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1. 发明申请

US20090191373A1 Single Layer Film and Hydrophilic Material Comprising the Same 有权
标题翻译：包含它的单层膜和亲水材料
公开(公告)号：US20090191373A1
公开(公告)日：2009-07-30
申请号：US12085832
申请日：2006-11-27
申请人： Koju Okazaki , Ryouichi Seki , Takazou Katou , Masatoshi Takagi
发明人： Koju Okazaki , Ryouichi Seki , Takazou Katou , Masatoshi Takagi
IPC分类号： B32B33/00 , C08F20/06 , B32B27/36 , C08G63/46
CPC分类号： G02B1/18 , B05D5/00 , C03C17/30 , C08J7/047 , C08J2367/00 , C08J2443/02 , C09D5/1668 , C09D133/14 , C09D143/02 , C09K3/16 , C09K3/18 , G02B1/16 , G02B27/0006 , Y10T428/14 , Y10T428/1476 , Y10T428/23 , Y10T428/263 , Y10T428/269 , Y10T428/28 , Y10T428/31 , Y10T428/31786 , Y10T428/31855
摘要： A single layer film containing at least one anionic hydrophilic group selected from a sulfonic acid group, a carboxyl group and a phosphate group, wherein an anion concentration ratio (Sa/Da) of an anion concentration at a surface (Sa) to an anion concentration at a deep part (Da) is 1.1 or more. The single layer film is a copolymer prepared by polymerizing a composition containing a compound (I) represented by the general formula (1) ([X]s[M1]1[M2]m (1)) and a compound (II) having two or more (meth)acryloyl groups in a molecule at a molar ratio of 15:1 to 1:30 and having a water contact angle of 30° or less. Such a single layer film has high hydrophilicity and surface hardness and is excellent in antifogging property, antifouling property and antistatic property, thus is useful as an antifogging material, an antifouling material, an antistatic material and a multilayer body.
摘要翻译：含有选自磺酸基，羧基和磷酸酯基的至少一个阴离子亲水基团的单层膜，其中表面处的阴离子浓度（Sa）与阴离子浓度的阴离子浓度比（Sa / Da）在深部（Da）为1.1以上。单层膜是通过使含有通式（1）表示的化合物（I）（[X] s [M1] 1 [M2] m（1））的化合物和具有式分子中的摩尔比为15:1至1:30的两个或多个（甲基）丙烯酰基，并且具有30°或更低的水接触角。这样的单层膜的亲水性和表面硬度高，防雾性，防污性，抗静电性优异，因此可用作防雾材料，防污材料，抗静电材料和多层体。

