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1. 发明授权

US4900324A Agents for non-formaldehyde durable press finishing and textile products therefrom 失效
标题翻译：非甲醛耐久压机加工剂及其纺织品
公开(公告)号：US4900324A
公开(公告)日：1990-02-13
申请号：US229420
申请日：1988-08-08
申请人： Leon H. Chance , Gary F. Danna , Bethlehem K. Andrews
发明人： Leon H. Chance , Gary F. Danna , Bethlehem K. Andrews
IPC分类号： D06M13/137
CPC分类号： D06M13/137
摘要： The acetals, 2,3-dihydroxy-1,1,4,4-tetramethoxybutane, 3,4-dihydroxy-2,5-dimethoxytetrahydrofuran, and glyceraldehyde dimethylacetal, when applied to cotton fabric by conventional pad-dry-cure procedures using special combined acid catalysts, were found to crosslink cellulose hydroxy groups at a very rapid rate (e.g., 20 seconds at 160.degree. C.), thereby imparting improved wrinkle recovery in the range of that required for durable press finishing. Cotton fabrics treated with these acetals have the advantage of no formaldehyde release.
摘要翻译：缩醛，2,3-二羟基-1,1,4,4-四甲氧基丁烷，3,4-二羟基-2,5-二甲氧基四氢呋喃和甘油醛二甲基缩醛，当通过常规的垫干固化程序使用特殊的发现合并的酸催化剂以非常快的速率交联纤维素羟基（例如在160℃下20秒），从而在耐久的压力加工所需的范围内赋予改善的皱纹恢复。用这些缩醛处理的棉织物具有无甲醛释放的优点。

2. 发明授权

US4818243A Wrinkle resistant fabric produced by crosslinking cellulosic materials with acetals of glyceraldehyde 失效
标题翻译：通过用甘油醛的缩醛交联纤维素材料而生产的抗皱织物
公开(公告)号：US4818243A
公开(公告)日：1989-04-04
申请号：US050436
申请日：1987-05-18
申请人： Leon H. Chance , Gary F. Danna
发明人： Leon H. Chance , Gary F. Danna
IPC分类号： D06M13/137 , D06M13/12
CPC分类号： D06M13/137
摘要： Acetals of glyceraldehyde, when applied to cotton fabric by conventional pad-dry-cure procedures using special combined acid catalysts, were found to crosslink the cellulose hydroxyl groups at a very rapid rate (e.g., 10 seconds at 170.degree. C.), thereby imparting improved wrinkle recovery. In particular, the aldehydes studied were the diethyl and dimethyl acetals of glyceraldehyde. The best results were obtained with glyceraldehyde dimethyl acetal.
摘要翻译：甘油醛的缩醛当通过使用特殊组合酸催化剂的常规垫 - 干 - 固化方法应用于棉织物时，发现纤维素羟基以非常快的速率交联（例如，在170℃下10秒），由此赋予改善皱纹恢复。特别地，所研究的醛是甘油醛的二乙基和二甲基缩醛。用甘油醛二甲基缩醛得到最好的结果。

3. 发明授权

US4006274A 2,4,6-Tris(carbamoylmethylamino)-1,3,5,-s-triazine 失效
标题翻译： 2,4,6-三（氨基甲酰基甲基氨基）-1,3,5，-s-三嗪
公开(公告)号：US4006274A
公开(公告)日：1977-02-01
申请号：US615015
申请日：1975-09-19
申请人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
发明人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
IPC分类号： C07D251/70 , B05D3/02
CPC分类号： C07D251/70
摘要： 2,4,6-Tris(carbamoylmethylamino)-1,3,5-s-triazine, abbreviated TCMT, is prepared by the reaction of 2,4,6-tris(carbethoxymethylamino)-1,3,5-s-triazine with ammonia. The methylol derivative of TCMT is prepared and applied to cotton textiles and blends of cotton and polyester to impart wrinkle recovery thereto.
摘要翻译：通过2,4,6-三（乙酰氧基甲基氨基）-1,3,5-s-三嗪的反应制备2,4,6-三（氨基甲酰基甲基氨基）-1,3,5-s-三嗪，缩写为TCMT 与氨。制备TCMT的羟甲基衍生物，并应用于棉纺织物和棉和聚酯的共混物以赋予皱纹恢复性。

