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1. 发明授权

US09688819B2 Silicone resin composition for optical semiconductors 有权
公开(公告)号：US09688819B2
公开(公告)日：2017-06-27
申请号：US14909165
申请日：2014-07-30
申请人： Wacker Chemie AG
发明人： Frank Sandmeyer , Enno Funk , Georg Loessel
IPC分类号： C08G77/04 , C09D183/04 , C08G77/12 , C08G77/20 , H01L23/29 , H01L33/56 , C08G77/00
CPC分类号： C08G77/04 , C08G77/12 , C08G77/20 , C08G77/70 , C08G77/80 , C09D183/04 , H01L23/296 , H01L33/56 , H01L2924/0002 , C08K5/5403 , C08L83/00 , H01L2924/00
摘要： Addition-crosslinkable silicone resin compositions containing a branched organopolysiloxane bearing each of Si—H groups, alkenyl groups, and aryl groups, and also containing blocks of linear organopolysiloxane free of Si—H and alkenyl groups with a chain length of at least three siloxy groups, and further bearing at least one aryl group, serve as excellent potting compositions for electronic devices, particularly LEDs, with high refractive index and optical transmittance, and wide processing latitude.

2. 发明申请

US20220243015A1 SILICONE COMPOSITION THAT CAN BE CROSS-LINKED TO FORM A SILICONE RESIN COMPOSITE MATERIAL 有权
公开(公告)号：US20220243015A1
公开(公告)日：2022-08-04
申请号：US17612194
申请日：2019-05-17
申请人： Wacker Chemie AG
发明人： Jens Lambrecht , Frank Sandmeyer , Markus Winterer
IPC分类号： C08G77/16 , C08L83/04 , C08K7/14 , C08K7/02 , C08K5/56 , C08G77/00 , C08G77/20 , C08G77/12
摘要： Silicone resin having the general formula where R1 are identical or independently different monovalent hydrocarbon radicals or —OH and R2 are identical or independently different monovalent organofunctional hydrocarbon radicals, olefinically unsaturated hydrocarbon radicals or a hydrogen radical. Where R2 is bonded to the silicon atom via a carbon atom and R2 is a hydrogen radical that is bonded to the silicon atom directly. Where c is 0 or 1, (Ic) present in not less than 5 mol %, (Ia) present in not less than 20 mol %, (Ib) present in not more than 20 mol %, (Id) present in not more than 20 mol %. Not less than 1 mol % of units (Ic) contain a radical R2 that is a hydrogen radical and not less than 1 mol % of (Ic) contain radicals R2 that is an olefinically unsaturated hydrocarbon radical and includes pulverulent and fibrous fillers.

3. 发明授权

US10125225B2 Process for preparing organopolysiloxanes 有权
公开(公告)号：US10125225B2
公开(公告)日：2018-11-13
申请号：US15537163
申请日：2016-07-21
申请人： Wacker Chemie AG
发明人： Frank Sandmeyer , Georg Loessel , Marko Prasse
IPC分类号： C08G77/06 , C08G77/18
摘要： Multistep continuous and semicontinuous hydrolysis and condensation of chlorosilanes with alcohol containing minimal water in a column in a first step to form a silicone resin intermediate, followed by further condensation provides silicone resins in reproducible fashion substantially free of hydrogen chloride, without reactor gelatin.

4. 发明授权

US08748554B2 Production of high-molecular-weight silicone resins 失效
标题翻译：生产高分子量有机硅树脂
公开(公告)号：US08748554B2
公开(公告)日：2014-06-10
申请号：US13687112
申请日：2012-11-28
申请人： Wacker Chemie AG
发明人： Frank Sandmeyer
IPC分类号： C08G77/06
CPC分类号： C08G77/02 , C08G77/06
摘要： Silicone resins with a weight average molecular weight of at least 5000 g/mol and polydispersity of ≦65 are prepared by hydrolyzing and condensing: (A) silicon-bonded alkoxylated and optionally hydroxylated silicone resin intermediate(s), (C) a basic or acidic catalyst or mixture thereof which is not completely self-neutralizing, (D) water, and (E) in the presence of an aliphatic carboxylic ester as the sole process solvent, with the provisos that I) alcohol eliminated in the reaction is removed from the reaction mixture by distillation, II) the catalyst (C) is deactivated by thermal treatment or neutralization, and III) a portion of (E) remains in the final product.
摘要翻译：通过水解和缩合制备重均分子量至少为5000g / mol和多分散性为nlE; 65的硅氧烷树脂：（A）硅键合的烷氧基化和任选羟基化的有机硅树脂中间体，（C）碱性或不是完全自中和的酸性催化剂或其混合物，（D）水和（E）在脂肪族羧酸酯作为唯一的加工溶剂的存在下进行，条件是除去反应中除去的醇通过蒸馏从反应混合物中，II）催化剂（C）通过热处理或中和而失活，和III）部分（E）保留在最终产物中。

5. 发明授权

US11654098B2 Process for preparing organopolysiloane gels 有权
公开(公告)号：US11654098B2
公开(公告)日：2023-05-23
申请号：US16622056
申请日：2017-06-12
申请人： WACKER CHEMIE AG
发明人： Frank Sandmeyer , Christoph Schosser
IPC分类号： A61K8/899 , A61K8/04 , A61Q19/00 , A61K8/895 , C08G77/50 , C08G77/08 , A61K8/891 , C08G77/00
CPC分类号： A61K8/899 , A61K8/042 , A61K8/891 , A61K8/895 , A61Q19/00 , C08G77/08 , C08G77/50 , A61K2800/10 , C08G77/70
摘要： Storage stable organopolysiloxane gels, preparable in commercial quantities are prepared by the hydrosilylation reaction of a silicone resin containing a hydrosilyatable group, a short chain Si—H-functional silicone, and a long chain Si—H-functional silicone.

