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1. 发明授权

US4006274A 2,4,6-Tris(carbamoylmethylamino)-1,3,5,-s-triazine 失效
标题翻译： 2,4,6-三（氨基甲酰基甲基氨基）-1,3,5，-s-三嗪
公开(公告)号：US4006274A
公开(公告)日：1977-02-01
申请号：US615015
申请日：1975-09-19
申请人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
发明人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
IPC分类号： C07D251/70 , B05D3/02
CPC分类号： C07D251/70
摘要： 2,4,6-Tris(carbamoylmethylamino)-1,3,5-s-triazine, abbreviated TCMT, is prepared by the reaction of 2,4,6-tris(carbethoxymethylamino)-1,3,5-s-triazine with ammonia. The methylol derivative of TCMT is prepared and applied to cotton textiles and blends of cotton and polyester to impart wrinkle recovery thereto.
摘要翻译：通过2,4,6-三（乙酰氧基甲基氨基）-1,3,5-s-三嗪的反应制备2,4,6-三（氨基甲酰基甲基氨基）-1,3,5-s-三嗪，缩写为TCMT 与氨。制备TCMT的羟甲基衍生物，并应用于棉纺织物和棉和聚酯的共混物以赋予皱纹恢复性。

2. 发明授权

UST100601I4 Compositions and processes for producing flame retardant textile materials based on methylolaminotrihalopropyl triazines and antimony oxides 失效
标题翻译：基于甲基丙烯酰氧基丙烯酸酯和抗氧化剂生产阻燃纺织材料的组合物和方法
公开(公告)号：UST100601I4
公开(公告)日：1981-05-05
申请号：US134014
申请日：1980-03-26
申请人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
发明人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
IPC分类号： D06M11/47 , D06M13/358 , D06M13/44 , D06M9/00 , D06M13/34
CPC分类号： D06M11/47 , D06M13/358
摘要： The tetramethylol derivatives of 2,4-diamino-6(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-diamino-6(3,3,3-trichloro-1-propyl)-1,3,5-triazine, namely: 2,4-bis[di(hydroxymethyl)amino]-6-(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-bis[di(hydroxymethyl)amino]-6-(3,3,3-trichloro-1-propyl)-1,3,5-triazine, respectively, were used in combination with colloidal antimony oxides and or water emulsifying agents and suitable solvent to impart durable flame-retardancy to cellulosic materials, protein fibers such as wool, and to blends of cellulosic materials and synthetic fibers, particularly to cotton textiles or textiles composed of blends of cotton and polyester. Afterglow was eliminated by the use of small amounts of reactive phosphorus compounds.

3. 发明授权

US3979533A .alpha.,.alpha.'-Bis-(phosphono)dicarboxylic acid derivatives 失效
标题翻译： {60，{60 {40-双（膦酰））二羧酸衍生物
公开(公告)号：US3979533A
公开(公告)日：1976-09-07
申请号：US627326
申请日：1975-10-30
申请人： Jerry P. Moreau , Leon H. Chance , Gordon J. Boudreaux , George L. Drake, Jr.
发明人： Jerry P. Moreau , Leon H. Chance , Gordon J. Boudreaux , George L. Drake, Jr.
IPC分类号： C07F9/38 , C07F9/40 , D06M13/288 , B05D3/02
CPC分类号： D06M13/288 , C07F9/3869 , C07F9/4046
摘要： Derivatives of dicarboxylic acids containing a phosphono group in the alpha and alpha prime position have been made. These have a wide variety of uses as intermediates. Specifically, one of the new compounds is useful in imparting wrinkle resistance as well as flame retardance to cellulosic textiles.
摘要翻译：已经制备了在α和α主要位置含有膦酰基的二羧酸的衍生物。这些作为中间体具有广泛的用途。具体地说，其中一种新化合物可用于赋予纤维素纺织品抗皱性和阻燃性。

4. 发明授权

US3933944A .alpha..alpha.'-Bis-(phosphono)dicarboxylic acid derivatives 失效
标题翻译： {60 {60 {40-双（膦酰））二羧酸衍生物
公开(公告)号：US3933944A
公开(公告)日：1976-01-20
申请号：US311609
申请日：1972-12-04
申请人： Jerry P. Moreau , Leon H. Chance , Gordon J. Boudreaux , George L. Drake, Jr.
发明人： Jerry P. Moreau , Leon H. Chance , Gordon J. Boudreaux , George L. Drake, Jr.
IPC分类号： C07F9/38 , C07F9/40 , D06M13/288
CPC分类号： D06M13/288 , C07F9/3869 , C07F9/4046 , Y10S428/921
摘要： Derivatives of dicarboxylic acids containing a phosphono group in the alpha and alpha prime position have been made. These have a wide variety of uses as intermediates. Specifically, one of the new compounds is useful in imparting wrinkle resistance as well as flame retardance to cellulosic textiles.
摘要翻译：已经制备了在α和α主要位置含有膦酰基的二羧酸的衍生物。这些作为中间体具有广泛的用途。具体地说，其中一种新化合物可用于赋予纤维素纺织品抗皱性和阻燃性。

