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1. 发明授权

US09102785B2 Curable compositions based on polyuretidiones, polythiols and photoactivable bases and generation of isocyanates from uretidiones 有权
标题翻译：基于聚赖氨酸，多硫醇和可光活化碱的可固化组合物和来自脲类的异氰酸酯的生成
公开(公告)号：US09102785B2
公开(公告)日：2015-08-11
申请号：US12411429
申请日：2009-03-26
申请人： Jonathan T. Martz , Deborah E. Hayes , Debra L. Singer
发明人： Jonathan T. Martz , Deborah E. Hayes , Debra L. Singer
IPC分类号： C08G18/79 , C08G18/20 , C08G18/38 , C09D175/04
CPC分类号： C08G18/2018 , C07C263/08 , C08G18/2063 , C08G18/3876 , C08G18/798 , C09D175/04
摘要： Curable compositions based on polyuretidiones, polythiols and photoactivable bases are disclosed. Also a process for generating isocyanate groups by exposing uretidiones to radiation in the range of 100-315 nm is disclosed. The process can be used in a dual curing system for curing compositions that comprise groups that under go photoinduced polymerizations and active hydrogen groups that react with the generated isocyanates.
摘要翻译：公开了基于聚脲酸酯，多硫醇和可光活化碱的固化组合物。还公开了通过将脲类溶剂暴露于100-315nm范围内的辐射产生异氰酸酯基团的方法。该方法可用于双重固化体系，用于固化组合物，其包含经过光诱导聚合的基团和与所生成的异氰酸酯反应的活性氢基团。

2. 发明申请

US20090258962A1 CURABLE COMPOSITIONS BASED ON POLYURETIDIONES, POLYTHIOLS AND PHOTOACTIVABLE BASES AND GENERATION OF ISOCYANATES FROM URETIDIONES 有权
标题翻译：基于聚合物，聚硅氧烷和可光化基团的可固化组合物和来自尿素的异氰酸酯的生成
公开(公告)号：US20090258962A1
公开(公告)日：2009-10-15
申请号：US12411429
申请日：2009-03-26
申请人： Jonathan T. Martz , Deborah E. Hayes , Debra L. Singer
发明人： Jonathan T. Martz , Deborah E. Hayes , Debra L. Singer
IPC分类号： C08F2/50 , C08J3/28
CPC分类号： C08G18/2018 , C07C263/08 , C08G18/2063 , C08G18/3876 , C08G18/798 , C09D175/04
摘要： Curable compositions based on polyuretidiones, polythiols and photoactivable bases are disclosed. Also a process for generating isocyanate groups by exposing uretidiones to radiation in the range of 100-315 nm is disclosed. The process can be used in a dual curing system for curing compositions that comprise groups that under go photoinduced polymerizations and active hydrogen groups that react with the generated isocyanates.
摘要翻译：公开了基于聚脲酸酯，多硫醇和可光活化碱的固化组合物。还公开了通过将脲类溶剂暴露于100-315nm范围内的辐射产生异氰酸酯基团的方法。该方法可用于双重固化体系，用于固化组合物，其包含经过光诱导聚合的基团和与所生成的异氰酸酯反应的活性氢基团。

3. 发明授权

US08129492B1 Coating compositions comprising polyurea and a phosphorous-containing polyol 有权
标题翻译：包含聚脲和含磷多元醇的涂料组合物
公开(公告)号：US08129492B1
公开(公告)日：2012-03-06
申请号：US12122980
申请日：2008-05-19
申请人： Steven V. Barancyk , Howard L. Senkfor , Debra L. Singer , John M. Furar , Michael A. Zalich , Thomas R. Hockswender
发明人： Steven V. Barancyk , Howard L. Senkfor , Debra L. Singer , John M. Furar , Michael A. Zalich , Thomas R. Hockswender
IPC分类号： C08G71/02 , C08L75/02
CPC分类号： C08G18/721 , C08G18/10 , C08G18/3878 , C08G18/5075 , C09D175/02 , C08G18/3225
摘要： The present invention is directed to a coating composition comprising polyurea formed from a reaction mixture comprising: (a) a first component comprising isocyanate, wherein said isocyanate comprises an isocyanate functional prepolymer formed from a reaction mixture comprising isocyanate and a material comprising a phosphorus-containing polyol; and (b) a second component comprising an amine.
摘要翻译：本发明涉及包含由反应混合物形成的聚脲的涂料组合物，其包含：（a）包含异氰酸酯的第一组分，其中所述异氰酸酯包含由包含异氰酸酯的反应混合物形成的异氰酸酯官能预聚物和包含含磷多元醇和（b）包含胺的第二组分。

