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1. 发明授权

US07732537B2 Methods addressing aging in flocculated molecular sieve catalysts for hydrocarbon conversion processes 有权
标题翻译：解决用于烃转化过程的絮凝分子筛催化剂中的老化的方法
公开(公告)号：US07732537B2
公开(公告)日：2010-06-08
申请号：US12021918
申请日：2008-01-29
申请人： Yun-feng Chang , Luc R. M. Martens , Machteld Maria Mertens , Stephen N. Vaughn
发明人： Yun-feng Chang , Luc R. M. Martens , Machteld Maria Mertens , Stephen N. Vaughn
IPC分类号： C08F2/00 , B01J29/06 , C08F10/00
CPC分类号： C08F10/00 , B01J29/06 , B01J29/7015 , B01J29/84 , B01J29/85 , B01J37/0045 , B01J2229/40 , B01J2229/42 , C07C1/20 , C07C2529/85 , Y02P20/52 , Y02P30/42 , C07C11/06 , C07C11/04 , C08F4/16 , C08F4/12
摘要： One aspect of the invention relates to a method for formulating a molecular sieve catalyst composition, the method comprising the steps of: (a) providing a synthesized molecular sieve having been recovered in the presence of a flocculant; (b) thermally treating the synthesized molecular sieve at a temperature from about 50° C. to about 250° C. and under other conditions sufficient to form a thermally treated synthesized molecular sieve having a first LOI less than 26% and a first micropore surface area; (c) aging the thermally treated synthesized molecular sieve for at least one year; (d) analyzing the aged, thermally treated molecular sieve to determine a second micropore surface area, wherein the second micropore surface area is 3% or less lower than the first micropore surface area; and (e) combining the aged, thermally treated synthesized molecular sieve, a binder, and optionally a matrix material to produce an aged, formulated molecular sieve catalyst composition.
摘要翻译：本发明的一个方面涉及一种配制分子筛催化剂组合物的方法，该方法包括以下步骤：（a）提供在絮凝剂存在下回收的合成分子筛; （b）在约50℃至约250℃的温度和在足以形成具有第一LOI小于26％的热处理合成分子筛的其它条件下热处理合成的分子筛和第一微孔表面区; （c）将经热处理的合成分子筛老化至少一年; （d）分析老化的热处理分子筛以确定第二微孔表面积，其中第二微孔表面积比第一微孔表面积低3％或更低; 和（e）将老化的热处理合成分子筛，粘合剂和任选的基质材料组合以制备老化的配制分子筛催化剂组合物。

2. 发明申请

US20090192276A1 Methods Addressing Aging In Flocculated Molecular Sieve Catalysts For Hydrocarbon Conversion Processes 有权
标题翻译：用于烃转化过程的絮凝分子筛催化剂中的老化方法
公开(公告)号：US20090192276A1
公开(公告)日：2009-07-30
申请号：US12021918
申请日：2008-01-29
申请人： Yun-Feng Chang , Luc R.M. Martens , Machteld Maria Mertens , Stephen N. Vaughn
发明人： Yun-Feng Chang , Luc R.M. Martens , Machteld Maria Mertens , Stephen N. Vaughn
IPC分类号： C08F4/16 , C08F4/12 , C07C5/333 , B01J27/182
CPC分类号： C08F10/00 , B01J29/06 , B01J29/7015 , B01J29/84 , B01J29/85 , B01J37/0045 , B01J2229/40 , B01J2229/42 , C07C1/20 , C07C2529/85 , Y02P20/52 , Y02P30/42 , C07C11/06 , C07C11/04 , C08F4/16 , C08F4/12
摘要： One aspect of the invention relates to a method for formulating a molecular sieve catalyst composition, the method comprising the steps of: (a) providing a synthesized molecular sieve having been recovered in the presence of a flocculant; (b) thermally treating the synthesized molecular sieve at a temperature from about 50° C. to about 250° C. and under other conditions sufficient to form a thermally treated synthesized molecular sieve having a first LOI less than 26% and a first micropore surface area; (c) aging the thermally treated synthesized molecular sieve for at least one year; (d) analyzing the aged, thermally treated molecular sieve to determine a second micropore surface area, wherein the second micropore surface area is 3% or less lower than the first micropore surface area; and (e) combining the aged, thermally treated synthesized molecular sieve, a binder, and optionally a matrix material to produce an aged, formulated molecular sieve catalyst composition.
摘要翻译：本发明的一个方面涉及一种配制分子筛催化剂组合物的方法，该方法包括以下步骤：（a）提供在絮凝剂存在下回收的合成分子筛; （b）在约50℃至约250℃的温度和在足以形成具有第一LOI小于26％的热处理合成分子筛的其它条件下热处理合成的分子筛和第一微孔表面区; （c）将经热处理的合成分子筛老化至少一年; （d）分析老化的热处理分子筛以确定第二微孔表面积，其中第二微孔表面积比第一微孔表面积低3％或更低; 和（e）将老化的热处理合成分子筛，粘合剂和任选的基质材料组合以制备老化的配制分子筛催化剂组合物。

