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1. 发明授权

US10653824B2 Two-dimensional materials and uses thereof 有权
公开(公告)号：US10653824B2
公开(公告)日：2020-05-19
申请号：US15099588
申请日：2016-04-14
申请人： Lockheed Martin Corporation
发明人： Peter V. Bedworth , Steven Edward Bullock , Sarah M. Simon , Steven W. Sinton , John B. Stetson, Jr. , Jacob L. Swett , Scott E. Heise
IPC分类号： A61M1/16 , H01J37/305 , B01D61/24 , B01D71/02 , B01D67/00 , B01D69/10
摘要： Various systems and methods relating to two-dimensional materials such as graphene. A membrane include a cross-linked graphene platelet polymer that includes a plurality of cross-linked graphene platelets. The cross-linked graphene platelets include a graphene portion and a cross-linking portion. The cross-linking portion contains a 4 to 10 atom link. The cross-linked graphene platelet polymer is produced by reaction of an epoxide functionalized graphene platelet and a (meth)acrylate or (meth)acrylamide functionalized cross-linker.

2. 发明授权

US10281550B2 Spin relaxometry based molecular sequencing 有权
公开(公告)号：US10281550B2
公开(公告)日：2019-05-07
申请号：US15350303
申请日：2016-11-14
申请人： Lockheed Martin Corporation
发明人： Steven W. Sinton , Peter V. Bedworth , Jacob Louis Swett
IPC分类号： G01R33/60 , C12Q1/6869 , G01R33/12 , G01N24/10
摘要： A method and system for detecting a target molecule. The method includes allowing a fluid containing the target molecule to pass by a complementary moiety attached to a paramagnetic ion so as to cause the complementary moiety and the paramagnetic ion to change a position. A magnetic effect change caused by the change in position of the paramagnetic ion is detected. The target molecule is identified based on the identity of the complementary moiety and the detected magnetic effect change.

3. 发明授权

US10017852B2 Method for treating graphene sheets for large-scale transfer using free-float method 有权
公开(公告)号：US10017852B2
公开(公告)日：2018-07-10
申请号：US15099464
申请日：2016-04-14
申请人： Lockheed Martin Corporation
发明人： Scott E. Heise , Peter V. Bedworth , Jacob L. Swett , Steven W. Sinton
IPC分类号： C23C16/26 , C23C16/01 , C23C16/56 , C23F1/18
CPC分类号： C23C16/26 , C23C16/01 , C23C16/56 , C23F1/18
摘要： A method for transferring a graphene sheet from a copper substrate to a functional substrate includes forming the graphene sheet on the copper substrate using chemical vapor deposition, and irradiating the graphene sheet disposed on the copper substrate with a plurality of xenon ions using broad beam irradiation to form a prepared graphene sheet. The prepared graphene sheet is resistant to forming unintentional defects induced during transfer of the prepared graphene sheet to the functional substrate. The method further includes removing the copper substrate from the prepared graphene sheet using an etchant bath, floating the prepared graphene sheet in a floating bath, submerging the functional substrate in the floating bath, and decreasing a fluid level of the floating bath to lower the prepared graphene sheet onto the functional substrate.

4. 发明授权

US09844757B2 Separation membranes formed from perforated graphene and methods for use thereof 有权
公开(公告)号：US09844757B2
公开(公告)日：2017-12-19
申请号：US14656580
申请日：2015-03-12
申请人： LOCKHEED MARTIN CORPORATION
发明人： Steven W. Sinton , Peter V. Bedworth , Padraig Moloney
IPC分类号： B01D69/12 , B01D53/22 , B01D71/02 , B01D71/68 , C10L3/10 , B01D67/00
CPC分类号： B01D69/12 , B01D53/228 , B01D67/0062 , B01D67/0079 , B01D71/021 , B01D2256/245 , B01D2257/304 , B01D2257/504 , B01D2257/80 , C10L3/103 , C10L3/104 , C10L3/106 , C10L2290/548 , Y02C10/10
摘要： Perforated graphene sheets can be used in forming separation membranes. Separation membranes of the present disclosure, which can be used in gas separation processes in some embodiments, can include one or more polymer layers and one or more layers of perforated graphene. Methods for separating a gas mixture can include contacting a gas mixture with the separation membranes, and transiting one or more of the gases through the perforated graphene so as to affect separation.