4. 发明授权

US06228974B1 Aminoplast curable film-forming compositions providing films having resistance to acid etching 失效
公开(公告)号：US06228974B1
公开(公告)日：2001-05-08
申请号：US08345918
申请日：1994-11-28
申请人： Gregory J. McCollum , Debra L. Singer , Kurt G. Olson , S. Tonya Stefko , Michael A. Mayo , Dennis L. Faler
发明人： Gregory J. McCollum , Debra L. Singer , Kurt G. Olson , S. Tonya Stefko , Michael A. Mayo , Dennis L. Faler
IPC分类号： C09D17404
CPC分类号： C09D167/00 , C08F8/30 , C08L61/20 , C08L61/32 , C09D133/062 , C09D201/06 , C08L2666/14 , C08L2666/16
摘要： An aminoplast-curable film-forming composition is disclosed. The film-forming composition is a crosslinkable composition comprising (1) a material containing a plurality of carbamate and/or urea functional groups and (2) an aminoplast crosslinking agent. The composition provides a coating with improved acid etch resistance, making the coating particularly useful as an automotive clear coat.

5. 发明授权

US4749803A Reaction products of mercapto-functional monohydric alcohols and vinyl silanes, and NCO-functional compounds therefrom 失效
标题翻译：巯基官能的一元醇和乙烯基硅烷的反应产物，以及由它们构成的NCO-官能的化合物
公开(公告)号：US4749803A
公开(公告)日：1988-06-07
申请号：US816078
申请日：1986-01-03
申请人： Rostyslaw Dowbenko , Debra L. Singer
发明人： Rostyslaw Dowbenko , Debra L. Singer
IPC分类号： C07F7/08 , C07F7/18 , C08G18/10 , C08G18/38 , C07F7/10
CPC分类号： C08G18/3893 , C07F7/182 , C08G18/10
摘要： Disclosed is an adduct of a mercapto-functional monohydric alcohol and a vinyl-type silane having at least one hydrolyzable group directly attached to a silicon atom, the adduct prepared by reacting the mercapto-functional monohydric alcohol and the vinyl-type silane in the presence of a free radical initiator.Also disclosed is an NCO-functional compound comprising the reaction product of: (A) the aforesaid adduct of a mercapto-functional monohydric alcohol and a vinyl-type silane having at least one hydrolyzable group directly attached to a silicon atom, and (B) an organic polyisocyanate.
摘要翻译：公开了一种巯基官能的一元醇和具有至少一个直接连接到硅原子上的可水解基团的乙烯基型硅烷的加合物，该加成物是通过巯基官能的一元醇和乙烯基型硅烷在存在下反应制备的的自由基引发剂。还公开了包含以下反应产物的NCO官能化合物：（A）上述巯基官能化一元醇的上述加成物和至少具有直接与硅原子连接的可水解基团的乙烯基型硅烷，（B）有机多异氰酸酯。