3. 发明授权

US07947621B2 Method of making and process for using molecular sieve catalyst 有权
标题翻译：分子筛催化剂的制备及加工方法
公开(公告)号：US07947621B2
公开(公告)日：2011-05-24
申请号：US11653132
申请日：2007-01-12
申请人： Yun-feng Chang , Machteld Maria Mertens , Stephen N. Vaughn
发明人： Yun-feng Chang , Machteld Maria Mertens , Stephen N. Vaughn
IPC分类号： B01J29/06 , B01J27/182
CPC分类号： B01J35/002 , B01J29/005 , B01J29/83 , B01J29/85 , B01J35/0026 , B01J35/1009 , B01J35/1038 , B01J35/1042 , B01J37/0045 , B01J2229/42 , C07C1/20 , C07C2521/04 , C07C2521/08 , C07C2529/83 , C08F4/65916 , C10G3/48 , C10G3/49 , C10G3/62 , C10G2300/4018 , C10G2300/802 , C10G2400/02 , C10G2400/04 , C10G2400/10 , C10G2400/20 , Y02P20/52 , Y02P30/20 , Y02P30/42 , C07C11/04 , C07C11/06
摘要： This invention provides a process for manufacturing a catalyst with a desired attrition index, comprising the steps of selecting at least one molecular sieve having a morphology and size index (MSI) of from 1 to about 1000 to secure said desired attrition index of said catalyst.
摘要翻译：本发明提供了一种制备具有所需磨耗指数的催化剂的方法，包括以下步骤：选择至少一种形态和尺寸指数（MSI）为1至约1000的分子筛，以确保所述催化剂的所需要的磨损指数。

4. 发明申请

US20070203385A1 Method of making and process for using molecular sieve catalyst 有权
标题翻译：分子筛催化剂的制备及加工方法
公开(公告)号：US20070203385A1
公开(公告)日：2007-08-30
申请号：US11653132
申请日：2007-01-12
申请人： Yun-feng Chang , Machteld Maria Mertens , Stephen N. Vaughn
发明人： Yun-feng Chang , Machteld Maria Mertens , Stephen N. Vaughn
IPC分类号： C07C1/00
CPC分类号： B01J35/002 , B01J29/005 , B01J29/83 , B01J29/85 , B01J35/0026 , B01J35/1009 , B01J35/1038 , B01J35/1042 , B01J37/0045 , B01J2229/42 , C07C1/20 , C07C2521/04 , C07C2521/08 , C07C2529/83 , C08F4/65916 , C10G3/48 , C10G3/49 , C10G3/62 , C10G2300/4018 , C10G2300/802 , C10G2400/02 , C10G2400/04 , C10G2400/10 , C10G2400/20 , Y02P20/52 , Y02P30/20 , Y02P30/42 , C07C11/04 , C07C11/06
摘要： This invention provides a process for manufacturing a catalyst with a desired attrition index, comprising the steps of selecting at least one molecular sieve having a morphology and size index (MSI) of from 1 to about 1000 to secure said desired attrition index of said catalyst.
摘要翻译：本发明提供了一种制备具有所需磨耗指数的催化剂的方法，包括以下步骤：选择至少一种形态和尺寸指数（MSI）为1至约1000的分子筛，以确保所述催化剂的所需要的磨损指数。