2. 发明授权

US08617711B2 Single layer film and hydrophilic material comprising the same 有权
标题翻译：单层膜和包含其的亲水材料
公开(公告)号：US08617711B2
公开(公告)日：2013-12-31
申请号：US12085832
申请日：2006-11-27
申请人： Koju Okazaki , Ryouichi Seki , Takazou Katou , Masatoshi Takagi
发明人： Koju Okazaki , Ryouichi Seki , Takazou Katou , Masatoshi Takagi
IPC分类号： B32B7/06 , B32B7/12 , B32B27/30 , B32B33/00 , B05D3/00 , B05D5/00 , C08F20/26 , C08F20/38 , C09D133/10 , C09D133/14 , C09K3/00 , C09K3/16 , C09K3/18 , B05D3/02 , B05D3/06
CPC分类号： G02B1/18 , B05D5/00 , C03C17/30 , C08J7/047 , C08J2367/00 , C08J2443/02 , C09D5/1668 , C09D133/14 , C09D143/02 , C09K3/16 , C09K3/18 , G02B1/16 , G02B27/0006 , Y10T428/14 , Y10T428/1476 , Y10T428/23 , Y10T428/263 , Y10T428/269 , Y10T428/28 , Y10T428/31 , Y10T428/31786 , Y10T428/31855
摘要： A single layer film containing at least one anionic hydrophilic group selected from a sulfonic acid group, a carboxyl group and a phosphate group, wherein an anion concentration ratio (Sa/Da) of an anion concentration at a surface (Sa) to an anion concentration at a deep part (Da) is 1.1 or more. The single layer film is a copolymer prepared by polymerizing a composition containing a compound (I) represented by the general formula (1) ([X]s[M1]l[M2]m (1)) and a compound (II) having two or more (meth)acryloyl groups in a molecule at a molar ratio of 15:1 to 1:30 and having a water contact angle of 30° or less. Such a single layer film has high hydrophilicity and surface hardness and is excellent in antifogging property, antifouling property and antistatic property, thus is useful as an antifogging material, an antifouling material, an antistatic material and a multilayer body.
摘要翻译：含有选自磺酸基，羧基和磷酸酯基的至少一个阴离子亲水基团的单层膜，其中表面处的阴离子浓度（Sa）与阴离子浓度的阴离子浓度比（Sa / Da）在深部（Da）为1.1以上。单层膜是通过聚合含有通式（1）表示的化合物（I）（[X] s [M1] l [M2] m（1））和具有式分子中的摩尔比为15:1至1:30的两个或多个（甲基）丙烯酰基，并且具有30°或更低的水接触角。这样的单层膜的亲水性和表面硬度高，防雾性，防污性，抗静电性优异，因此可用作防雾材料，防污材料，抗静电材料和多层体。

3. 发明授权

US06797805B2 Organic polymers and novel polymerizable compounds 有权
标题翻译：有机聚合物和新型可聚合化合物
公开(公告)号：US06797805B2
公开(公告)日：2004-09-28
申请号：US10169190
申请日：2002-06-28
申请人： Koju Okazaki , Ryouichi Seki , Shiro Nakatsuka
发明人： Koju Okazaki , Ryouichi Seki , Shiro Nakatsuka
IPC分类号： C08G7356
CPC分类号： C07D233/32 , C08F20/36 , C08G18/38
摘要： Organic polymers having water contact angles of 20° or smaller, preferably 7° or smaller and equipped with both high wettability and high transparency. The organic polymers may contain as partial structures polar structures of about 3 debyes or higher in dipole moment and are available especially from polymerization of polymerizable compounds having alkylene(thio)urea structures.
摘要翻译：水接触角为20°以下，优选为7°以下，具有高润湿性和高透明性的有机聚合物。有机聚合物可以以偶极矩含有约3德拜或更高的部分结构极性结构，并且特别是可聚合具有亚烷基（硫）脲结构的可聚合化合物。

4. 发明授权

US07008571B2 Optical component and sulfur-containing poly(thio)ester (co)polymer 有权
标题翻译：光学组分和含硫聚（硫）酯（共）聚合物
公开(公告)号：US07008571B2
公开(公告)日：2006-03-07
申请号：US10275704
申请日：2002-03-11
申请人： Chojiro Higuchi , Atsuo Otsuji , Kenichi Sugimoto , Mitsuo Nakamura , Masatoshi Takagi , Yasuhiro Nukii , Koju Okazaki
发明人： Chojiro Higuchi , Atsuo Otsuji , Kenichi Sugimoto , Mitsuo Nakamura , Masatoshi Takagi , Yasuhiro Nukii , Koju Okazaki
IPC分类号： B29D11/00
CPC分类号： G02B1/04 , C08G63/6886 , C08G75/26 , C08L81/00 , C08L67/00
摘要： A poly(thio)ester (co)polymer which comprises a repeating structural unit represented by the formula (1-A) as an essential structural unit: [wherein R11 is a divalent aliphatic hydrocarbon group which may contain at least one sulfur atom in a sulfide group; R12 is a mono- or poly-cyclic aliphatic or aromatic dicarboxylic acid residue; and X11 and X12 are each independently an oxygen atom or sulfur atom, and when X11 and X12 are the oxygen atoms, R11 is a divalent aliphatic hydrocarbon group containing at least one sulfur atom in the sulfide group]; and an optical component obtainable by molding the poly(thio)ester (co)polymer. The poly(thio)ester (co)polymer is excellent in transparency and optical characteristics (e.g., a higher refractive index, higher Abbe number, and lower birefringence), and has also good mechanical characteristics and thermal characteristics, and further is excellent in melt fluidity and injection moldability.
摘要翻译：包含由式（1-A）表示的重复结构单元作为必要结构单元的聚（硫代）酯（共）聚合物：[其中R 11是二价脂族烃基，其可以是在硫化物基团中含有至少一个硫原子; R 12是单环或多环脂族或芳族二羧酸残基; X 11和X 12各自独立地是氧原子或硫原子，当X 11和X 12时， >是氧原子，R 11是在硫化物基团中含有至少一个硫原子的二价脂族烃基]; 以及通过模制聚（硫代）酯（共）聚合物而获得的光学部件。聚（硫代）酯（共）聚合物的透明度和光学特性（例如，较高的折射率，较高的阿贝数和较低的双折射）具有优异的机械特性和热特性，而且熔体流动性和注塑成型性。

