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1. 发明授权

US06559271B2 Method for producing polyesters with a reduced content of free acetaldehyde 有权
公开(公告)号：US06559271B2
公开(公告)日：2003-05-06
申请号：US09951177
申请日：2001-09-13
申请人： Eckehart Schaaf , Gerald Rafler , Rainer Hagen
发明人： Eckehart Schaaf , Gerald Rafler , Rainer Hagen
IPC分类号： B29D2200
CPC分类号： C08G63/85 , B29C2045/1883 , B29K2105/0002 , C08G63/183 , C08G63/78 , C08G63/90 , Y10T428/1352
摘要： The invention relates to a method for producing polyesters with a reduced content of free acetaldehyde from terephthalic acid and ethylene glycol via a catalyzed polycondensation in the melt and also the use of this method. The method is based thereby on the usage of highly active polycondensation catalysts, on the deactivation of these catalysts by the addition of phosphorous-containing inhibitors and the addition of acetaldehyde-bonding substances. The entire polycondensation is thereby implemented at temperatures beneath 280° C.

2. 发明授权

US6013756A Process for producing polyesters using titanium-containing catalyst-inhibitor combinations 失效
标题翻译：使用含钛催化剂 - 抑制剂组合制备聚酯的方法
公开(公告)号：US6013756A
公开(公告)日：2000-01-11
申请号：US973042
申请日：1998-02-12
申请人： Rainer Hagen , Eckehart Schaaf , Heinz Zimmermann
发明人： Rainer Hagen , Eckehart Schaaf , Heinz Zimmermann
IPC分类号： C08G63/82 , C08G63/00
CPC分类号： C08G63/82
摘要： The invention relates to a process for producing polyesters, especially high-molecular polyethylene terephthalate (PET) using titanium-containing catalyst-inhibitor combinations.
摘要翻译： PCT No.PCT / DE96 / 00932 Sec。 371日期1998年2月12日 102（e）1998年2月12日PCT PCT 1996年5月22日PCT公布。第WO96 / 37534号公报日期1996年11月28日本发明涉及使用含钛催化剂 - 抑制剂组合制备聚酯，特别是高分子量聚对苯二甲酸乙二醇酯（PET）的方法。

3. 发明授权

US08957229B2 Method for the production of a mixture of lactide derivatives 有权
标题翻译：制备丙交酯衍生物混合物的方法
公开(公告)号：US08957229B2
公开(公告)日：2015-02-17
申请号：US13060553
申请日：2009-08-28
申请人： Rainer Hagen , Adam B. Verweij , Udo Muhlbauer , Joachim Schulze , Wolfgang Tietz , Olga Renate Göhler
发明人： Rainer Hagen , Adam B. Verweij , Udo Muhlbauer , Joachim Schulze , Wolfgang Tietz , Klaus-Dieter Göhler
IPC分类号： C07D319/00 , C07D319/12 , C07B55/00
CPC分类号： C07D319/12 , C07B55/00
摘要： A mixture of cyclic diesters derived from lactic acid and in cases a mixture of a racemate of dilactide may be produced in several different processes. In some instances, the process can thereby start from the corresponding alpha-hydroxycarboxylic acids, the corresponding cyclic diesters or oligomers of the corresponding alpha-hydroxycarboxylic acids.
摘要翻译：衍生自乳酸的环状二酯的混合物和在外消旋物的混合物的情况下可以以几种不同的方法制备。在一些情况下，该方法可以由相应的α-羟基羧酸，相应的α-羟基羧酸的相应的环状二酯或低聚物开始。

4. 发明授权

US08399602B2 Polymerisation reactor, polymerisation device, method for producing bio-degradeable polyester and uses 有权
标题翻译：聚合反应器，聚合装置，生物可降解聚酯的生产方法和用途
公开(公告)号：US08399602B2
公开(公告)日：2013-03-19
申请号：US12676299
申请日：2008-08-25
申请人： Rainer Hagen , Udo Muhlbauer
发明人： Rainer Hagen , Udo Muhlbauer
IPC分类号： C08G63/08 , C08F2/00
CPC分类号： B01J19/2415 , B01J19/006 , B01J19/18 , B01J19/1862 , B01J19/245 , B01J2219/00164 , B01J2219/00166 , B01J2219/00768 , B01J2219/0077 , B01J2219/00774 , B01J2219/00777 , C08G63/08 , C08G63/785
摘要： The present invention relates to a polymerization reactor for continuous polymerization, the reactor being constructed in two stages and comprising a prepolymerization stage which is configured as a stirred vessel or as a loop-type bubble column and also a main polymerization stage which is configured as a tubular reactor. Furthermore, the present invention relates to a method for the production of biodegradable polyester, in particular polylactide, the reactor according to the invention being used. Likewise, the invention relates to a polymerization device which comprises further components in addition to the polymerization reactor.
摘要翻译：本发明涉及一种用于连续聚合的聚合反应器，该反应器分为两个阶段构成，包括预聚合阶段，其被配置为搅拌容器或循环式鼓泡塔，以及主要聚合阶段，其被配置为管状反应器。此外，本发明涉及用于生产可生物降解的聚酯，特别是聚丙交酯的方法，所使用的根据本发明的反应器。同样地，本发明涉及除了聚合反应器之外还包含其它组分的聚合装置。