4. 发明授权

US3617346A Aziridine adducts of {60 ,{62 -unsaturated nitriles and polymers thereof 失效
标题翻译： {60，{62-氮氧化物及其聚合物的AZIRIDINE ADDUCTS
公开(公告)号：US3617346A
公开(公告)日：1971-11-02
申请号：US3617346D
申请日：1969-03-25
申请人： LEON H CHANCE , DRAKE GEORGE L JUN
发明人： CHANCE LEON H , DRAKE GEORGE L JR
IPC分类号： D06M13/48 , B44D1/092 , D06P3/60
CPC分类号： D06M13/48 , Y10S8/93
摘要： This invention relates to a process for pretreating cellulosic fabrics with acid catalysts, and then impregnating said fabrics with aziridine adducts of Alpha , Beta -unsaturated nitriles.

5. 发明授权

US4405806A Bromine-containing 2,4-diaminotriazines 失效
标题翻译：含溴的2,4-二氨基三嗪
公开(公告)号：US4405806A
公开(公告)日：1983-09-20
申请号：US370009
申请日：1982-04-20
申请人： Leon H. Chance
发明人： Leon H. Chance
IPC分类号： C07D251/18 , C07C101/44
CPC分类号： C07D251/18
摘要： The following new compounds, useful in flame retardant compositions for cotton, are disclosed in the invention:2,4-diamino-6-carbamoylmethyl-1, 3,5-triazine (Ib),2,4-diamino-6-(dibromocyanomethyl)-1,3,5-triazine (IIa),2,4-diamino-6-(dibromocarbamoylmethyl)-1,3,5-triazine (IIb),2,4-diamino-6-(3,5-dibromo-4'-aminophenyl)-1,3,5-triazine (IIc),ethyl N-(2,4,6-tribromophenyl)glycinate (IV),N-(2,4,6-tribromophenyl)glycinamide (V),2,4-bis[di(hydroxymethyl)amino]-6-(3,5-dibromo-4'-aminophenyl)-1,3,5-triazine (III),2,4-diamino-6-(2',4',6'-tribromoanilinomethyl)-1,3,5-triazine (Id), and2,4-bis[di(hydroxymethyl)amino]-6-(2',4',6'-tribromoanilinomethyl)-1,3,5-triazine (VI).
摘要翻译：在本发明中公开了以下可用于棉花阻燃组合物的新化合物：2,4-二氨基-6-氨基甲酰基甲基-1,3,5-三嗪（Ib），2,4-二氨基-6-（二溴氰基甲基）-1,3,5-三嗪（IIa），2,4-二氨基-6-（二溴氨基甲酰基甲基）-1,3,5-三嗪（IIb），2,4-二氨基-6-（3,5-二溴 -4'-氨基苯基）-1,3,5-三嗪（IIc），N-（2,4,6-三溴苯基）甘氨酸乙酯（IV），N-（2,4,6-三溴苯基）甘氨酰胺（V），2,4-双[二（羟甲基）氨基] -6-（3,5-二溴-4'-氨基苯基）-1,3,5-三嗪（III），2,4-二氨基-6-（ 2'，4'，6'-三溴苯胺甲基）-1,3,5-三嗪（Id）和2,4-双[二（羟甲基）氨基] -6-（2'，4'，6'-三溴苯胺基甲基）-1,3,5-三嗪（VI）。