5. 发明授权

US09238769B2 Monolayer film and hydrophilic material comprising the same 有权
标题翻译：单层膜和包含其的亲水性材料
公开(公告)号：US09238769B2
公开(公告)日：2016-01-19
申请号：US14234941
申请日：2011-07-25
申请人： Koju Okazaki
发明人： Koju Okazaki
IPC分类号： C09K3/18 , C09K8/16 , C09D4/00 , C09D5/00 , C09D133/06 , C09D133/14 , C08F220/38 , C09D5/16 , B05D1/18
CPC分类号： C09K3/18 , B05D1/185 , C08F220/38 , C09D4/00 , C09D5/00 , C09D5/1668 , C09D133/06 , C09D133/14 , C09K8/16 , Y10T428/1462 , Y10T428/263 , Y10T428/2848 , Y10T428/31938 , C08F2220/382 , C08F222/1006
摘要： The invention provides monolayer films which not only have hydrophilicity and are excellent in such properties as antifogging properties, antifouling properties, antistatic properties and anti-condensation properties but also tend to exhibit excellent transparency even with a large film thickness and excellent scratch resistance, as well as stacks having the monolayer film. The monolayer film is obtained by preparing a mixture including a monomer composition and a solvent, the monomer composition including a specific monomer and a polyvalent monomer having two or more (meth)acryloyl groups and being free of sulfonic group, carboxyl group and phosphoric group in a specific molar ratio, the solvent having a specific solubility parameter σ; applying the mixture onto a substrate and removing at least part of the solvent; and polymerizing the monomer composition to produce a monolayer film having at least one anionic hydrophilic group selected from a sulfonic group, a carboxyl group and a phosphoric group and a specific anion concentration ratio (Sa/Da) of the anion concentration (Sa) at the outer surface to the anion concentration (Da) at the middle point between the inner surface in contact with the substrate and the outer surface.
摘要翻译：本发明提供了单层膜，其不仅具有亲水性，并且在防雾性，防污性，抗静电性和抗缩合性等性能方面优异，而且即使具有大的膜厚度和优异的耐刮擦性也倾向于表现出优异的透明性，以及作为具有单层膜的堆叠。通过制备包含单体组合物和溶剂的混合物获得单层膜，所述单体组合物包含特定单体和具有两个以上（甲基）丙烯酰基并且不含磺酸基，羧基和磷酸基的多价单体特定摩尔比，具有特定溶解度参数的溶剂; 将混合物施加到基材上并除去至少一部分溶剂; 并且使单体组合物聚合以制备具有至少一个选自磺酸基，羧基和磷酸基的阴离子亲水基团的单层膜和阴离子浓度（Sa）的特定阴离子浓度比（Sa / Da）外表面与底物接触的内表面与外表面之间的中点处的阴离子浓度（Da）。