5. 发明授权

US4067687A Phosphorus, nitrogen, bromine containing polymers and process for producing flame retardant textiles 失效
标题翻译：含磷，氮，溴的聚合物和制造阻燃纺织品的方法
公开(公告)号：US4067687A
公开(公告)日：1978-01-10
申请号：US652277
申请日：1976-01-23
申请人： Darrell J. Donaldson , George L. Drake, Jr. , John V. Beninate , Wilson A. Reeves , Donald J. Daigle
发明人： Darrell J. Donaldson , George L. Drake, Jr. , John V. Beninate , Wilson A. Reeves , Donald J. Daigle
IPC分类号： D06M15/431 , D06M15/673 , D06M1/00
CPC分类号： D06M15/673 , D06M15/431 , Y10S428/921
摘要： Textile treating compositions containing the elements phosphorus, nitrogen, and bromine and the processes for imparting flame resistance to organic fibrous materials have been prepared. This is accomplished by impregnating the textile treating compositions consisting of (1) tris(hydroxymethyl)phosphine mixed with nitrogenous compounds containing at least two members of the group hydrogen and methylol radicals (--CH.sub.2 OH) attached to trivalent nitrogen atoms, or (2) soluble methylol phosphine adducts which contain one or more methylol phosphine radicals (P--CH.sub.2 OH) prepared by reacting tris(hydroxymethyl)phosphine with an amide or amine which contains one or more hydrogens attached to a trivalent nitrogen with an organic bromine containing material with at least 10% bromine in the form of bromine atoms attached to carbon atoms, in proportions selected so that generally the phosphorus contained in structures of the group (--CH.sub.2).sub.3 P amount to a small portion of the total weight of the mixture, and heating to cause insolubilization in or on the fibrous structure.
摘要翻译：已经制备了含有磷，氮和溴元素的纺织品处理组合物和赋予有机纤维材料阻燃性的方法。这是通过浸渍由（1）三（羟甲基）膦混合的纺织品处理组合物实现的，所述组合物与含有至少两个连接到三价氮原子的氢和羟甲基（-CH 2 OH）的成员的含氮化合物混合，或（2）可溶的含有一个或多个羟甲基膦加成物的羟甲基膦加合物（P-CH 2 OH），其通过使三（羟甲基）膦与含有一个或多个与三价氮连接的氢的酰胺或胺与含有有机溴的材料与至少10 以溴原子连接碳原子形式的溴的比例按所选择的比例，使得通常基团（-CH 2）3 P的结构中所含的磷相当于混合物总重量的一小部分，并加热以引起不溶解在纤维结构中或之上。

6. 发明授权

US3987098A Quaternary arylaminoalkyl phosphonium salts 失效
标题翻译：季铵盐氨基磷酸盐钠盐
公开(公告)号：US3987098A
公开(公告)日：1976-10-19
申请号：US529974
申请日：1974-12-05
申请人： Arlen W. Frank , George L. Drake, Jr.
发明人： Arlen W. Frank , George L. Drake, Jr.
IPC分类号： C07F9/50 , C07F9/54 , C07F9/6584 , C08K5/49 , C08K5/50 , D06M13/285 , C07C87/48
CPC分类号： D06M13/285 , C07F9/5004 , C07F9/5407 , C07F9/6584 , C08K5/49 , C08K5/50
摘要： Novel quaternary arylaminoalkyl phosphonium salts having the formula [(ArNHCHR).sub.4 P].sup.+X.sup.-, where R is a radical selected from the group consisting of hydrogen, alkyl and aryl, Ar is aryl, and X is halogen, are prepared by the reaction of primary aromatic amines with quaternary hydroxyalkyl phosphonium salts having the formula [(HOCHR).sub.4 P].sup.+X.sup.-, where R and X are similarly defined. The compounds of this invention are useful as flame retardant for cotton, plasticizers, lubricant additives, and surface-active agents.

7. 发明授权

US3954866A Process for the preparation of quaternary arylaminoalkyl phosphonium salts 失效
标题翻译：制备季芳基氨基烷基鏻盐的方法
公开(公告)号：US3954866A
公开(公告)日：1976-05-04
申请号：US529975
申请日：1974-12-05
申请人： Arlen W. Frank , George L. Drake, Jr.
发明人： Arlen W. Frank , George L. Drake, Jr.
IPC分类号： C07F9/50 , C07F9/54 , C07F9/6584 , C08K5/49 , C08K5/50 , D06M13/285 , C07C85/06
CPC分类号： D06M13/285 , C07F9/5004 , C07F9/5407 , C07F9/6584 , C08K5/49 , C08K5/50
摘要： Novel quaternary arylaminoalkyl phosphonium salts having the formula [(ArNHCHR).sub.4 P].sup.+X.sup.-, where R is a radical selected from the group consisting of hydrogen, alkyl and aryl, Ar is aryl, and X is halogen, are prepared by the reaction of primary aromatic amines with quaternary hydroxyalkyl phosphonium salts having the formula [(HOCHR).sub.4 P].sup.+X.sup.-, where R and X are similarly defined. The compounds of this invention are useful as flame retardant for cotton, plasticizers, lubricant additives, and surface-active agents.
摘要翻译：具有式[（ArNHCHR）4 P] + X'的新型季芳基氨基烷基鏻盐，其中R是选自氢，烷基和芳基的基团，Ar是芳基，X是卤素。通过伯芳族胺与具有式[（HOCHR）4 P] +）的季羟烷基鏻盐的反应，其中R和X的定义类似。本发明的化合物可用作棉花，增塑剂，润滑剂添加剂和表面活性剂的阻燃剂。

