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1. 发明授权

US6015458A Process for the preparation of highly chromatic perylene pigments 有权
标题翻译：制备高色苝颜料的方法
公开(公告)号：US6015458A
公开(公告)日：2000-01-18
申请号：US211349
申请日：1998-12-15
申请人： Gregory R. Schulz , Michael J. Greene
发明人： Gregory R. Schulz , Michael J. Greene
IPC分类号： C09B67/20 , C07D221/14 , C07D471/04 , C09B3/18 , C09B5/62 , C07D221/00 , C07D309/00 , C09B3/14
CPC分类号： C07D221/14 , C07D471/04 , C09B5/62
摘要： This invention relates to a process for preparing perylene pigment compositions by reaction of(a) a perylene tetracarboxylic compound;(b) about 0.01 to about 20% by weight, relative to the perylene tetracarboxylic compound, of a non-pigmentary cyclic anhydride or imide of formula (I) ##STR1## wherein W is O or NR.sup.1 (where R.sup.1 is hydrogen, a metal, or optionally substituted alkyl, cycloalkyl, aralkyl, or aryl), R.sup.2, R.sup.3, and R.sup.4 are various combinations of substituents and/or fused-on rings, and the dotted line is an optional double bond representing R.sup.2 --C.dbd.C--R.sup.3 or R.sup.3 --C.dbd.C--R.sup.4 ; and(c) ammonia or a primary alkyl, aralkyl, or aryl amine;optionally in the presence of(d) a solvent and/or(e) one or more dispersants.
摘要翻译：本发明涉及通过（a）苝四羧酸化合物的反应制备苝颜料组合物的方法; （b）相对于苝四羧酸化合物，其中W为O或NR 1（其中R 1为氢，金属或任选地（其中R 1为氢）的式（I）的非颜料环状酸酐或酰亚胺为约0.01至约20重量％取代的烷基，环烷基，芳烷基或芳基），R2，R3和R4是取代基和/或稠合环的各种组合，虚线是任选的双键，表示R2-C = C-R3或R3- C = C-R4; 和（c）氨或伯烷基，芳烷基或芳基胺; 任选地在（d）溶剂和/或（e）一种或多种分散剂的存在下。

2. 发明授权

US06224665B1 Process for the preparation of highly chromatic perylene pigments 失效
标题翻译：制备高色苝颜料的方法
公开(公告)号：US06224665B1
公开(公告)日：2001-05-01
申请号：US09491493
申请日：2000-01-25
申请人： Gregory R. Schulz , Michael J. Greene
发明人： Gregory R. Schulz , Michael J. Greene
IPC分类号： C09B318
CPC分类号： C07D207/26 , C09B57/08 , C09B67/0034
摘要： This invention relates to a process for preparing perylene pigment compositions by reaction of (a) a perylene tetracarboxylic compound; (b) about 0.01 to about 20% by weight, relative to the perylene tetracarboxylic compound, of a non-pigmentary cyclic anhydride or imide of formula (I) wherein W is O or NR1 (where R1 is hydrogen, a metal, or optionally substituted alkyl, cycloalkyl, aralkyl, or aryl), R2, R3, and R4 are various combinations of substituents and/or fused-on rings, and the dotted line is an optional double bond representing R2−C=C—R3; (c) ammonia or a primary alkyl, aralkyl, or aryl amine; optionally in the presence of (d) a solvent and/or (e) one or more dispersants.
摘要翻译：本发明涉及通过（a）苝四羧酸化合物的反应制备苝颜料组合物的方法;（b）相对于苝四羧酸化合物为非颜料环状酸酐或酰亚胺的约0.01至约20重量％其中W是O或NR 1（其中R 1是氢，金属或任选取代的烷基，环烷基，芳烷基或芳基）的式（I），R 2，R 3和R 4是取代基和/或稠合的各种组合并且虚线是表示R2-C = C-R3的任选的双键;（c）氨或伯烷基，芳烷基或芳基胺;任选地在（d）溶剂和/或）一种或多种分散剂。