6. 发明授权

US09034464B2 Single layer film and hydrophilic material comprising the same 有权
标题翻译：单层膜和包含其的亲水材料
公开(公告)号：US09034464B2
公开(公告)日：2015-05-19
申请号：US13812779
申请日：2011-07-25
申请人： Koju Okazaki
发明人： Koju Okazaki
IPC分类号： C08G75/24 , C08F2/38 , C09D4/00 , C08J7/04 , C08F222/10
CPC分类号： C08G75/24 , C08F2/38 , C08F222/1006 , C08J7/047 , C09D4/00
摘要： There is stably provided a hydrophilic cured product, such as a single-layer film, in which anionic hydrophilic groups are concentrated at a surface that is in contact with the air and which is excellent in transparency and adhesion to a substrate and tends to be rarely cracked. The hydrophilic cured product or single-layer film comprising a resin composition is produced by applying a mixture containing a polyvalent monomer (II) having two or more (meth) acryloyl groups and a compound (IV) having a specific group and a sulfonic acid group to a substrate or the like, drying the mixture if necessary, and then performing polymerization.
摘要翻译：稳定地提供亲水性固化物，例如单层膜，其中阴离子亲水基团在与空气接触的表面上浓缩，并且透明性和对基材的粘合性优异，并且倾向于很少破裂了含有树脂组合物的亲水性固化物或单层膜通过涂布含有具有两个以上（甲基）丙烯酰基的多元单体（II）和具有特定基团和磺酸基的化合物（IV）加入到基材等中，根据需要干燥混合物，然后进行聚合。

7. 发明授权

US5955206A Polysulfide-based resin composition, polysulfide-based resin, and optical material comprising the resin 失效
标题翻译：聚硫醚系树脂组合物，聚硫醚系树脂，以及包含该树脂的光学材料
公开(公告)号：US5955206A
公开(公告)日：1999-09-21
申请号：US640442
申请日：1996-04-30
申请人： Koju Okazaki , Chitoshi Shimakawa , Mamoru Tanaka , Yoshinobu Kanemura , Teruyuki Nagata , Yoshihiro Irizato , Shinichi Umeda
发明人： Koju Okazaki , Chitoshi Shimakawa , Mamoru Tanaka , Yoshinobu Kanemura , Teruyuki Nagata , Yoshihiro Irizato , Shinichi Umeda
IPC分类号： C08G18/38 , C08G59/66 , G02B1/04 , B29B1/02
CPC分类号： C08G59/66 , C08G18/3876 , G02B1/041
摘要： A composition for polysulfide-based resin comprising a polythiol having 4 or more functional groups and a compound having a reactive unsaturated bond(s) and/or b epoxy group(s) and/or c iso(thio)cyanato group(s) in one molecule (however, a+b+c.gtoreq.2, and a and b are not simultaneously 0). A polysulfide-based resin obtained by curing the composition, an optical material comprising the resin, a lens consisting of the optical material and a method for producing the polysulfide-based resin are also set forth.
摘要翻译：一种用于多硫化物基树脂的组合物，其包含具有4个或更多个官能团的多硫醇和具有一个或多个反应性不饱和键和/或b个环氧基和/或c（硫代）氰基的化合物，一个分子（然而，a + b + c> / = 2，a和b不同时为0）。还提出了通过固化组合物获得的聚硫化物基树脂，包含树脂的光学材料，由光学材料组成的透镜和用于制备多硫化物基树脂的方法。