8. 发明授权

US3949108A Process for producing fire resistant organic textile materials 失效
标题翻译：生产耐火有机纺织材料的工艺
公开(公告)号：US3949108A
公开(公告)日：1976-04-06
申请号：US365895
申请日：1973-06-01
申请人： Darrell J. Donaldson , Floyd L. Normand , George L. Drake, Jr. , Wilson A. Reeves
发明人： Darrell J. Donaldson , Floyd L. Normand , George L. Drake, Jr. , Wilson A. Reeves
IPC分类号： D06M11/47 , D06M15/252 , D06M15/423 , C09K3/28
CPC分类号： D06M15/423 , D06M11/47 , D06M15/252 , Y10S428/921
摘要： Organic fibrous materials especially cellulosic and other textiles are rendered flame resistant upon treatment with an emulsion containing either (1) an organic bromine containing material having at least 65% bromine such as polyvinylbromide, (2) polyvinylbromide and an N-methylol agent such as trimethylolmethylglycoluril, (3) polyvinylbromide and a metal oxide such as antimony oxide, and (4) polyvinylbromide, N-methylol agent and metal oxide. The emulsions are applied to various fibers by the pad-dry-cure technique. The finish contained the added quality of wrinkle resistance and rot resistance. The treated textiles, including polyester/cotton blends remain highly flame resistant through innumerable laundry cycles.
摘要翻译：有机纤维材料，特别是纤维素和其它纺织品在用含有（1）含有至少65％溴的有机溴物质如聚溴乙烯，（2）聚乙烯基溴和N-羟甲基试剂如三羟甲基甲基甘脲，（3）聚溴乙烯和金属氧化物如氧化锑，和（4）聚乙烯基溴，N-羟甲基试剂和金属氧化物。乳液通过垫 - 干固化技术施加到各种纤维上。整理含有抗皱和抗腐蚀的附加品质。被处理的纺织品，包括聚酯/棉混纺，经过无数的洗衣循环，保持高度的阻燃性。

9. 发明授权

US3954400A Phosphorus, nitrogen, bromin containing polymers and process for producing flame retardant textiles 失效
标题翻译：磷，氮，溴化聚合物和制造阻燃纺织品的方法
公开(公告)号：US3954400A
公开(公告)日：1976-05-04
申请号：US499810
申请日：1974-08-22
申请人： Wilson A. Reeves , Darrell J. Donaldson , Donald J. Daigle , George L. Drake, Jr. , John V. Beninate
发明人： Wilson A. Reeves , Darrell J. Donaldson , Donald J. Daigle , George L. Drake, Jr. , John V. Beninate
IPC分类号： D06M15/431 , C08G51/24 , D06M13/32 , D06M13/38
CPC分类号： D06M15/431 , Y10S428/921
摘要： Textile treating compositions containing the elements phosphorus, nitrogen, and bromine and the processes for imparting flame resistance to organic fibrous materials have been prepared. This is accomplished by impregnating the textile treating compositions consisting of (1) tris(hydroxymethyl)phosphine mixed with nitrogenous compounds containing at least two members of the group hydrogen and methylol radicals (--CH.sub.2 OH) attached to trivalent nitrogen atoms, or (2) soluble methylol phosphine adducts which contain one or more methylol phosphine radicals (P--CH.sub.2 OH) prepared by reacting tris(hydroxymethyl)phosphine with an amide or amine which contains one or more hydrogens attached to a trivalent nitrogen with an organic bromine containing material with at least 10% bromine in the form of bromine atoms attached to carbon atoms, in proportions selected so that generally the phosphorus contained in structures of the group (--CH.sub.2).sub.3 P amounts to a small portion of the total weight of the mixture, and heating to cause insolubilization in or on the fibrous structure.
摘要翻译：已经制备了含有磷，氮和溴元素的纺织品处理组合物和赋予有机纤维材料阻燃性的方法。这是通过浸渍由（1）三（羟甲基）膦混合的纺织品处理组合物实现的，所述组合物与含有至少两个连接到三价氮原子的氢和羟甲基（-CH 2 OH）的成员的含氮化合物混合，或（2）可溶的含有一个或多个羟甲基膦加成物的羟甲基膦加合物（P-CH 2 OH），其通过使三（羟甲基）膦与含有一个或多个与三价氮连接的氢的酰胺或胺与含有有机溴的材料与至少10 以溴原子连接碳原子的形式的溴，以选定的比例，使得通常基团（-CH 2）3 P的结构中所含的磷相当于混合物总重量的一小部分，并加热以引起不溶解在纤维结构中或之上。

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