5. 发明申请

US20090239737A1 Method Of Synthesizing Aluminophosphate And Silicoaluminophosphate Molecular Sieves 有权
标题翻译：合成磷酸铝和硅铝磷酸盐分子筛的方法
公开(公告)号：US20090239737A1
公开(公告)日：2009-09-24
申请号：US12424366
申请日：2009-04-15
申请人： Machteld Maria Mertens , Thomas H. Colle
发明人： Machteld Maria Mertens , Thomas H. Colle
IPC分类号： B01J29/85 , B01J29/83
CPC分类号： C01B39/54 , B01J29/83 , B01J29/85 , C07C1/20 , C07C2529/85 , Y02P20/52 , Y02P30/42 , C07C11/04 , C07C11/02 , C07C11/06
摘要： In a method of synthesizing an aluminophosphate or silicoaluminophosphate molecular sieve, a synthesis mixture is prepared by mixing a plurality of starting materials including at least a source of water, a source of phosphorus, a source of aluminum, optionally, a source of silicon and, and at least one organic directing agent for directing the formation of said molecular sieve. The starting materials are maintained at a temperature between 25° C. and 50° C., preferably between 30° C. and 45° C., during the mixing and until preparation of the starting mixture is complete, whereafter the synthesis mixture is heated to a crystallization temperature between about 100° C. and about 350° C. until crystals of the molecular sieve are produced. When crystallization is complete, the molecular sieve is recovered.
摘要翻译：在合成磷酸铝或硅铝磷酸盐分子筛的方法中，通过混合多种起始材料来制备合成混合物，所述起始材料至少包括水源，磷源，铝源，任选的硅源，和用于引导所述分子筛形成的至少一种有机导向剂。起始原料在混合期间保持在25℃至50℃之间，优选在30℃至45℃之间，直到起始混合物的制备完成，然后将合成混合物加热至约100℃至约350℃的结晶温度，直至产生分子筛的晶体。当结晶完成时，回收分子筛。

6. 发明授权

US07014827B2 Synthesis of silicoaluminophosphates 失效
公开(公告)号：US07014827B2
公开(公告)日：2006-03-21
申请号：US10002241
申请日：2001-10-23
申请人： Machteld Maria Mertens , Brita Engels
发明人： Machteld Maria Mertens , Brita Engels
IPC分类号： C01B25/36 , B01J27/00 , C07C1/02
CPC分类号： C07C1/20 , B01J29/85 , C01B37/04 , C01B37/06 , C01B37/08 , C10G3/49 , C10G2300/703 , C10G2400/20 , Y02P30/20
摘要： Disclosed is a method for the manufacture of silicoaluminophosphate (SAPO) and/or aluminophosphate (ALPO) molecular sieves. The method includes maintaining the slurry of the as crystallized molecular sieve under substantially static conditions when stored after substantially complete crystallization and prior to recovery of the product.