8. 发明授权

US5608115A Polythiol useful for preparing sulfur-containing urethane-based resin and process for producing the same 失效
标题翻译：用于制备含硫氨基甲酸酯基树脂的聚硫醇及其制备方法
公开(公告)号：US5608115A
公开(公告)日：1997-03-04
申请号：US373083
申请日：1995-01-17
申请人： Koju Okazaki , Yoshinobu Kanemura , Teruyuki Nagata
发明人： Koju Okazaki , Yoshinobu Kanemura , Teruyuki Nagata
IPC分类号： G02B1/04 , C07C319/20 , C07C321/14 , C08G18/30 , C08G18/38 , C08G18/52 , C08G18/77
CPC分类号： C08G18/775 , C07C321/14 , C08G18/3876 , C08G18/52 , G02B1/041
摘要： A novel polythiol having four or more functional groups, a process for producing the polythiol comprising reacting thiourea with a specific compound, a sulfur-containing urethane-based resin prepared from the polythiol and a lens made of the resin. The resin has a high refractive index, and low dispersion of refractive index, is lightweight, colorless and transparent, has no optical distortion, and has excellent characteristics in weatherability, dye-affinity, heat resistance, impact resistance and machinability.
摘要翻译：一种具有四个或更多个官能团的新型多硫醇，一种制备多硫醇的方法，包括使硫脲与特定化合物反应，由多硫醇制备的含硫氨基甲酸酯基树脂和由该树脂制成的透镜。该树脂折射率高，折射率分散性低，重量轻，无色透明，无变形，耐候性，染料亲合性，耐热性，耐冲击性和切削性优异。

9. 发明授权

US5302749A Stabilizing method of isocyanate compounds and isocyanate compositions stabilized thereby 失效
标题翻译：由此稳定异氰酸酯化合物和异氰酸酯组合物的稳定方法
公开(公告)号：US5302749A
公开(公告)日：1994-04-12
申请号：US852724
申请日：1992-03-17
申请人： Teruyuki Nagata , Hiroyuki Yamashita , Masahiko Kusumoto , Koju Okazaki
发明人： Teruyuki Nagata , Hiroyuki Yamashita , Masahiko Kusumoto , Koju Okazaki
IPC分类号： C07C263/18 , C08G18/70
CPC分类号： C08G18/70 , C07C263/18 , C07C265/14 , C08G18/7642
摘要： A method for stabilizing an isocyanate compound by adding 10-5000 ppm of phenol to the isocyanate compound, and also an isocyanate composition so stabilized. In the isocyanate composition stabilized by the above method, coloring due to time-dependent changes and the occurrence of turbidity through self-polymerization are both suppressed so that it shows outstanding storage stability compared with a corresponding isocyanate composition containing a conventional stabilizer.
摘要翻译：通过向异氰酸酯化合物中加入10-5000ppm的苯酚以及如此稳定的异氰酸酯组合物来稳定异氰酸酯化合物的方法。在通过上述方法稳定的异氰酸酯组合物中，由于时间依赖性变化引起的着色和通过自聚合的浊度的发生都被抑制，因此与含有常规稳定剂的相应的异氰酸酯组合物相比，它具有优异的储存稳定性。

10. 发明授权

US5084545A Resin having a large refractive index, lenses comprising the resin and process for preparing the lens 失效
$Resin having a large refractive index, lenses comprising the resin and process for preparing the lens$
标题翻译：树脂具有大的折射指数，包含树脂的镜片和准备镜片的过程
公开(公告)号：US5084545A
公开(公告)日：1992-01-28
申请号：US379378
申请日：1989-07-13
申请人： Teruyuki Nagata , Koju Okazaki , Tohru Miura
发明人： Teruyuki Nagata , Koju Okazaki , Tohru Miura
IPC分类号： G02B1/04 , B29C33/60 , B29C39/00 , B29C39/02 , B29D11/00 , B29K75/00 , B29K105/32 , B29L11/00 , C08G18/32 , C08G18/38 , C08G18/42 , C08G18/46 , C08G18/48 , C08G18/50 , C08G18/70 , C08G18/72 , C08G18/76 , C08G18/77 , C08G18/78
CPC分类号： B29C33/60 , C08G18/3203 , C08G18/3221 , C08G18/381 , C08G18/3863 , C08G18/3874 , C08G18/3876 , C08G18/72 , C08G18/76 , C08G18/775 , C08G18/7893
摘要： The present invention relates to a process for producing a resin useful in plastic lenses, to plastic lenses containing the resin and to a process for producing the lenses.

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