5. 发明申请

US20170035943A1 IMPLANTABLE GRAPHENE MEMBRANES WITH LOW CYTOTOXICITY 审中-公开
标题翻译：具有低细胞毒性的可植入的石墨膜
公开(公告)号：US20170035943A1
公开(公告)日：2017-02-09
申请号：US15099193
申请日：2016-04-14
申请人： Lockheed Martin Corporation
发明人： Sarah M. SIMON , Jacob L. Swett , Peter V. Bedworth , Scott E. Heise
IPC分类号： A61L31/02 , A61L31/00 , A61L31/10 , A61L31/16 , A61L31/08 , A61L31/06 , A61L31/04
CPC分类号： A61L31/024 , A61L31/084 , A61L31/122 , A61L31/146 , A61L31/16 , A61L2300/62 , A61L2300/64 , A61L2420/04 , A61L2420/08
摘要： Two-dimensional materials can be formed into enclosures for various substances and a substrate layer can be provided on an outside and/or on an inside of the enclosure, wherein the enclosure is not cytotoxic. The enclosures can be exposed to an environment, such as a biological environment (in vivo or in vitro), where the fibrous layer can promote vascular ingrowth. One or more substances within the enclosure can be released into the environment, one or more selected substances from the environment can enter the enclosure, one or more selected substances from the environment can be prevented from entering the enclosure, one or more selected substances can be retained within the enclosure, or combinations thereof. The enclosure can, for example, allow a sense-response paradigm to be realized. The enclosure can, for example, provide immunoisolation for materials, such as living cells, retained therein.
摘要翻译：二维材料可以形成为各种物质的外壳，并且可以在外壳的外部和/或内部提供基底层，其中外壳不是细胞毒性的。外壳可以暴露于诸如生物环境（体内或体外）的环境中，其中纤维层可以促进血管向内生长。外壳内的一种或多种物质可以释放到环境中，来自环境的一种或多种选择的物质可以进入外壳，可以防止来自环境的一种或多种选择的物质进入外壳，一种或多种选择的物质可以是保持在外壳内，或其组合。例如，外壳可以允许实现感应响应范例。外壳可以例如为保留在其中的材料（例如活细胞）提供免疫隔离。

6. 发明授权

US09169575B1 Methods for releasing graphene from a metal substrate by electrowetting 有权
标题翻译：通过电润湿从金属基底释放石墨烯的方法
公开(公告)号：US09169575B1
公开(公告)日：2015-10-27
申请号：US14195802
申请日：2014-03-03
申请人： LOCKHEED MARTIN CORPORATION
发明人： Peter V. Bedworth , Jacob Louis Swett
IPC分类号： H01L21/30 , C25D1/14 , H01L21/311 , H01L21/308 , C23F1/00
CPC分类号： C25D1/14 , C01B32/194 , C23C18/1204 , C23C18/1254 , H01L21/02365 , H01L21/02425 , H01L21/02527 , H01L21/02664
摘要： It is often desirable to release graphene from its growth substrate. Present graphene release techniques can damage the graphene and produce significant quantities of hazardous waste. Electrowetting techniques can be used in alternative approaches for releasing graphene from its growth substrate. Methods for releasing graphene by electrowetting can include providing a metal substrate having graphene adhered thereto, applying a dielectric layer to the graphene to form a coated structure, placing the coated structure in a liquid medium, establishing an electrical potential between the metal substrate and a conductor disposed proximate to at least a portion of the dielectric layer such that the electrical potential induces infiltration of the liquid medium between at least a portion of the metal substrate and the graphene, and releasing the graphene from the metal substrate in the presence of the infiltrated liquid medium. The electrical potential can be maintained until the graphene is released.
摘要翻译：通常希望从其生长基质中释放石墨烯。目前的石墨烯释放技术可能会损坏石墨烯并产生大量危险废物。电润湿技术可用于从其生长衬底释放石墨烯的替代方法。通过电润湿释放石墨烯的方法可以包括提供具有粘附到其上的石墨烯的金属基底，向石墨烯施加电介质层以形成涂覆结构，将涂覆结构放置在液体介质中，在金属基底和导体之间建立电位设置在电介质层的至少一部分附近，使得电势在金属衬底和石墨烯的至少一部分之间引起液体介质的渗透，并且在渗透液体存在下从金属衬底释放石墨烯中。可以保持电位，直到石墨烯被释放。

7. 发明授权

US10696424B2 Spacecraft structures incorporating graphene and operation thereof 有权
公开(公告)号：US10696424B2
公开(公告)日：2020-06-30
申请号：US15196745
申请日：2016-06-29
申请人： LOCKHEED MARTIN CORPORATION
发明人： Vadim Khayms , Steven W. Sinton , Peter V. Bedworth
IPC分类号： B64G1/10 , B64G1/22 , B64G1/40 , B64G1/44 , B64G1/58 , B64G1/66
摘要： Functional components of spacecraft structures can be subject to detrimental impacts by energetic particles produced from an electric propulsion system. A graphene coating applied to a functional component can maintain electrical conductivity upon a surface of the functional component, thereby allowing charge dissipation to take place, while also resisting sputtering erosion resulting from impacts of the energetic particles. Accordingly, spacecraft structures can include an electric propulsion system, a functional component that is at least partially impacted by an outflow of the electric propulsion system, and a graphene coating upon the functional component. Methods for operating such spacecraft structures can include generating an outflow of energetic particles from an electric propulsion system of a spacecraft structure, and at least partially impacting the outflow of energetic particles upon a functional component of the spacecraft structure, where the functional component has a graphene coating thereon.