7. 发明授权

US06858129B2 Tailored zeolite bound zeolite catalysts and its use for hydrocarbon conversion 失效
标题翻译：定性沸石结合沸石催化剂及其用于烃转化
公开(公告)号：US06858129B2
公开(公告)日：2005-02-22
申请号：US10635400
申请日：2003-08-06
申请人： Gary David Mohr , Kenneth Ray Clem , Wilfried Jozef Mortier , Machteld Maria Mertens , Xiaobing Feng , Marc H. Anthonis , Bart Schoofs
发明人： Gary David Mohr , Kenneth Ray Clem , Wilfried Jozef Mortier , Machteld Maria Mertens , Xiaobing Feng , Marc H. Anthonis , Bart Schoofs
IPC分类号： B01J29/40 , B01J29/70 , B01J29/80 , B01J29/87 , B01J29/89 , B01J37/00 , C10G11/05 , C10G29/20 , C10G45/64 , C07C5/22
CPC分类号： B01J29/7042 , B01J29/06 , B01J29/40 , B01J29/80 , B01J29/87 , B01J29/89 , B01J37/0009 , B01J2229/42 , B01J2229/62 , C10G11/05 , C10G29/205 , C10G45/64
摘要： There is provided a zeolite bound zeolite catalyst which does not contain significant amount of non-zeolitic binder and can be tailored to optimize its performance and a process for converting hydrocarbons utilizing the zeolite bound zeolite catalyst. The zeolite bound zeolite catalyst comprises core crystals containing first crystals of a first zeolite and optionally second crystals of a second zeolite having a composition, structure type, or both that is different from said first zeolite and binder crystals containing third crystals of a third zeolite and optionally fourth crystals of a fourth zeolite having a composition, structure type, or both that is different from said third zeolite. If the core crystals do not contain the second crystals of the second zeolite, then the binder crystals must contain the fourth crystals of the fourth zeolite. The zeolite bound zeolite finds application in hydrocarbon conversion processes, e.g., catalytic cracking, alkylation, disproportional of toluene, isomerization, and transalkylation reactions.
摘要翻译：提供沸石结合的沸石催化剂，其不含有显着量的非沸石粘合剂，并且可以调整其优化其性能，以及使用沸石结合的沸石催化剂转化烃的方法。沸石结合的沸石催化剂包括含有第一沸石的第一晶体的芯晶体和任选具有与所述第一沸石不同的组成，结构类型或两者的第二沸石的第二晶体，以及包含第三沸石的第三晶体的粘结剂晶体，任选具有与所述第三沸石不同的组成，结构类型或二者的第四沸石的第四晶体。如果核心晶体不含第二沸石的第二晶体，则粘合剂晶体必须含有第四沸石的第四晶体。沸石结合的沸石可用于烃转化过程，例如催化裂化，烷基化，甲苯不成比例，异构化和烷基转移反应。

8. 发明授权

US07459136B2 Process for manufacture of silicoaluminophosphate molecular sieves 有权
标题翻译：硅铝磷酸盐分子筛的制备方法
公开(公告)号：US07459136B2
公开(公告)日：2008-12-02
申请号：US11221192
申请日：2005-09-07
申请人： Machteld Maria Mertens
发明人： Machteld Maria Mertens
IPC分类号： C01B39/54 , B01J27/182 , C07C1/20
CPC分类号： B01J29/85 , C01B37/08 , C01B39/54 , C07C1/20 , C07C2529/85 , Y10S423/30 , C07C11/02
摘要： A process for manufacturing a silicoaluminophosphate molecular sieve, the process comprising the steps of: (a) dissolving a silicon source into in a template at conditions sufficient to form a solution having a silicon concentration of at least 0.05 wt. %; (b) adding at least one aluminium source and at least one phosphorus source to at least a portion of the solution of step (a) to form a synthesis mixture, wherein at least the major portion of the aluminum source and phosphorus source are added to the solution after the solution has reached a dissolved silicon concentration of at least 0.03 wt. %; and (c) treating the synthesis mixture for a period of time with mixing and at a temperature sufficient to form the silicoaluminophosphate molecular sieve, wherein the silicoaluminophosphate molecular sieve comprises at least one intergrown phase of molecular sieves having AEI and CHA framework types, wherein the intergrown phase has an AEI/CHA mass ratio of from about 5/95 to 40/60 as determined by DIFFaX analysis.
摘要翻译：一种制备硅铝磷酸盐分子筛的方法，该方法包括以下步骤：（a）在足以形成硅浓度至少为0.05重量％的溶液的条件下将硅源溶解在模板中。％; （b）向步骤（a）的溶液的至少一部分添加至少一种铝源和至少一种磷源以形成合成混合物，其中至少将铝源和磷源的主要部分加入溶液达到溶解硅浓度至少为0.03wt。％; 和（c）通过混合并在足以形成硅铝磷酸盐分子筛的温度下处理合成混合物一段时间，其中硅铝磷酸盐分子筛包含具有AEI和CHA骨架类型的至少一个共生相分子筛，其中共生相具有通过DIFFaX分析测定的约5/95至40/60的AEI / CHA质量比。