5. 发明授权

US07259227B2 Method for continuous production of high-molecular weight polyesters and device for implementation of the method 有权
标题翻译：连续生产高分子量聚酯的方法及其实施方法
公开(公告)号：US07259227B2
公开(公告)日：2007-08-21
申请号：US11373937
申请日：2006-03-13
申请人： Eike Schulz Van Endert , Rainer Hagen , Thomas Hille , Christian Atlas , Ulrich Thiele
发明人： Eike Schulz Van Endert , Rainer Hagen , Thomas Hille , Christian Atlas , Ulrich Thiele
IPC分类号： C08G63/02
CPC分类号： C08G63/785 , B01J19/1887 , B01J2219/00085 , B01J2219/00087 , B01J2219/0011 , B01J2219/00166 , C08G63/78
摘要： The invention relates to a method for producing high-molecular weight polyesters, such as e.g. polyethylene terephthalate (PET), polybutylene terephthalate (PBT), polynaphthalene terephthalate (PEN), polytrimethylene terephthalate (PTT) and/or polyesters of other dicarboxylic acids and diols including copolymers thereof. The invention relates likewise to a device for implementing this method. The latter concerns a single-stage tower reactor with which a method, comprising only two reactors, is made available for the total process.
摘要翻译：本发明涉及一种生产高分子量聚酯的方法，例如，聚对苯二甲酸乙二醇酯（PET），聚对苯二甲酸丁二醇酯（PBT），聚萘二甲酸对苯二甲酸酯（PEN），聚对苯二甲酸丙二醇酯（PTT）和/或其他二羧酸和二醇的聚酯，包括它们的共聚物。本发明同样涉及用于实现该方法的装置。后者涉及单级塔式反应器，其中仅包括两个反应器的方法可用于整个方法。

6. 发明申请

US20060141395A1 Metal complexes as light-absorbing compounds in the information layer of optical data carriers 审中-公开
标题翻译：金属络合物作为光学数据载体的信息层中的吸光化合物
公开(公告)号：US20060141395A1
公开(公告)日：2006-06-29
申请号：US10522476
申请日：2003-07-15
申请人： Horst Berneth , Friedrich-Karl Bruder , Rainer Hagen , Karin Hassenruck , Serguei Kostromine , Christa Kruger , Timo Meyer-Friedrichsen , Rafael Oser , Josef-Walter Stawitz
发明人： Horst Berneth , Friedrich-Karl Bruder , Rainer Hagen , Karin Hassenruck , Serguei Kostromine , Christa Kruger , Timo Meyer-Friedrichsen , Rafael Oser , Josef-Walter Stawitz
IPC分类号： G11B7/24 , C07F15/00
CPC分类号： C09B45/00
摘要： Novel metal complexes for optical data carriers which comprise a preferably transparent substrate which may, if desired, have preivously been coated with one or more reflection layers and to whose surface a light-writable information layer, if desired one or more reflection layers and if desired a protective layer or a further substrate or a covering layer have been applied and which can be written on and read by means of blue or red light, preferably laser light, where the information layer comprises a light-absorbent compound and, if desired, a binder, characterized in that at least one such metal complex is used as light-absorbent compound, have been found.
摘要翻译：用于光学数据载体的新型金属络合物，其包含优选透明的基底，如果需要，其可以预先涂覆有一个或多个反射层，并且如果需要，可以根据需要在其表面上具有可光写信息层（如果需要）一个或多个反射层，如果需要已经施加了保护层或另外的基底或覆盖层，并且可以通过蓝色或红色光（优选地激光）将其写入和读取，其中信息层包含吸光性化合物，并且如果需要，可以使用粘合剂，其特征在于，使用至少一种这样的金属络合物作为吸光性化合物。

7. 发明申请

US20050094958A1 Layer structure and optical waveguide sensor based on photoaddressable polymers 失效
标题翻译：基于光可寻址聚合物的层结构和光波导传感器
公开(公告)号：US20050094958A1
公开(公告)日：2005-05-05
申请号：US10969814
申请日：2004-10-20
申请人： Ingmar Dorn , Thomas Bieringer , Rainer Hagen , Serguei Kostromine , Rino Kunz
发明人： Ingmar Dorn , Thomas Bieringer , Rainer Hagen , Serguei Kostromine , Rino Kunz
IPC分类号： G01N21/77 , G02B1/04 , G02B6/10
CPC分类号： G01N21/7703 , G01N21/648 , G02B1/045
摘要： An optical layer structure having at least two layers and also a sensor based on this layer structure are described. The layer structure comprises at least a substrate layer and at least one (light) waveguide layer and a coupling element for the coupling of the optical beam, the layer adjacent to the waveguide layer having a smaller refractive index than the waveguide layer, and at least one layer consisting of a photoaddressable polymer.
摘要翻译：描述了具有至少两层的光学层结构以及基于该层结构的传感器。该层结构包括至少一个衬底层和至少一个（光）波导层和用于耦合光束的耦合元件，与波导层相邻的具有比波导层更小的折射率的层，并且至少一层由可光寻址聚合物组成。

