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1. 发明授权

US08329108B2 Isoolefin-diolefin production process and apparatus therefore 有权
标题翻译：因此，异烯烃二烯的生产工艺和设备
公开(公告)号：US08329108B2
公开(公告)日：2012-12-11
申请号：US12970057
申请日：2010-12-16
申请人： John Lovegrove , Hans-Juergen Mick
发明人： John Lovegrove , Hans-Juergen Mick
IPC分类号： B01J19/20 , B01J19/00
CPC分类号： C08F210/12 , B01J19/20 , B01J19/22 , B01J2219/00094 , B01J2219/00123 , B29C47/6025 , C08F2/14 , C08F236/06
摘要： In an isoolefin-diolefin rubber production process (e.g. a butyl rubber production process), the cold rubber slurry produced in the reaction vessel is transported from the reaction vessel to the flash tank during which time the cold slurry may be expressed to separate at least part of the cold liquid reaction medium from the isoolefin-diolefin rubber. The separated cold liquid reaction medium is transported off stream, for example by a mechanical filter, where it can be recycled back into the reaction vessel and/or where it can be used to cool a feed stream or streams of the reaction components. The isoolefin-diolefin rubber and the residual liquid reaction medium are transported to a flash tank for further processing. The ability to separate and recycle cold liquid reaction medium makes the process more economical. In one aspect, the slurry may be transported from the reaction vessel to the flash tank by a self-cleaning fully intermeshing co-rotating twin screw extruder, which helps overcome the problem of plugging due to rubber sticking to the surfaces of the slurry transfer apparatus.
摘要翻译：在异烯烃 - 二烯烃橡胶生产方法（例如丁基橡胶生产方法）中，在反应容器中产生的冷橡胶淤浆从反应容器输送到闪蒸罐，在此期间冷浆可以被表达以分开至少部分的来自异烯烃 - 二烯烃橡胶的冷液体反应介质。分离的冷液体反应介质例如通过机械过滤器被输送出去，其中可以将其再循环回到反应容器中和/或其中可用于冷却反应组分的进料流或流的地方。将异烯烃 - 二烯烃橡胶和残留的液体反应介质输送到闪蒸罐以进行进一步处理。分离和循环冷液体反应介质的能力使得该方法更经济。在一个方面，浆料可以通过自清洁完全相互啮合的同向旋转双螺杆挤出机从反应容器输送到闪蒸罐，这有助于克服由于橡胶粘附到浆料输送装置的表面而堵塞的问题。

2. 发明申请

US20050187366A1 Isoolefin-diolefin production process and apparatus therefore 有权
标题翻译：因此，异烯烃二烯的生产工艺和设备
公开(公告)号：US20050187366A1
公开(公告)日：2005-08-25
申请号：US11058875
申请日：2005-02-16
申请人： John Lovegrove , Hans-Juergen Mick
发明人： John Lovegrove , Hans-Juergen Mick
IPC分类号： B01J8/08 , B01J19/20 , B01J19/22 , C08F2/14 , C08F2/18 , C08F210/12 , C08L23/22 , C08F36/00
CPC分类号： C08F210/12 , B01J19/20 , B01J19/22 , B01J2219/00094 , B01J2219/00123 , B29C47/6025 , C08F2/14 , C08F236/06
摘要： In an isoolefin-diolefin rubber production process (e.g. a butyl rubber production process), the cold rubber slurry produced in the reaction vessel is transported from the reaction vessel to the flash tank during which time the cold slurry may be expressed to separate at least part of the cold liquid reaction medium from the isoolefin-diolefin rubber. The separated cold liquid reaction medium is transported off stream, for example by a mechanical filter, where it can be recycled back into the reaction vessel and/or where it can be used to cool a feed stream or streams of the reaction components. The isoolefin-diolefin rubber and the residual liquid reaction medium are transported to a flash tank for further processing. The ability to separate and recycle cold liquid reaction medium makes the process more economical. In one aspect, the slurry may be transported from the reaction vessel to the flash tank by a self-cleaning fully intermeshing co-rotating twin screw extruder, which helps overcome the problem of plugging due to rubber sticking to the surfaces of the slurry transfer apparatus.
摘要翻译：在异烯烃 - 二烯烃橡胶生产方法（例如丁基橡胶生产方法）中，在反应容器中产生的冷橡胶淤浆从反应容器输送到闪蒸罐，在此期间冷浆可以被表达以将至少部分的来自异烯烃 - 二烯烃橡胶的冷液体反应介质。分离的冷液体反应介质例如通过机械过滤器被输送出去，其中可以将其再循环回到反应容器中和/或其中可用于冷却反应组分的进料流或流的地方。将异烯烃 - 二烯烃橡胶和残留的液体反应介质输送到闪蒸罐以进行进一步处理。分离和循环冷液体反应介质的能力使得该方法更经济。在一个方面，浆料可以通过自清洁完全相互啮合的同向旋转双螺杆挤出机从反应容器输送到闪蒸罐，这有助于克服由于橡胶粘附到浆料输送装置的表面而堵塞的问题。