9. 发明授权

US07335295B2 Coated zeolite catalysts and use for hydrocarbon conversion 有权
标题翻译：涂层沸石催化剂和用于烃转化
公开(公告)号：US07335295B2
公开(公告)日：2008-02-26
申请号：US10862849
申请日：2004-06-07
申请人： Jannetje Maatje van den Berge , Gary David Mohr , Kenneth Ray Clem , Wilfried Jozef Mortier , Machteld Maria Mertens , Michael C. Bradford
发明人： Jannetje Maatje van den Berge , Gary David Mohr , Kenneth Ray Clem , Wilfried Jozef Mortier , Machteld Maria Mertens , Michael C. Bradford
IPC分类号： C10G35/04
CPC分类号： B01J35/023 , B01J29/40 , B01J29/70 , B01J29/80 , B01J37/0246 , B01J2229/12 , B01J2229/26 , B01J2229/42 , B01J2229/62 , C07C2/864 , C07C5/2708 , C07C6/123 , C07C2529/40 , C07C2529/70 , C07C2529/87 , C10G3/45 , C10G3/47 , C10G3/49 , C10G11/05 , C10G35/065 , C10G35/095 , C10G45/64 , C10G2300/1044 , C10G2300/4018 , C10G2300/708 , C10G2400/20 , Y02P20/52 , Y02P30/20 , C07C15/08
摘要： There is provided a coated zeolite catalyst in which the accessibility of the acid sites on the external surfaces of the zeolite is controlled and a process for converting hydrocarbons utilizing the coated zeolite catalyst. The zeolite catalyst comprises core crystals of a first zeolite and a discontinuous layer of smaller size second crystals of a second zeolite which cover at least a portion of the external surface of the first crystals The coated zeolite catalyst finds particular application in hydrocarbon conversion processes where catalyst activity in combination with zeolite structure are important for reaction selectivity, e.g., catalytic cracking, alkylation, disproportional of toluene, isomerization, and transalkylation reactions.
摘要翻译：提供了一种涂层沸石催化剂，其中控制沸石外表面上的酸性位点的可及性以及利用涂覆的沸石催化剂转化烃的方法。沸石催化剂包括第一沸石的核心晶体和覆盖第一晶体的至少部分外表面的第二沸石的较小尺寸的第二晶体的不连续层。涂覆的沸石催化剂在烃转化过程中特别适用于其中催化剂结合沸石结构的活性对于反应选择性是重要的，例如催化裂化，烷基化，甲苯不成比例，异构化和烷基转移反应。

10. 发明授权

US06300535B1 Preparation of zeolite bound by MFI structure type zeolite and use thereof 有权
标题翻译：通过MFI结构型沸石结合的沸石的制备及其用途
公开(公告)号：US06300535B1
公开(公告)日：2001-10-09
申请号：US09593122
申请日：2000-06-13
申请人： Jannetje Maatje van den Berge , Machteld Maria Mertens , Wilfried Jozef Mortier
发明人： Jannetje Maatje van den Berge , Machteld Maria Mertens , Wilfried Jozef Mortier
IPC分类号： C07C522
CPC分类号： C07C6/126 , B01J29/40 , B01J29/70 , B01J29/80 , B01J37/0009 , B01J2229/26 , B01J2229/42 , B01J2229/62 , B01J2229/64 , C01B39/40 , C07C1/20 , C07C2/66 , C07C4/06 , C07C5/2708 , C07C6/123 , C07C2529/70 , C07C15/00
摘要： The preparation of zeolite bound zeolite comprising zeolite core crystals other than MFI structure zeolite which are bound by MFI structure type zeolite and the use of the zeolite bound by MFI structure type zeolite prepared by the process as an adsorbent or as a catalyst for hydrocarbon conversion. The zeolite bound zeolite is produced by including seed crystals of MFI structure type zeolite into the silica bound aggregate forming mixture and then converting the silica binder of the aggregate to the MFI binder crystals. The resulting zeolite bound zeolite has good strength and integrity.
摘要翻译：包含由MFI结构型沸石结合的除MFI结构沸石以外的沸石核心晶体的沸石结合沸石的制备以及通过该方法制备的MFI结构型沸石结合的沸石作为吸附剂或用作烃转化的催化剂的用途。沸石结合的沸石通过将MFI结构型沸石的晶种包括在二氧化硅结合的聚集体形成混合物中，然后将聚集体的二氧化硅粘合剂转化为MFI粘结剂晶体来制备。所得沸石结合的沸石具有良好的强度和完整性。

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