6. 发明授权

US4055720A Diaminotrihalopropyl triazines: and their methylol derivatives 失效
标题翻译：二氨基三卤丙基三嗪：及其羟甲基衍生物
公开(公告)号：US4055720A
公开(公告)日：1977-10-25
申请号：US689771
申请日：1976-05-25
申请人： Leon H. Chance , Judy D. Timpa
发明人： Leon H. Chance , Judy D. Timpa
IPC分类号： C07D251/18 , D06M13/358 , C07D251/48
CPC分类号： C07D251/18 , D06M13/358 , Y10S428/921
摘要： 2,4-Diamino-6(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-diamino-6(3,3,3-trichloro-1-propyl)-1,3,5-triazine were prepared by the reaction of the corresponding methyl or ethyl .gamma.-tribromo-butyrate or methyl or ethyl .gamma.-trichlorobutyrate with biguanide. The N-methylol derivatives of the diaminotrihalopropyl triazines were prepared by the reaction of the triazines with aqueous formaldehyde. Two pure tetramethylol derivatives were prepared, namely: 2,4-bis[bis(hydroxymethyl)amino]-6-(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-bis[bis(hydroxymethyl)amino]-6-(3,3,3-trichloro-1-propyl)-1,3,5-triazine. The tetramethylol derivatives were used to impart durable flame retardancy and wrinkle recovery to cellulosic textiles, particularly to cotton. Flame-retardancy was also imparted to wool and to blends of cotton and polyester.
摘要翻译： 2,4-二氨基-6（3,3,3-三溴-1-丙基）-1,3,5-三嗪和2,4-二氨基-6（3,3,3-三氯-1-丙基） - 通过相应的甲基或乙基γ-三溴丁酸酯或γ-三氯丁酸乙酯与双胍反应制备1,3,5-三嗪。二氨基三卤代丙基三嗪的N-羟甲基衍生物通过三嗪与甲醛水溶液的反应来制备。制备两种纯的四羟甲基衍生物，即2,4-双[双（羟甲基）氨基] -6-（3,3,3-三溴-1-丙基）-1,3,5-三氮杂和2,4 双[双（羟甲基）氨基] -6-（3,3,3-三氯-1-丙基）-1,3,5-三嗪。使用四羟甲基衍生物赋予纤维素纺织品特别是棉花持久的阻燃性和皱纹恢复性。还赋予了羊毛和棉和聚酯的混合物的阻燃性。

7. 发明授权

US4352930A Bromine-containing 2,4-diaminotriazines 失效
标题翻译：含溴的2,4-二氨基三嗪
公开(公告)号：US4352930A
公开(公告)日：1982-10-05
申请号：US276768
申请日：1981-06-24
申请人： Leon H. Chance
发明人： Leon H. Chance
IPC分类号： C07D251/18
CPC分类号： C07D251/18
摘要： The following new compounds, useful in flame retardant compositions for cotton, are disclosed in the invention:2,4-diamino-6-carbamoylmethyl-1,3,5-triazine (Ib),2,4-diamino-6-(dibromocyanomethyl)-1,3,5-triazine (IIa),2,4-diamino-6-(dibromocarbamoylmethyl)-1,3,5-triazine (IIb),2,4-diamino-6-(3,5-dibromo-4'-aminophenyl)-1,3,5-triazine (IIc),ethyl N-(2,4,6-tribromophenyl)glycinate (IV),N-(2,4,6-tribromophenyl)glycinamide (V),2,4-bis[di(hydroxymethyl)amino]-6-(3,5-dibromo-4'-amino-phenyl)-1,3,5-triazine (III),2,4-diamino-6-(2',4',6'-tribromoanilinomethyl)-1,3,5-triazine (Id), and2,4-bis[di(hydroxymethyl)amino]-6-(2',4',6'-tribromoanilinomethyl)-1,3,5-triazine (VI).
摘要翻译：在本发明中公开了以下用于棉花阻燃组合物的新化合物：2,4-二氨基-6-氨基甲酰基甲基-1,3,5-三嗪（Ib），2,4-二氨基-6-（二溴氰基甲基）-1,3,5-三嗪（IIa），2,4-二氨基-6-（二溴氨基甲酰基甲基）-1,3,5-三嗪（IIb），2,4-二氨基-6-（3,5-二溴 -4'-氨基苯基）-1,3,5-三嗪（IIc），N-（2,4,6-三溴苯基）甘氨酸乙酯（IV），N-（2,4,6-三溴苯基）甘氨酰胺（V），2,4-双[二（羟甲基）氨基] -6-（3,5-二溴-4'-氨基 - 苯基）-1,3,5-三嗪（III），2,4-二氨基-6- （2'，4'，6'-三溴苯胺甲基）-1,3,5-三嗪（Id）和2,4-双[二（羟甲基）氨基] -6-（2'，4'，6'- 三溴苯胺甲基）-1,3,5-三嗪（VI）。