6. 发明授权

US4454274A Aminoplast curable coating compositions containing cycloaliphatic sulfonic acid esters as latent acid catalysts 失效
标题翻译：含有脂环族磺酸酯作为潜酸催化剂的氨基塑料可固化涂料组合物
公开(公告)号：US4454274A
公开(公告)日：1984-06-12
申请号：US427400
申请日：1982-09-29
申请人： Debra L. Singer , Gregory J. McCollum , Rostyslaw Dowbenko , Roger M. Christenson
发明人： Debra L. Singer , Gregory J. McCollum , Rostyslaw Dowbenko , Roger M. Christenson
IPC分类号： C08F8/36 , C08K5/42
CPC分类号： C08K5/42 , C07C309/00
摘要： A high solids, organic solvent based, sprayable coating composition which is capable of acid catalyzed crosslinking is composed of an active hydrogen-containing resin, a curing agent present externally and/or internally as a part of the active hydrogen-containing resin; and a catalytic amount of a non-ionic ester of a sulfonic acid. The sulfonic acid ester is represented by the following structural formulas: ##STR1## wherein: Z is a radical selected from the group consisting of amino and an organic radical, said organic radical being connected to the sulfur atom by a carbon atom;W is C.sub.1 -C.sub.18 alkylene, C.sub.2 -C.sub.18 alkenylene;V is C.sub.1 -C.sub.18 alkylene, C.sub.1 -C.sub.18 hydroxyl substituted alkylene, C.sub.2 -C.sub.18 alkenylene, C.sub.2 -C.sub.18 hydroxyl substituted alkenylene; andR.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5 are independently hydrogen or an organic radical.
摘要翻译：能够进行酸催化交联的高固含量有机溶剂型可喷涂涂料组合物由含活性氢的树脂，外部存在和/或内部作为活性含氢树脂的一部分存在的固化剂组成。和催化量的磺酸的非离子酯。磺酸酯由以下结构式表示：其中：Z是选自氨基和有机基团的基团，所述有机基团与硫连接原子由碳原子; W是C 1 -C 18亚烷基，C 2 -C 18亚烯基; V是C 1 -C 18亚烷基，C 1 -C 18羟基取代的亚烷基，C 2 -C 18亚烯基，C 2 -C 18羟基取代的亚烯基; 并且R 1，R 2，R 3，R 4，R 5独立地为氢或有机基团。

7. 发明授权

US08039517B2 Colloidal particle sols and methods for preparing the same 有权
标题翻译：胶体颗粒溶胶及其制备方法
公开(公告)号：US08039517B2
公开(公告)日：2011-10-18
申请号：US11001543
申请日：2004-12-01
申请人： Lawrence G. Anderson , Debra L. Singer , Thomas R. Hockswender
发明人： Lawrence G. Anderson , Debra L. Singer , Thomas R. Hockswender
IPC分类号： B01F3/12 , B01F3/22 , C04B14/00
CPC分类号： C01B33/145 , B01J13/0008 , B01J13/0026 , C01B33/1485
摘要： A method of preparing an organic sol of particles is provided. Steps include: a) providing a suspension of particles in an aqueous medium; b) adding an organic liquid to form an admixture where the concentration of particles in the admixture is less than or equal to 40 percent by weight; c) maintaining the admixture at a temperature and pressure and for a time sufficient to reduce the water content to less than 30 percent by weight while simultaneously adding a water-compatible organic liquid at a rate sufficient to maintain a concentration of particles in the admixture at less than or equal to 50 percent by weight; and d) adding at least one polymer while maintaining the admixture at a temperature and pressure and for a time sufficient to provide an organic sol of particles comprising 1 percent by weight or less of water.
摘要翻译：提供了一种制备颗粒有机溶胶的方法。步骤包括：a）在水介质中提供颗粒的悬浮液; b）加入有机液体以形成其中混合物中颗粒的浓度小于或等于40重量％的混合物; c）将混合物在温度和压力下保持足够的时间以将水含量降低至小于30重量％，同时以足以将混合物中的颗粒浓度保持在混合物中的速率同时加入水相容性有机液体小于或等于50重量％; 和d）在保持混合物的温度和压力下加入至少一种聚合物，并持续足以提供包含1重量％或更少的水的颗粒的有机溶胶。

8. 发明申请

US20080302273A1 UV CURABLE COATING COMPOSITION AND METHOD OF MAKING 有权
标题翻译： UV可固化涂料组合物及其制备方法
公开(公告)号：US20080302273A1
公开(公告)日：2008-12-11
申请号：US11760215
申请日：2007-06-08
申请人： Charles M. Kania , Debra L. Singer , Diane J. Schillinger
发明人： Charles M. Kania , Debra L. Singer , Diane J. Schillinger
IPC分类号： C08J3/28
CPC分类号： C08G18/423 , C08G18/672 , C08G18/673 , C08G18/792 , C08G2150/20 , C08G18/42
摘要： The present invention relates to solid, particulate free film-forming compositions, multi-layer composite coatings comprising such film-forming compositions and methods of applying such multi-component composite coatings to a substrate. The solvent free film-forming compositions include UV-curable powder coating compositions comprising an amorphous (meth)acrylate terminated poly(ester-urethane) and optionally a second (meth)acrylate terminated polyurethane.
摘要翻译：本发明涉及固体，无颗粒状成膜组合物，包含这种成膜组合物的多层复合涂层以及将这种多组分复合涂层施加到基底上的方法。无溶剂的成膜组合物包括包含无定形（甲基）丙烯酸酯封端的聚（酯 - 氨基甲酸酯）和任选的第二（甲基）丙烯酸酯封端的聚氨酯）的UV固化粉末涂料组合物。