3. 发明授权

US6143068A Process for the preparation of highly chromatic perylene pigments 有权
标题翻译：制备高色苝颜料的方法
公开(公告)号：US6143068A
公开(公告)日：2000-11-07
申请号：US491600
申请日：2000-01-25
申请人： Gregory R. Schulz , Michael J. Greene
发明人： Gregory R. Schulz , Michael J. Greene
IPC分类号： C09B5/62 , C07D207/26 , C09B3/18 , C09B57/08 , C09B67/22 , C09B67/20 , C07D307/26
CPC分类号： C07D207/26 , C09B57/08 , C09B67/0034
摘要： This invention relates to a process for preparing perylene pigment compositions by reaction of(a) a perylene tetracarboxylic compound;(b) about 0.01 to about 20% by weight, relative to the perylene tetracarboxylic compound, of a non-pigmentary cyclic anhydride or imide of formula (I) ##STR1## wherein W is O or NR' (where R.sup.1 is hydrogen, a metal, or optionally substituted alkyl, cycloalkyl, aralkyl, or aryl), R.sup.2, R.sup.3, and R.sup.4 are various combinations of substituents and/or fused-on rings, and the dotted line is an optional double bond representing R.sup.2 --C.dbd.C--R.sup.3 ;(c) ammonia or a primary alkyl, aralkyl, or aryl amine; optionally in the presence of(d) a solvent and/or(e) one or more dispersants.
摘要翻译：本发明涉及通过（a）苝四羧酸化合物的反应制备苝颜料组合物的方法; （b）相对于苝四羧酸化合物，其中W是O或NR'（其中R 1是氢，金属或其中的）的式（I）的非颜料环状酸酐或酰亚胺的约0.01至约20重量％任选取代的烷基，环烷基，芳烷基或芳基），R 2，R 3和R 4是取代基和/或稠合环的各种组合，虚线是任选的表示R2-C = C-R3的双键; （c）氨或伯烷基，芳烷基或芳基胺; 任选地在（d）溶剂和/或（e）一种或多种分散剂的存在下。

4. 发明授权

US06410619B2 Method for conditioning organic pigments 有权
标题翻译：有机颜料调理方法
公开(公告)号：US06410619B2
公开(公告)日：2002-06-25
申请号：US09444589
申请日：1999-11-22
申请人： Michael J. Greene , Patrick F. McIntyre , James G. King , Gregory R. Schulz , Karyn B. Visscher
发明人： Michael J. Greene , Patrick F. McIntyre , James G. King , Gregory R. Schulz , Karyn B. Visscher
IPC分类号： C09B6750
CPC分类号： C09B67/0063 , C09B67/0002 , C09B67/0022
摘要： This invention relates to a process for preparing conditioned organic pigments by (a) milling a mixture comprising: (1) one or more crude organic pigments; (2) at least about 0.1% by weight, relative to the organic pigment, of one or more acrylic copolymer dispersants; and (3) 0 to about 100 parts by weight, relative to the organic pigment, of a milling liquid in which the organic pigment is substantially insoluble; and (b) isolating the milled organic pigment.
摘要翻译：本发明涉及通过（a）研磨混合物来制备调节的有机颜料的方法，所述混合物包含：（1）一种或多种粗有机颜料;（2）相对于有机颜料，至少约0.1重量％更多丙烯酸共聚物分散剂; 和（3）相对于有机颜料0至约100重量份的有机颜料基本上不溶的研磨液体; 和（b）分离研磨的有机颜料。

5. 发明授权

US6039769A Process for the preparation of highly chromatic perylene pigments 有权
公开(公告)号：US6039769A
公开(公告)日：2000-03-21
申请号：US211728
申请日：1998-12-15
申请人： Gregory R. Schulz , Michael J. Greene
发明人： Gregory R. Schulz , Michael J. Greene
IPC分类号： C09B5/62 , C07D207/26 , C09B3/18 , C09B57/08 , C09B67/22 , C09B67/20
CPC分类号： C07D207/26 , C09B57/08 , C09B67/0034
摘要： This invention relates to a process for preparing perylene pigment compositions by reaction of(a) a perylene tetracarboxylic compound;(b) about 0.01 to about 20% by weight, relative to the perylene tetracarboxylic compound, of a non-pigmentary cyclic anhydride or imide of formula (I) ##STR1## wherein W is O or NR.sup.1 (where R.sup.1 is hydrogen, a metal, or optionally substituted alkyl, cycloalkyl, aralkyl, or aryl), R.sup.2, R.sup.3, and R.sup.4 are various combinations of substituents and/or fused-on rings, and the dotted line is an optional double bond representing R.sup.2 --C.dbd.C--R.sup.3 ;(c) ammonia or a primary alkyl, aralkyl, or aryl amine; optionally in the presence of(d) a solvent and/or(e) one or more dispersants.