8. 发明授权

US06274696B1 Continuous process for the production of segmented elastomer polyester copolymer 有权
标题翻译：用于生产分段弹性体聚酯共聚物的连续工艺
公开(公告)号：US06274696B1
公开(公告)日：2001-08-14
申请号：US09659740
申请日：2000-09-11
申请人： Geert I. V. Bonte , Rainer Hagen , Eike Schulz Van Endert
发明人： Geert I. V. Bonte , Rainer Hagen , Eike Schulz Van Endert
IPC分类号： C08G6300
CPC分类号： C08G63/78 , C08G63/672
摘要： The invention relates to a continuous process for the preparation of segmented elastomer polyester copolymers that shows greater flexibility with respect to the types and amounts of product to be produced than the known processes. The flexibility is achieved by splitting up a low-molecular PBT product stream from a continuous PBT process and partly using it as feed for the transesterification reaction with the polyalkyleneoxide glycol yielding soft segments to form a low-molecular segmented polyester copolymer, which is subsequently further condensed in the melt or optionally in the solid phase to form high-molecular segmented polyester copolymers. Even greater flexibility can be obtained by operating several parallel production lines for segmented polyester copolymer. Fluctuations in the types of copolyester product to be produced and the amounts thereof are accommodated predominantly in the polycondensation step of the PBT production.
摘要翻译：本发明涉及用于制备分段弹性体聚酯共聚物的连续方法，其显示出比已知方法要生产的产品的类型和数量更大的灵活性。通过将低分子PBT产物流来自连续的PBT方法，并且部分地将其用作与聚环氧烷二醇的酯交换反应的进料，产生软链段以形成低分子链段聚酯共聚物，随后在熔体中或任选地在固相中进一步浓缩，分子分段的聚酯共聚物。通过操作多个平行的分段聚酯共聚物生产线可以获得更大的柔韧性。待生产的共聚酯产物类型和其用量的影响主要适用于PBT生产的缩聚步骤。

9. 发明授权

US4492808A Method for separating ethanol from an ethanol containing solution 失效
标题翻译：从含乙醇溶液中分离乙醇的方法
公开(公告)号：US4492808A
公开(公告)日：1985-01-08
申请号：US600301
申请日：1984-04-13
申请人： Rainer Hagen , Jurgen Hartwig
发明人： Rainer Hagen , Jurgen Hartwig
IPC分类号： C07C29/86 , C07C29/76 , C07C29/78 , C07C31/08
CPC分类号： C07C29/86 , Y02P20/544
摘要： A process is disclosed for the separation of ethanol from an ethanol containing water solution, wherein the ethanol containing solution is extracted by means of a solvent which is in the liquid or supercritical state, the ethanol containing solvent phase is separated into its components by being conducted over an adsorption medium without changing the pressure or temperature, and the ethanol is recovered by treating the ethanol containing adsorption medium with the solvent used for the extraction at a pressure from 1 to 30 bar and at a temperature from 150.degree. to 300.degree. C.
摘要翻译：公开了一种用于从含乙醇的水溶液中分离乙醇的方法，其中含有乙醇的溶液通过处于液体或超临界状态的溶剂萃取，含乙醇的溶剂相通过进行的方式分离成其组分在不改变压力或温度的情况下通过吸附介质吸收乙醇，通过在1至30巴的压力和150至300℃的温度下用用于萃取的溶剂处理含乙醇的吸附介质来回收乙醇。

10. 发明授权

US08569517B2 Cleaning device for separating dilactide from mixtures, polymerisation device, method for separating dilactide from mixtures and use thereof 有权
公开(公告)号：US08569517B2
公开(公告)日：2013-10-29
申请号：US12676214
申请日：2008-08-25
申请人： Rainer Hagen , Udo Muhlbauer
发明人： Rainer Hagen , Udo Muhlbauer
IPC分类号： C07D319/00
CPC分类号： C08G63/08 , B01D3/14 , B01D3/141 , C08G63/785
摘要： The present invention relates to a device for separating a biodegradable, intermolecular cyclic diester of an alpha-hydroxycarboxylic acid from material mixtures which contain in addition the alpha-hydroxycarboxylic acid of the diester corresponding thereto. In particular, the diester is thereby dilactide and the acid lactic acid. Furthermore, the present invention relates to a method for separating dilactide from material mixtures, which is based on a modified, distillative method. In addition, the present invention describes a polymerization device, in particular for preparing polylactide. Likewise, purposes of use of both the devices and of the method are indicated.

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