9. 发明授权

US06313224B1 Coating of film-forming resin and functional flow control copolymer 失效
标题翻译：成膜树脂和功能流动控制共聚物的涂层
公开(公告)号：US06313224B1
公开(公告)日：2001-11-06
申请号：US09437891
申请日：1999-11-09
申请人： Debra L. Singer , Kurt G. Olson , Kurt A. Humbert , Karen A. Barkac , Mark E. Wozniak
发明人： Debra L. Singer , Kurt G. Olson , Kurt A. Humbert , Karen A. Barkac , Mark E. Wozniak
IPC分类号： C08L2304
CPC分类号： C09D201/00 , C09D7/47 , Y10T428/31692 , C08L2666/04
摘要： Curable coating compositions comprising either a liquid or particulate curable film-forming resinous material, a flow control agent which is a copolymer and optionally a carrier for the liquid resinous material. The copolymer is from at least one non-amino, non-hydroxyl and non-acid functional alkyl acrylate or methacrylate containing from 1 to 20 carbon atoms in the alkyl group, and functional monomer of either (i) amino functional acrylates and methacrylates in an effective amount to give the copolymer an amine value in the range from 2 to 70, or (ii) acid functional acrylate and methacrylate in an effective amount to give the copolymer an acid value in the range of from 10 to 30. Additionally, with either functional monomer (i) or (ii) another functional comonomer (iii) can be present in the copolymer which is hydroxyalkyl acrylate and/or hydroxyalkyl methacrylate and/or caprolactone polyol monomer. Comonomer (iii) can be present in the copolymer in an effective amount to give the copolymer a hydroxyl number is in the range of about 0 to 100.
摘要翻译：可固化的涂料组合物包括液体或颗粒状可固化成膜树脂材料，流动控制剂，其是共聚物和任选的液体树脂材料的载体。该共聚物来自烷基中至少一个含有1-20个碳原子的非氨基，非羟基和非酸官能的丙烯酸酯或甲基丙烯酸烷基酯，和（i）氨基官能的丙烯酸酯和甲基丙烯酸酯的官能单体有效量使得共聚物的胺值在2-70范围内，或（ii）酸官能丙烯酸酯和甲基丙烯酸酯有效量，以使共聚物的酸值在10至30的范围内。另外，在丙烯酸羟烷基酯和/或甲基丙烯酸羟烷基酯和/或己内酯多元醇单体的共聚物中可以存在官能单体（i）或（ii）另一功能性共聚单体（iii）。共聚单体（iii）可以以有效的量存在于共聚物中，得到共聚物，羟值在约0-100范围内。

10. 发明授权

US06268055B1 Photochromic epoxy resin coating composition and articles having such a coating 有权
标题翻译：光致变色环氧树脂涂料组合物和具有这种涂层的制品
公开(公告)号：US06268055B1
公开(公告)日：2001-07-31
申请号：US09187698
申请日：1998-11-06
申请人： Robert W. Walters , Cletus N. Welch , John W. Burgman , Debra L. Singer , Shanti Swarup
发明人： Robert W. Walters , Cletus N. Welch , John W. Burgman , Debra L. Singer , Shanti Swarup
IPC分类号： C08G5942
CPC分类号： C09D163/00 , G02B5/23 , Y10T428/31511 , C08L2666/28
摘要： Described are photochromic epoxy resin coatings that meet commercially acceptable “cosmetic” standards for optical coatings. Also described are articles having such coatings. The coatings exhibit a Fischer microhardness of from 50 to 150 Newtons per mm2 and desirable photochromic properties, i.e., the formation of darker activated colors and faster rates of photochromic activation and fade when irradiated with ultraviolet light.
摘要翻译：描述了满足商业上可接受的用于光学涂层的“化妆品”标准的光致变色环氧树脂涂料。还描述了具有这种涂层的制品。涂层表现出每毫米50至150牛顿的菲舍尔显微硬度和所需的光致变色性质，即，当用紫外线照射时，形成更暗的活化颜色和更快的光致变色激活速率和褪色。

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