6. 发明授权

US06403797B1 Process for the preparation of perylene pigments 有权
标题翻译：苝颜料的制备方法
公开(公告)号：US06403797B1
公开(公告)日：2002-06-11
申请号：US09747058
申请日：2000-12-22
申请人： Charles W. Sandefur , Brian L. Thompson , Michael J. Greene , Gregory R. Schulz
发明人： Charles W. Sandefur , Brian L. Thompson , Michael J. Greene , Gregory R. Schulz
IPC分类号： C07D22100
CPC分类号： C09B5/62 , C09B67/0033
摘要： This invention relates to a process for preparing perylene pigment compositions by (a) reacting, at a temperature of less than about 25° C., a mixture of (1) a perylene tetracarboxylic compound, (2) at least about 0.1% by weight, relative to the perylene tetracarboxylic compound, of a surfactant of formula (I) wherein R1, R2, R3, X, Y, Z, and Z′ are defined herein, (3) an equivalent excess, relative to the amount of the perylene tetracarboxylic compound, of ammonia or a primary amine RA—NH2, wherein RA is defined herein, and (4) optionally, a solvent, to form a perylene intermediate; (b) heating the perylene intermediate at a temperature of about 50° C. to about 250° C., optionally in the presence of certain non-pigmentary cyclic anhydrides or imides and/or solvents; and (c) collecting the perylene pigment composition.
摘要翻译：本发明涉及一种制备苝颜料组合物的方法，该方法是（a）在小于约25℃的温度下使（1）苝四羧酸化合物，（2）至少约0.1重量％相对于苝四羧酸化合物，其中R 1，R 2，R 3，X，Y，Z和Z'在本文中定义的式（I）表面活性剂，（3）相对于苝的量的当量过量四羧酸化合物，氨或伯胺RA-NH 2，其中RA在本文中定义，和（4）任选的溶剂，以形成苝中间体;（b）在约50℃的温度下加热苝中间体至约250℃，任选地在某些非颜料环状酸酐或酰亚胺和/或溶剂的存在下进行; 和（c）收集苝颜料组合物。

7. 发明授权

US6153764A Process for the preparation of highly chromatic perylene pigments 失效
标题翻译：制备高色苝颜料的方法
公开(公告)号：US6153764A
公开(公告)日：2000-11-28
申请号：US491499
申请日：2000-01-25
申请人： Gregory R. Schulz , Michael J. Greene
发明人： Gregory R. Schulz , Michael J. Greene
IPC分类号： C09B5/62 , C07D207/26 , C09B3/18 , C09B57/08 , C09B67/22 , C07D487/02 , C07D307/89 , C09B67/20 , D06P1/44 , C07D493/82
CPC分类号： C07D207/26 , C09B57/08 , C09B67/0034
摘要： This invention relates to a process for preparing perylene pigment compositions by reaction of(a) a perylene tetracarboxylic compound;(b) about 0.01 to about 20% by weight, relative to the perylene tetracarboxylic compound, of a non-pigmentary cyclic anhydride or imide of formula (I) ##STR1## wherein W is O or NR.sup.1 (where R.sup.1 is hydrogen, a metal, or optionally substituted alkyl, cycloalkyl, aralkyl, or aryl), R.sup.2, R.sup.3, and R.sup.4 are various combinations of substituents and/or fused-on rings, and the dotted line is an optional double bond representing R.sup.2 --C.dbd.C--R.sup.3 ;(c) ammonia or a primary alkyl, aralkyl, or aryl amine; optionally in the presence of(d) a solvent and/or(e) one or more dispersants.
摘要翻译：本发明涉及通过（a）苝四羧酸化合物的反应制备苝颜料组合物的方法; （b）相对于苝四羧酸化合物，其中W为O或NR 1（其中R 1为氢，金属或任选地（其中R 1为氢）的式（I）的非颜料环状酸酐或酰亚胺为约0.01至约20重量％取代的烷基，环烷基，芳烷基或芳基），R 2，R 3和R 4是取代基和/或稠环的各种组合，虚线是任选的表示R2-C = C-R3的双键; （c）氨或伯烷基，芳烷基或芳基胺; 任选地在（d）溶剂和/或（e）一种或多种分散剂的存在下。

8. 发明授权

US06692562B2 Process for making perylene pigment compositions 有权
标题翻译：制备苝颜料组合物的方法
公开(公告)号：US06692562B2
公开(公告)日：2004-02-17
申请号：US10093546
申请日：2002-03-08
申请人： Gregory R. Schulz
发明人： Gregory R. Schulz
IPC分类号： C08K500
CPC分类号： C09B57/12 , C09B5/62 , C09B67/0034
摘要： This invention relates to a process of preparing a perylene pigment compositions containing a reactive co-precipitated blend of (1) about 75 to about 99.9 mol %, relative to the pigment composition, of a compound having the formula (I) wherein R is hydrogen, C1-C6 alkyl, C5-C8 cycloalkyl, C7-C16 aralkyl, or C6-C10 aryl, A is C1-C6 alkyl, C1-C6 alkoxy, a sulfonyl group, amino, ammonium, hydroxy, nitro, or halogen, and m is zero or a number from 1 to 8; and (2) about 0.1 to about 25 mol %, relative to the pigment composition, of a perylene dicarboxamidine imide having the formula (II) wherein W is optionally substituted or modified C2-C3 alkylene.
摘要翻译：本发明涉及一种制备苝颜料组合物的方法，该组合物含有相对于颜料组合物的（1）约75-约99.9mol％的具有式（I）的化合物（其中R是氢）的反应性共沉淀共混物， C 1 -C 6烷基，C 5 -C 8环烷基，C 7 -C 16芳烷基或C 6 -C 10芳基，A是C 1 -C 6烷基，C 1 -C 6烷氧基，磺酰基，氨基，铵，羟基，硝基或卤素，零或数字从1到8; 相对于颜料组合物，（2）约0.1至约25摩尔％的具有式（II）的苝二甲脒酰亚胺，其中W是任选取代或修饰的C 2 -C 3亚烷基。