3. 发明授权

US07960491B2 Isoolefin-diolefin production process and apparatus therefore 有权
标题翻译：因此，异烯烃二烯的生产工艺和设备
公开(公告)号：US07960491B2
公开(公告)日：2011-06-14
申请号：US12606561
申请日：2009-10-27
申请人： John Lovegrove , Hans-Juergen Mick
发明人： John Lovegrove , Hans-Juergen Mick
IPC分类号： C08F36/00 , C08F10/00 , B01J19/00 , B01J19/20
CPC分类号： C08F210/12 , B01J19/20 , B01J19/22 , B01J2219/00094 , B01J2219/00123 , B29C47/6025 , C08F2/14 , C08F236/06
摘要： In an isoolefin-diolefin rubber production process (e.g. a butyl rubber production process), the cold rubber slurry produced in the reaction vessel is transported from the reaction vessel to the flash tank during which time the cold slurry may be expressed to separate at least part of the cold liquid reaction medium from the isoolefin-diolefin rubber. The separated cold liquid reaction medium is transported off stream, for example by a mechanical filter, where it can be recycled back into the reaction vessel and/or where it can be used to cool a feed stream or streams of the reaction components. The isoolefin-diolefin rubber and the residual liquid reaction medium are transported to a flash tank for further processing. The ability to separate and recycle cold liquid reaction medium makes the process more economical. In one aspect, the slurry may be transported from the reaction vessel to the flash tank by a self-cleaning fully intermeshing co-rotating twin screw extruder, which helps overcome the problem of plugging due to rubber sticking to the surfaces of the slurry transfer apparatus.
摘要翻译：在异烯烃 - 二烯烃橡胶生产方法（例如丁基橡胶生产方法）中，在反应容器中产生的冷橡胶淤浆从反应容器输送到闪蒸罐，在此期间冷浆可以被表达以分开至少部分的来自异烯烃 - 二烯烃橡胶的冷液体反应介质。分离的冷液体反应介质例如通过机械过滤器被输送出去，其中可以将其再循环回到反应容器中和/或其中可用于冷却反应组分的进料流或流的地方。将异烯烃 - 二烯烃橡胶和残留的液体反应介质输送到闪蒸罐以进行进一步处理。分离和循环冷液体反应介质的能力使得该方法更经济。在一个方面，浆料可以通过自清洁完全相互啮合的同向旋转双螺杆挤出机从反应容器输送到闪蒸罐，这有助于克服由于橡胶粘附到浆料输送装置的表面而堵塞的问题。

4. 发明申请

US20110150712A1 ISOOLEFIN-DIOLEFIN PRODUCTION PROCESS AND APPARATUS THEREFORE 有权
标题翻译： ISOOLEFIN-DIOLEFIN生产工艺及其设备
公开(公告)号：US20110150712A1
公开(公告)日：2011-06-23
申请号：US12970057
申请日：2010-12-16
申请人： John Lovegrove , Hans-Juergen Mick
发明人： John Lovegrove , Hans-Juergen Mick
IPC分类号： B01J19/00
CPC分类号： C08F210/12 , B01J19/20 , B01J19/22 , B01J2219/00094 , B01J2219/00123 , B29C47/6025 , C08F2/14 , C08F236/06
摘要： In an isoolefin-diolefin rubber production process (e.g. a butyl rubber production process), the cold rubber slurry produced in the reaction vessel is transported from the reaction vessel to the flash tank during which time the cold slurry may be expressed to separate at least part of the cold liquid reaction medium from the isoolefin-diolefin rubber. The separated cold liquid reaction medium is transported off stream, for example by a mechanical filter, where it can be recycled back into the reaction vessel and/or where it can be used to cool a feed stream or streams of the reaction components. The isoolefin-diolefin rubber and the residual liquid reaction medium are transported to a flash tank for further processing. The ability to separate and recycle cold liquid reaction medium makes the process more economical. In one aspect, the slurry may be transported from the reaction vessel to the flash tank by a self-cleaning fully intermeshing co-rotating twin screw extruder, which helps overcome the problem of plugging due to rubber sticking to the surfaces of the slurry transfer apparatus.
摘要翻译：在异烯烃 - 二烯烃橡胶生产方法（例如丁基橡胶生产方法）中，在反应容器中产生的冷橡胶淤浆从反应容器输送到闪蒸罐，在此期间冷浆可以被表达以将至少部分的来自异烯烃 - 二烯烃橡胶的冷液体反应介质。分离的冷液体反应介质例如通过机械过滤器被输送出去，其中可以将其再循环回到反应容器中和/或其中可用于冷却反应组分的进料流或流的地方。将异烯烃 - 二烯烃橡胶和残留的液体反应介质输送到闪蒸罐以进行进一步处理。分离和循环冷液体反应介质的能力使得该方法更经济。在一个方面，浆料可以通过自清洁完全相互啮合的同向旋转双螺杆挤出机从反应容器输送到闪蒸罐，这有助于克服由于橡胶粘附到浆料输送装置的表面而堵塞的问题。

