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    • 3. 发明授权
    • Package dye process
    • 包装染色工艺
    • US3871821A
    • 1975-03-18
    • US42829973
    • 1973-12-26
    • DOW CHEMICAL CO
    • WINN WILLIAM DDUNN JR JAMES L
    • D06B9/02B05C8/02
    • D06B9/02
    • A method for kier-dyeing packaged yarn in a discontinuous manner employing a chlorinated solvent as the sole fluid to evacuate the air from the kier and to heat the yarn to achieve dye fixation temperature as the principal vehicle for the dye formulation, and as the means for recovering residual solvent from the dyed yarn packages and kier. The method is practiced by subjecting a kier, which has been loaded with packages of yarn to be dyed, to an initial vacuum followed by introduction of vapors of a chlorinated solvent into the bottom of the kier until the kier is filled with such vapors and substantially all air has been evacuated, discontinuing the exhaustion under vacuum but continuing the introduction of vapors to the kier until the contents achieve the temperature of the vapors, introducing a solvent dyebath into the kier and circulating the dyebath through the kier until the dyebath is spent, removing the spent dyebath from the kier under the pressure of solvent vapors, and circulating the vapors to a heater to superheat the vapors, returning the vapors to the kier, condensing vapors in excess of those necessary to fill the kier and superheater, continuing the circulation of vapors until the solvent is substantially completely removed from the yarn in the kier. Residual solvent is removed by evacuating and purging the kier with an inert gas. Thereafter, the kier is cooled to enable removal of the yarn packages. Finally, solvent is recovered from the spent dyebath and returned to storage.