓度足够高的第一有机液体溶剂中的锂盐，使得当在20℃下测量时，电解质的蒸汽压力低于0.01kPa，闪点高于闪光灯的至少20摄氏度第一有机液体溶剂点，闪点高于150℃，或无闪点。该电池不易燃，安全，循环寿命长，容量大，能量密度高。

8. 发明授权

US09059481B2 Non-flammable quasi-solid electrolyte and non-lithium alkali metal or alkali-ion secondary batteries containing same 有权
标题翻译：不易燃的准固体电解质和含有其的非锂碱金属或碱金属二次电池
公开(公告)号：US09059481B2
公开(公告)日：2015-06-16
申请号：US13987764
申请日：2013-08-30
申请人： Hui He , Bor Z Jang , Yanbo Wang , Aruna Zhamu
发明人： Hui He , Bor Z Jang , Yanbo Wang , Aruna Zhamu
IPC分类号： H01M6/18 , H01M10/0568 , H01M10/05 , H01M4/40
CPC分类号： H01M10/0568 , H01M4/40 , H01M4/405 , H01M4/587 , H01M10/05 , H01M10/054 , H01M10/0569
摘要： A non-flammable quasi-solid electrolyte and a rechargeable non-lithium alkali metal cell containing this electrolyte. The electrolyte comprises an alkali metal salt dissolved in an organic liquid solvent with a concentration higher than 2.5 M (preferably >3.5 M) or a molecular ratio greater than 0.2 (preferably >0.3), wherein the alkali metal is selected from Na, K, a combination of Na and K, or a combination of Na and/or K with Li. The alkali metal salt concentration is sufficiently high so that the electrolyte exhibits a vapor pressure
摘要翻译：不可燃的准固体电解质和含有这种电解质的可再充电的非锂碱金属电池。电解质包含溶解在浓度高于2.5M（优选> 3.5M）或分子比大于0.2（优选> 0.3））的有机液体溶剂中的碱金属盐，其中碱金属选自Na，K， Na和K的组合，或Na和/或K与Li的组合。碱金属盐浓度足够高，使得当在20℃下测量时，电解质的蒸气压<0.01kPa，当单独测量时，有机溶剂的蒸气压的蒸汽压<60％，至少闪点当单独测量时，有机液体溶剂的闪点高20摄氏度，闪点高于150℃，或无可检测的闪点。

9. 发明申请

US20150044565A1 Anode active material-coated graphene sheets for lithium batteries and process for producing same 有权
标题翻译：用于锂电池的阳极活性材料涂覆石墨烯片及其制造方法
公开(公告)号：US20150044565A1
公开(公告)日：2015-02-12
申请号：US13987566
申请日：2013-08-08
申请人： Yanbo Wang , Bor Z. Jang , Hui He , Aruna Zhamu
发明人： Yanbo Wang , Bor Z. Jang , Hui He , Aruna Zhamu
IPC分类号： H01M4/36 , H01M4/52 , H01M4/04 , H01M4/38 , H01M10/28 , H01M4/44 , H01M4/46 , H01M4/485 , H01M4/58 , H01M4/62 , H01M4/42
CPC分类号： H01M4/366 , H01M4/0423 , H01M4/0426 , H01M4/0428 , H01M4/133 , H01M4/134 , H01M4/1393 , H01M4/1395 , H01M4/386 , H01M4/387 , H01M4/42 , H01M4/44 , H01M4/463 , H01M4/485 , H01M4/587 , H01M4/625 , H01M10/0525 , H01M2004/027 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： The present invention provides a process for producing a graphene-enhanced anode active material for use in a lithium battery. The process comprises (a) providing a continuous film of a graphene material into a deposition zone; (b) introducing vapor or atoms of a precursor anode active material into the deposition zone, allowing the vapor or atoms to deposit onto a surface of the graphene material film to form a sheet of an anode active material-coated graphene material; and (c) mechanically breaking this sheet into multiple pieces of anode active material-coated graphene; wherein the graphene material is in an amount of from 0.1% to 99.5% by weight and the anode active material is in an amount of at least 0.5% by weight, all based on the total weight of the graphene material and the anode active material combined.
摘要翻译：本发明提供一种用于生产用于锂电池的石墨烯增强的阳极活性材料的方法。该方法包括（a）将石墨烯材料的连续膜提供到沉积区中; （b）将前体负极活性物质的蒸汽或原子引入沉积区，允许蒸气或原子沉积在石墨烯材料膜的表面上以形成负极活性材料涂覆石墨烯材料的片材; 和（c）将该片材机械地破碎成多片阳极活性材料涂覆的石墨烯; 其中所述石墨烯材料的量为0.1重量％至99.5重量％，并且所述负极活性材料的量为至少0.5重量％，全部基于所述石墨烯材料和所述负极活性材料的总重量。

10. 发明申请

US20150044556A1 Cathode active material-coated discrete graphene sheets for lithium batteries and process for producing same 有权
标题翻译：用于锂电池的阴极活性材料涂层离散石墨烯片及其制造方法
公开(公告)号：US20150044556A1
公开(公告)日：2015-02-12
申请号：US13987567
申请日：2013-08-08
申请人： Yanbo Wang , Bor Z. Jang , Hui He , Aruna Zhamu
发明人： Yanbo Wang , Bor Z. Jang , Hui He , Aruna Zhamu
IPC分类号： H01M4/36 , H01M4/04
CPC分类号： H01M4/366 , H01M4/04 , H01M4/0421 , H01M4/13 , H01M4/139 , H01M4/625 , H01M10/056 , H01M2004/028 , Y10T156/1075
摘要： The present invention provides a cathode (positive electrode) of a lithium battery and a process for producing this cathode. The electrode comprises a cathode active material-coated graphene sheet and the graphene sheet has two opposed parallel surfaces, wherein at least 50% area (preferably >80%) of one of the two surfaces is coated with a cathode active material coating. The graphene material is in an amount of from 0.1% to 99.5% by weight and the cathode active material is in an amount of at least 0.5% by weight (preferably >80% and more preferably >90%), all based on the total weight of the graphene material and the cathode active material combined. The cathode active material is preferably an inorganic material, an organic or polymeric material, a metal oxide/phosphate/sulfide, or a combination thereof. The invention also provides a lithium battery, including a lithium-ion, lithium-metal, or lithium-sulfur battery.
摘要翻译：本发明提供锂电池的阴极（正电极）及其制造方法。电极包括阴极活性材料涂覆的石墨烯片，并且石墨烯片具有两个相对的平行表面，其中两个表面中的一个表面的至少50％面积（优选> 80％）涂覆有阴极活性材料涂层。石墨烯材料的量为0.1重量％至99.5重量％，正极活性物质的量为至少0.5重量％（优选> 80重量％，更优选> 90重量％），均基于总量石墨烯材料和阴极活性材料的重量相结合。阴极活性材料优选为无机材料，有机或聚合材料，金属氧化物/磷酸盐/硫化物或其组合。本发明还提供一种锂电池，其包括锂离子，锂金属或锂硫电池。

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