9. 发明授权

US09546286B2 High resistivity coating compositions having unique percolation behavior, and electrostatic image developing systems and components thereof incorporating same 有权
标题翻译：具有独特渗滤行为的高电阻率涂料组合物和静电图像显影系统及其组合物
公开(公告)号：US09546286B2
公开(公告)日：2017-01-17
申请号：US14233457
申请日：2012-07-20
申请人： Eugene N. Step , Andriy Korchev , Agathagelos Kyrlidis , Clovis D. Haynes , Gregory R. Schulz , John R. Szwec
发明人： Eugene N. Step , Andriy Korchev , Agathagelos Kyrlidis , Clovis D. Haynes , Gregory R. Schulz , John R. Szwec
IPC分类号： C09C1/48 , C09D7/12 , C09C3/08 , G03G15/00 , C08K9/04 , G03G15/02 , G03G15/08 , G03G15/16
CPC分类号： C09D7/1208 , C01P2006/40 , C08K9/04 , C09C1/48 , C09C3/08 , C09D7/60 , G03G15/0233 , G03G15/0815 , G03G15/1685
摘要： Disclosed herein are resistive composites comprising at least one resin; at least one carbon black having a surface hydrophobically modified with at least one organic group, the at least one organic group having a molecular weight of the composite of 4000 or less and comprising the formula —X(G)-, wherein X is directly attached to the at least one carbon black and is selected from arylene, heteroarylene, and alkylene, G is a substituent of X, and —X(G)- is nonionic; and wherein the resistive composite has a volume resistivity, Rv, at a relative volume fraction, XCB, of the at least one carbon black in the coating, where Rv is at least 106 ohm-cm; and log Rv has a substantially linear relationship with XCB when XCB is varied from 0.1 to 0.5. Also disclosed are coatings made from such composites, such as coatings for rollers/belts for office automation machines, and methods of making such coatings.
摘要翻译：本文公开了包含至少一种树脂的电阻复合材料; 至少一种具有用至少一个有机基团疏水改性的表面的碳黑，所述至少一种有机基团的复合材料的分子量为4000以下，并且包含式-X（G） - ，其中X直接连接至少一个碳黑并且选自亚芳基，亚杂芳基和亚烷基，G是X的取代基，-X（G） - 是非离子的; 并且其中所述电阻复合材料在涂层中的至少一种炭黑的相对体积分数X C B具有体积电阻率R v，其中Rv为至少106欧姆 - 厘米; 并且当XCB从0.1变化到0.5时，log Rv与XCB具有基本线性关系。还公开了由这样的复合材料制成的涂层，例如用于办公室自动化机器的辊/带的涂层以及制造这种涂层的方法。

10. 发明申请

US20110216125A1 YELLOW PIGMENT DISPERSION 审中-公开
标题翻译：黄色素分散剂
公开(公告)号：US20110216125A1
公开(公告)日：2011-09-08
申请号：US13128964
申请日：2009-12-10
申请人： Christian Jackson , Robert Paul Held , C. Chad Roberts , Nathaniel Reed Schwartz , Gregory R. Schulz
发明人： Christian Jackson , Robert Paul Held , C. Chad Roberts , Nathaniel Reed Schwartz , Gregory R. Schulz
IPC分类号： B41J2/015 , C09D11/10
CPC分类号： C09D11/40 , C09D11/326
摘要： This invention pertains to an aqueous based dispersion of Pigment Yellow 74 which uses a certain class of polymeric dispersants which dispersant is particularly effective at dispersing the pigment and preventing pigment particle growth on storage. The classes of polymeric dispersants are based on random copolymers of an ionic momomer and a hydrophobic monomer chosen from benzyl(meth)acrylate or alkyl(meth)acrylate where the alkyl group has four to ten carbon atoms and (meth)acrylic acid. The invention also pertains to an inkjet ink comprising this Pigment Yellow 74 dispersion.
摘要翻译：本发明涉及颜料黄74的水基分散体，其使用某种类型的聚合物分散剂，该分散剂在分散颜料和防止颜料颗粒生长储存时特别有效。聚合物分散剂的种类基于离子单体和选自（甲基）丙烯酸苄酯或（甲基）丙烯酸烷基酯的疏水性单体的无规共聚物，其中烷基具有4-10个碳原子和（甲基）丙烯酸。本发明还涉及包含该颜料黄74分散体的喷墨油墨。

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