8. 发明授权

UST100601I4 Compositions and processes for producing flame retardant textile materials based on methylolaminotrihalopropyl triazines and antimony oxides 失效
标题翻译：基于甲基丙烯酰氧基丙烯酸酯和抗氧化剂生产阻燃纺织材料的组合物和方法
公开(公告)号：UST100601I4
公开(公告)日：1981-05-05
申请号：US134014
申请日：1980-03-26
申请人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
发明人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
IPC分类号： D06M11/47 , D06M13/358 , D06M13/44 , D06M9/00 , D06M13/34
CPC分类号： D06M11/47 , D06M13/358
摘要： The tetramethylol derivatives of 2,4-diamino-6(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-diamino-6(3,3,3-trichloro-1-propyl)-1,3,5-triazine, namely: 2,4-bis[di(hydroxymethyl)amino]-6-(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-bis[di(hydroxymethyl)amino]-6-(3,3,3-trichloro-1-propyl)-1,3,5-triazine, respectively, were used in combination with colloidal antimony oxides and or water emulsifying agents and suitable solvent to impart durable flame-retardancy to cellulosic materials, protein fibers such as wool, and to blends of cellulosic materials and synthetic fibers, particularly to cotton textiles or textiles composed of blends of cotton and polyester. Afterglow was eliminated by the use of small amounts of reactive phosphorus compounds.

9. 发明授权

US3979533A .alpha.,.alpha.'-Bis-(phosphono)dicarboxylic acid derivatives 失效
标题翻译： {60，{60 {40-双（膦酰））二羧酸衍生物
公开(公告)号：US3979533A
公开(公告)日：1976-09-07
申请号：US627326
申请日：1975-10-30
申请人： Jerry P. Moreau , Leon H. Chance , Gordon J. Boudreaux , George L. Drake, Jr.
发明人： Jerry P. Moreau , Leon H. Chance , Gordon J. Boudreaux , George L. Drake, Jr.
IPC分类号： C07F9/38 , C07F9/40 , D06M13/288 , B05D3/02
CPC分类号： D06M13/288 , C07F9/3869 , C07F9/4046
摘要： Derivatives of dicarboxylic acids containing a phosphono group in the alpha and alpha prime position have been made. These have a wide variety of uses as intermediates. Specifically, one of the new compounds is useful in imparting wrinkle resistance as well as flame retardance to cellulosic textiles.
摘要翻译：已经制备了在α和α主要位置含有膦酰基的二羧酸的衍生物。这些作为中间体具有广泛的用途。具体地说，其中一种新化合物可用于赋予纤维素纺织品抗皱性和阻燃性。

10. 发明授权

US3972924A 1-(1H,1H-perfluorooctyl)-1,3-trimethylenediphosphonic tetrachloride 失效
标题翻译： 1-（1H，1H-全氟辛基）-1,3-三亚甲基二膦酸四氯化物
公开(公告)号：US3972924A
公开(公告)日：1976-08-03
申请号：US630375
申请日：1975-11-10
申请人： Leon H. Chance , Jerry P. Moreau
发明人： Leon H. Chance , Jerry P. Moreau
IPC分类号： C07F9/38 , D06M13/493 , D06M15/356
CPC分类号： D06M15/3564 , C07F9/3808 , C07F9/3839 , D06M13/493
摘要： Perfluoroalkyl iodide monomer and telomer ester adducts of diethyl vinylphosphonate were prepared by free radical addition. Iodine of these adducts was replaced by hydrogen, and derivatives of the reduced phosphonate adducts were prepared, which include phosphonic acids, acid chlorides, and aziridinyl phosphine oxides. The aziridinyl phosphine oxides are used to impart oil and water repellency to cellulosic textiles. The other derivatives are useful as chemical intermediates as well as potential foaming agents.
摘要翻译：通过自由基加成制备乙烯基膦酸二乙酯的全氟烷基碘单体和调聚酯加成物。这些加合物的碘被氢代替，并且制备还原膦酸酯加合物的衍生物，其包括膦酸，酰氯和氮丙啶基氧化膦。氮杂环丙烷氧化膦用于赋予纤维素纺织品防油和防水性能。其他衍生物可用作化学中间体以及潜在的发泡剂。

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