6. 发明授权

US10696846B2 Siloxane resin compositions 有权
公开(公告)号：US10696846B2
公开(公告)日：2020-06-30
申请号：US16063430
申请日：2016-12-07
申请人： Wacker Chemie AG
发明人： Frank Sandmeyer , Arvid Kuhn , Young-Hyuk Joo , Hyun-Kwan Yang
IPC分类号： C08L83/04 , H01L23/29 , C08G77/20 , C08K5/56 , C08L83/00 , C09D183/04 , H01L33/56 , C08G77/12 , C08G77/08 , C08G77/18 , C08J3/24 , C08G77/00 , C08G77/50
摘要： Unique compositions containing organopolysiloxanes having both silicon-bonded hydrogen and aliphatically unsaturated groups exhibit robust processing characteristics and provide coatings or encapsulations of high transparency which can withstand numerous temperature cycles without failure.

7. 发明授权

US10655014B2 Siloxane resin compositions 有权
公开(公告)号：US10655014B2
公开(公告)日：2020-05-19
申请号：US16063411
申请日：2016-12-07
申请人： Wacker Chemie AG
发明人： Arvid Kuhn , Young-Hyuk Joo , Frank Sandmeyer , Hyun-Kwan Yang
IPC分类号： C08L83/04 , C08K5/56 , C08L83/00 , C08K3/013 , C08K5/00 , C08G77/12 , C08G77/20 , C08G77/00 , C08G77/18 , H01L23/29 , H01L33/56
摘要： Addition curable silicone resin compositions have excellent processing characteristics, and can be used to encapsulate electrical and electronic devices.

8. 发明申请

US20130150547A1 PRODUCTION OF HIGH-MOLECULAR-WEIGHT SILICONE RESINS 失效
标题翻译：生产高分子量有机硅树脂
公开(公告)号：US20130150547A1
公开(公告)日：2013-06-13
申请号：US13687112
申请日：2012-11-28
申请人： WACKER CHEMIE AG
发明人： Frank Sandmeyer
IPC分类号： C08G77/02
CPC分类号： C08G77/02 , C08G77/06
摘要： Silicone resins with a weight average molecular weight of at least 5000 g/mol and polydispersity of ≦65 are prepared by hydrolyzing and condensing: (A) silicon-bonded alkoxylated and optionally hydroxylated silicone resin intermediate(s), (C) a basic or acidic catalyst or mixture thereof which is not completely self-neutralizing, (D) water, and (E) in the presence of an aliphatic carboxylic ester as the sole process solvent, with the provisos that I) alcohol eliminated in the reaction is removed from the reaction mixture by distillation, II) the catalyst (C) is deactivated by thermal treatment or neutralization, and III) a portion of (E) remains in the final product.
摘要翻译：通过水解和缩合制备重均分子量至少为5000g / mol和多分散性为65的硅树脂：（A）硅键合的烷氧基化和任选羟基化的有机硅树脂中间体，（C）碱性或酸性催化剂或其混合物，其不完全自中和，（D）水和（E）在脂肪族羧酸酯作为唯一的加工溶剂的存在下，条件是将I）在反应中除去的醇从蒸馏反应混合物，II）催化剂（C）通过热处理或中和而失活，和III）部分（E）保留在最终产物中。

9. 发明授权

US10683434B2 Organocopolymer dispersions 有权
公开(公告)号：US10683434B2
公开(公告)日：2020-06-16
申请号：US15771623
申请日：2016-11-23
申请人： Wacker Chemie AG
发明人： Frank Sandmeyer , Amanda Andrews , James Greene
IPC分类号： C09D151/08 , C08F2/22 , C08F283/12 , C08F290/06 , B32B21/08 , C08F20/18 , C08F116/04 , C08F212/08 , C08F236/06
摘要： Aqueous dispersions of copolymers of ethylenically unsaturated monomers and silicone resins bearing functional groups which are free radically polymerizable are prepared by forming an aqueous miniemulsion of the silicone resin dissolved in an ethylenically unsaturated monomer, the miniemulsion having a D50 droplet size

10. 发明授权

US09988496B2 Method for producing organopolysiloxanes 有权
公开(公告)号：US09988496B2
公开(公告)日：2018-06-05
申请号：US15535453
申请日：2016-07-21
申请人： Wacker Chemie AG
发明人： Frank Sandmeyer , Georg Loessel , Marko Prasse
IPC分类号： C08G77/06 , C08G77/18
CPC分类号： C08G77/06 , C08G77/18
摘要： Highly condensed silicon resins are obtained by a three step continuous procedure without the use of organic solvent, by preliminarily forming a partial alkoxylate by reacting a chlorosilane with alcohol containing no or a minimal amount of water, feeding the partial alkoxylate to a reaction column to form a silicone resin of low degree of condensation, and further condensing the silicone resin intermediate thus formed to produce a silicone resin product.

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