5. 发明授权

US07931873B2 Isoolefin-diolefin production process and apparatus therefore 有权
公开(公告)号：US07931873B2
公开(公告)日：2011-04-26
申请号：US11058875
申请日：2005-02-16
申请人： John Lovegrove , Hans-Juergen Mick
发明人： John Lovegrove , Hans-Juergen Mick
IPC分类号： B01J19/20 , B01J19/00
CPC分类号： C08F210/12 , B01J19/20 , B01J19/22 , B01J2219/00094 , B01J2219/00123 , B29C47/6025 , C08F2/14 , C08F236/06
摘要： In an isoolefin-diolefin rubber production process (e.g. a butyl rubber production process), the cold rubber slurry produced in the reaction vessel is transported from the reaction vessel to the flash tank during which time the cold slurry may be expressed to separate at least part of the cold liquid reaction medium from the isoolefin-diolefin rubber. The separated cold liquid reaction medium is transported off stream, for example by a mechanical filter, where it can be recycled back into the reaction vessel and/or where it can be used to cool a feed stream or streams of the reaction components. The isoolefin-diolefin rubber and the residual liquid reaction medium are transported to a flash tank for further processing. The ability to separate and recycle cold liquid reaction medium makes the process more economical. In one aspect, the slurry may be transported from the reaction vessel to the flash tank by a self-cleaning fully intermeshing co-rotating twin screw extruder, which helps overcome the problem of plugging due to rubber sticking to the surfaces of the slurry transfer apparatus.

6. 发明申请

US20100048838A1 ISOOLEFIN-DIOLEFIN PRODUCTION PROCESS AND APPARATUS THEREFORE 有权
标题翻译： ISOOLEFIN-DIOLEFIN生产工艺及其设备
公开(公告)号：US20100048838A1
公开(公告)日：2010-02-25
申请号：US12606561
申请日：2009-10-27
申请人： John Lovegrove , Hans-Juergen Mick
发明人： John Lovegrove , Hans-Juergen Mick
IPC分类号： C08F2/01 , C08F136/02
CPC分类号： C08F210/12 , B01J19/20 , B01J19/22 , B01J2219/00094 , B01J2219/00123 , B29C47/6025 , C08F2/14 , C08F236/06
摘要： In an isoolefin-diolefin rubber production process (e.g. a butyl rubber production process), the cold rubber slurry produced in the reaction vessel is transported from the reaction vessel to the flash tank during which time the cold slurry may be expressed to separate at least part of the cold liquid reaction medium from the isoolefin-diolefin rubber. The separated cold liquid reaction medium is transported off stream, for example by a mechanical filter, where it can be recycled back into the reaction vessel and/or where it can be used to cool a feed stream or streams of the reaction components. The isoolefin-diolefin rubber and the residual liquid reaction medium are transported to a flash tank for further processing. The ability to separate and recycle cold liquid reaction medium makes the process more economical. In one aspect, the slurry may be transported from the reaction vessel to the flash tank by a self-cleaning fully intermeshing co-rotating twin screw extruder, which helps overcome the problem of plugging due to rubber sticking to the surfaces of the slurry transfer apparatus.
摘要翻译：在异烯烃 - 二烯烃橡胶生产方法（例如丁基橡胶生产方法）中，在反应容器中产生的冷橡胶淤浆从反应容器输送到闪蒸罐，在此期间冷浆可以被表达以将至少部分的来自异烯烃 - 二烯烃橡胶的冷液体反应介质。分离的冷液体反应介质例如通过机械过滤器被输送出去，其中可以将其再循环回到反应容器中和/或其中可用于冷却反应组分的进料流或流的地方。将异烯烃 - 二烯烃橡胶和残留的液体反应介质输送到闪蒸罐以进行进一步处理。分离和循环冷液体反应介质的能力使得该方法更经济。在一个方面，浆料可以通过自清洁完全相互啮合的同向旋转双螺杆挤出机从反应容器输送到闪蒸罐，这有助于克服由于橡胶粘附到浆料输送装置的表面而堵塞的问题。

