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    • 4. 发明申请
    • PROCESS FOR CONTINUOUS PRODUCTION OF BORON NITRIDE POWDER
    • 连续生产硝酸铁粉的方法
    • US20140314652A1
    • 2014-10-23
    • US14355020
    • 2012-10-24
    • KANEKA CORPORATION
    • Kazuaki MatsumotoToshiyuki KawaguchiMasashi Sakaguchi
    • C01B21/064
    • C01B21/0648C01B21/0645C01P2002/76C01P2004/61C01P2004/90C04B35/583C04B2235/5436C04B2235/767
    • The present invention provides a process for continuously producing crystalline hexagonal boron nitride powder having a large particle size and high crystalline. The present invention relates to a process comprising: the first step of heating a boron-containing material and a nitrogen-containing material to obtain crude boron nitride powder having boron nitride content of 80% by weight or higher, and the second step of feeding the crude boron nitride powder and a boron-containing flux component in the content satisfying the following formula (1) with a heat-resistant container, and heating the container including the crude boron nitride powder and the boron-containing flux component at 1550 to 2400° C. in a continuous furnace under the atmosphere of nitrogen gas, to grow hexagonal boron nitride in the form of crystal: formula (1): boron content contained in boron-containing flux component/crude boron nitride content ≦1.4 % by weight.
    • 本发明提供一种连续生产具有大粒径和高结晶度的结晶六方氮化硼粉末的方法。 本发明涉及一种方法,其包括:加热含硼材料和含氮材料的第一步骤,以获得氮化硼含量为80重量%以上的粗氮化硼粉末,第二步是将 粗制氮化硼粉末和含有助熔剂成分的含有满足下式(1)的含有助熔剂的容器,并将含有粗氮化硼粉末和含硼助焊剂成分的容器加热到1550〜2400℃ C.在氮气气氛的连续炉中,以晶体形式生长六方氮化硼:式(1):含硼助焊剂成分中含有的硼含量/粗氮化硼含量≦̸ 1.4重量%。