8. 发明授权

US10677953B2 Magneto-optical detecting apparatus and methods 有权
公开(公告)号：US10677953B2
公开(公告)日：2020-06-09
申请号：US15610526
申请日：2017-05-31
申请人： LOCKHEED MARTIN CORPORATION
发明人： John B. Stetson , Arul Manickam , Peter G. Kaup , Gregory Scott Bruce , Wilbur Lew , Joseph W. Hahn , Nicholas Mauriello Luzod , Kenneth Michael Jackson , Jacob Louis Swett , Peter V. Bedworth , Steven W. Sinton , Duc Huynh , Michael John Dimario , Jay T. Hansen , Andrew Raymond Mandeville , Bryan Neal Fisk , Joseph A. Villani , Jon C. Russo , David Nelson Coar , Julie Lynne Miller , Anjaney Pramod Kottapalli , Gary Edward Montgomery , Margaret Miller Shaw , Stephen Sekelsky , James Michael Krause , Thomas J. Meyer
IPC分类号： G01V3/14 , G01R33/032 , G01R33/26 , G01V3/10
摘要： A system for magnetic detection includes a magneto-optical defect center material including at least one magneto-optical defect center that emits an optical signal when excited by an excitation light; a radio frequency (RF) exciter system configured to provide RF excitation to the magneto-optical defect center material; an optical light source configured to direct the excitation light to the magneto-optical defect center material; and an optical detector configured to receive the optical signal emitted by the magneto-optical defect center material.

9. 发明授权

US10376845B2 Membranes with tunable selectivity 有权
公开(公告)号：US10376845B2
公开(公告)日：2019-08-13
申请号：US15099289
申请日：2016-04-14
申请人： Lockheed Martin Corporation
发明人： Jacob Louis Swett , Sarah M. Simon , Peter V. Bedworth
IPC分类号： B01D69/12 , A61M1/16 , B32B37/14 , B32B37/06 , B32B38/00 , A61M37/00 , A61K47/02 , A61M1/34 , B01D71/02 , B01D67/00 , B01D65/00 , B01D61/02 , C02F1/44 , A61K9/70 , B01D69/02 , B32B9/00 , C01B32/194 , C02F3/12
摘要： Some embodiments comprise membranes comprising a first layer comprising a porous graphene-based material; a second layer comprising a porous graphene-based material; a channel positioned between the first layer and the second layer, wherein the channel has a tunable channel diameter; and at least one spacer substance positioned in the channel, wherein the spacer substance is responsive to the environmental stimulus. In some cases, the membranes have more than two layers of porous graphene-based material. Permeability of a membrane can be altered by exposing the membrane to an environmental stimulus. Membranes can be used in methods of water filtration, immune-isolation, timed drug release (e.g., sustained or delayed release), hemodialysis, or hemofiltration.

10. 发明申请

US20170299537A1 METHODS FOR IN SITU MONITORING AND CONTROL OF DEFECT FORMATION OR HEALING 审中-公开
公开(公告)号：US20170299537A1
公开(公告)日：2017-10-19
申请号：US15099056
申请日：2016-04-14
申请人： Lockheed Martin Corporation
发明人： Jacob L. Swett , Peter V. Bedworth
IPC分类号： G01N27/20 , G01N27/04 , G01N33/00 , G01N25/72
CPC分类号： G01N27/20 , B82Y40/00 , G01N23/225 , G01N25/72 , G01N27/041 , G01N33/00 , G01N2033/0095 , G01N2223/603 , G01N2223/6462
摘要： Production of perforated two-dimensional materials with holes of a desired size range, a narrow size distribution, and a high and uniform density remains a challenge, at least partially, due to physical and chemical inconsistencies from sheet-to-sheet of the two-dimensional material and surface contamination. This disclosure describes methods for monitoring and adjusting perforation or healing conditions in real-time to address inter- and intra-sheet variability. In situ or substantially simultaneous feedback on defect production or healing may be provided either locally or globally on a graphene or other two-dimensional sheet. The feedback data can be used to adjust perforation or healing parameters, such as the total dose or efficacy of the perforating radiation, to achieve the desired defect state.

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