7. 发明授权

US09512240B2 Process for the production of water and solvent-free polymers 有权
标题翻译：生产水和无溶剂聚合物的方法
公开(公告)号：US09512240B2
公开(公告)日：2016-12-06
申请号：US13063227
申请日：2009-09-17
申请人： Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
发明人： Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
IPC分类号： B29C47/76 , C08C2/00 , C01B5/00 , C08F6/00 , B29C47/36 , B29C47/38 , B29C47/60 , B29C47/62 , B29B7/74
CPC分类号： C08C2/00 , B29B7/7485 , B29C47/364 , B29C47/38 , B29C47/6056 , B29C47/62 , C01B5/00 , C08F6/003 , C08L23/283
摘要： The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like non-halogenated and halogenated butyl rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
摘要翻译：本发明涉及无水和无溶剂的聚合物，特别是无水和无溶剂的合成橡胶产品，如非卤化和卤化丁基橡胶产品，以及其生产方法。本发明还涉及适合于完成所述过程的装置。

8. 发明授权

US08975361B2 Process for the production of water and solvent-free polymers 有权
标题翻译：生产水和无溶剂聚合物的方法
公开(公告)号：US08975361B2
公开(公告)日：2015-03-10
申请号：US13635781
申请日：2011-03-23
申请人： Wolfgang Krumbe , Rolf Feller , Paul Wagner , Hanns-Ingolf Paul , Martin Siebuerger , Heike Kloppenburg , Alicia Le-Sattler , John Lovegrove
发明人： Wolfgang Krumbe , Rolf Feller , Paul Wagner , Hanns-Ingolf Paul , Martin Siebuerger , Heike Kloppenburg , Alicia Le-Sattler , John Lovegrove
IPC分类号： C08G63/02 , C08L9/00 , C08F6/10 , C08F6/12 , C08C2/00 , C08G64/00
CPC分类号： C08F6/10 , C08C2/00 , C08F6/12 , C08L9/00
摘要： The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like styrene butadiene rubber products and butadiene rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
摘要翻译：本发明涉及无水和无溶剂的聚合物，特别是无溶剂的合成橡胶产品，如丁苯橡胶产品和丁二烯橡胶产品，以及其生产方法。本发明还涉及适合于完成所述过程的装置。

9. 发明授权

US09273154B2 Process for production of halobutyl ionomers 有权
标题翻译：卤代丁基离聚物的制备方法
公开(公告)号：US09273154B2
公开(公告)日：2016-03-01
申请号：US13522757
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
IPC分类号： C08F8/22 , C08C19/24 , C08F8/30 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/32 , C08F8/40 , C08F210/12
CPC分类号： C08C19/24 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/22 , C08F8/30 , C08F8/32 , C08F8/40 , C08F210/12 , C08F236/08
摘要： The invention relates to an energy efficient, environmentally favorable process for the preparation of butyl ionomers that uses a common medium for both solution polymerization and subsequent bromination of butyl rubber. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and bromination of butyl rubber in the presence of a brominating agent and optionally for subsequent reaction with at least one nitrogen and/or phosphorus based nucleophile.
摘要翻译：本发明涉及用于制备丁基离聚物的能量效率高，环境友好的方法，该方法使用普通介质进行溶液聚合和随后溴化丁基橡胶。更具体地说，本发明涉及一种在溴化剂存在下使用普通脂肪族介质进行丁基橡胶的溶液聚合和溴化的方法，并且任选地随后与至少一种基于氮和/或磷的亲核试剂反应。

10. 发明授权

US09062185B2 Process for production of polymer nanocomposites 有权
标题翻译：生产聚合物纳米复合材料的方法
公开(公告)号：US09062185B2
公开(公告)日：2015-06-23
申请号：US13522760
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
IPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08J5/00 , C08F210/12
CPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08F8/22 , C08F8/40 , C08F8/44 , C08F210/12 , C08J5/005 , C08J2323/28 , C08J2323/36 , Y02T10/862 , C08F236/08 , C08F2500/21
摘要： The invention relates to a processes for preparing nanocomposites comprising rubber ionomers which were prepared by an energy efficient, environmentally favorable process that uses a common medium for solution polymerization, bromination of rubber and optionally subsequent polymer nanocomposite formation. Polymer nanocomposites according to the present invention exhibit high oxygen impermeability.
摘要翻译：本发明涉及一种制备纳米复合材料的方法，其包括橡胶离聚物，其通过使用普通介质进行溶液聚合，溴化橡胶和任选的后续聚合物纳米复合材料形成的能量有效的，环境友好的方法制备。根据本发明的聚合物纳米复合材料显示出高的不透气性。

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