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1. 发明授权

US09624450B2 High-performance hydrolysis fuel formulation for micro fuel cells 有权
公开(公告)号：US09624450B2
公开(公告)日：2017-04-18
申请号：US14202613
申请日：2014-03-10
申请人： Honeywell International Inc.
发明人： Steven J. Eickhoff , Stephen Kenyon Swanson
IPC分类号： C01B6/06 , C01B3/06 , C01B3/08 , C10L5/44
CPC分类号： C10L5/44 , C01B3/065 , C01B6/06 , Y02E50/10 , Y02E50/30 , Y02E60/362
摘要： Embodiments of the present invention relate to a hydrogen generating fuel comprising grains comprising a promoter and AlH3, each grain having a size between 1 and 10 μm. In some embodiments, the grains can be pressed into a porous pellet.

2. 发明申请

US20170050846A1 MECHANOCHEMICAL SYNTHESIS OF ALANE 审中-公开
标题翻译： ALANE的机械合成
公开(公告)号：US20170050846A1
公开(公告)日：2017-02-23
申请号：US15118788
申请日：2015-02-12
申请人： Iowa State University Research Foundation, Inc.
发明人： Shalabh Gupta , Vitalij K. Pecharsky , Takeshi Kobayashi , Marek Pruski , Ihor Hlova
IPC分类号： C01B6/06 , C01B3/00
CPC分类号： C01B6/06 , C01B3/0026
摘要： In some examples, a method of forming alane (AlH3), the method comprising reacting one of: 1) a MAlH4, wherein M is an alkali metal; 2) alkali-metal hydride, MH; or 3) alkali-metal with one or more aluminum halides (AlX3, where X is a halogen), via a mechanochemical process, to form the alane, wherein the reaction is substantially solvent free and carried out in an environment with a temperature between approximately 250 K and approximately 330 K.
摘要翻译：在一些实例中，形成丙烷（AlH 3）的方法，所述方法包括使以下物质之一：1）MAH 4，其中M是碱金属; 2）碱金属氢化物，MH; 或3）碱金属与一种或多种卤化铝（AlX 3，其中X为卤素）通过机械化学方法形成丙烯，其中反应基本上无溶剂，并且在温度在约 250 K和约330 K.

3. 发明授权

US09550672B2 Method for preparation of an alane-etherate complex and alane 有权
标题翻译：丙烷 - 乙醚络合物和丙烷的制备方法
公开(公告)号：US09550672B2
公开(公告)日：2017-01-24
申请号：US14558240
申请日：2014-12-02
申请人： Intelligent Energy Inc.
发明人： Allison M. Fisher
IPC分类号： C01B6/06
CPC分类号： C01B6/06
摘要： The invention relates to methods of forming an alane-etherate complex and α-alane from the alane-etherate complex. The methods include reacting an alkyl halide with a metal alanate in a solvent including an ether. A tertiary amine may also be added to the reaction. The alane is collected after removal of the solvent and/or the tertiary amine. An electrospraying process can be used to remove the solvent.
摘要翻译：本发明涉及从丙烷 - 乙醚合物络合物形成丙烷 - 乙醚合物络合物和α-甲烷的方法。所述方法包括使烷基卤与金属铝酸盐在包括醚的溶剂中反应。也可以向反应中加入叔胺。在除去溶剂和/或叔胺之后收集丙烷。可以使用电喷雾方法除去溶剂。

4. 发明申请

US20160368768A1 Crystallization and Stabilization in the Synthesis of Microcrystalline Alpha Alane 审中-公开
标题翻译：微晶α-烯烃的合成中的结晶和稳定性
公开(公告)号：US20160368768A1
公开(公告)日：2016-12-22
申请号：US15184962
申请日：2016-06-16
申请人： Ardica Technologies, Inc.
发明人： David Stout , Henry Fong , Elisabeth Mclaughlin , Paul E. Penwell , Mark A. Petrie
IPC分类号： C01B6/06 , C01B3/00
CPC分类号： C01B6/06 , C01B3/0026 , C01D15/04 , Y02E60/327
摘要： Systems and methods for producing microcrystalline alpha alane are provided herein. An exemplary process comprises the elimination of the crystallization aid lithium borohydride through the use of excess lithium aluminum hydride or sodium borohydride. Further exemplary processes comprise methods for passivating microcrystalline alpha alane using a weak acid in a nonaqueous solvent solution.
摘要翻译：本文提供了用于生产微晶α阿拉曼的系统和方法。示例性方法包括通过使用过量的氢化铝锂或硼氢化钠消除结晶助剂锂硼氢化物。其它示例性方法包括使用非水溶剂溶液中的弱酸钝化微晶α阿拉伯的方法。

5. 发明申请

US20160115602A1 Use of Fluidized-Bed Electrode Reactors for Alane Production 审中-公开
标题翻译：使用流化床电极反应器进行烯烃生产
公开(公告)号：US20160115602A1
公开(公告)日：2016-04-28
申请号：US14986921
申请日：2016-01-04
申请人： Ardica Technologies, Inc.
发明人： Steven Crouch-Baker , Mark A. Petrie , David Stout , Francis Tanzella
IPC分类号： C25B9/16 , C01B6/06 , C25B13/00 , C25B1/00 , C25B11/02 , C25B11/04
CPC分类号： C25B9/162 , C01B6/06 , C25B1/00 , C25B11/02 , C25B11/0415 , C25B13/00 , C25B15/08
摘要： Fluidized-bed reactors for producing alane are provided herein. An exemplary process includes inducing an electrical potential difference in an electrolyte solution to produce an anolyte solution that includes an alane adduct, wherein an electrical potential difference is generated between anode aluminum particles and a cathode, the electrolyte solution including an alkali metal hydride dissolved in a solvent, the anode aluminum particles and cathode being separated by a diaphragm.
摘要翻译：本文提供了用于生产丙烷的流化床反应器。示例性方法包括在电解质溶液中诱导电位差以产生包含丙烯加合物的阳极电解液，所述阳极电解液在阳极铝颗粒和阴极之间产生电位差，所述电解质溶液包含溶于溶剂，阳极铝颗粒和阴极被隔膜隔开。

6. 发明申请

US20150093578A1 METHOD OF MANUFACTURING ALANE INCLUDING DESOLVATION OF AN ALANE -ETHERATE COMPLEX 审中-公开
标题翻译：制造ALANE-DEHERATE复合物的方法
公开(公告)号：US20150093578A1
公开(公告)日：2015-04-02
申请号：US14558155
申请日：2014-12-02
申请人： Intelligent Energy Inc.
发明人： Allison Fisher
IPC分类号： B01J2/06 , D01D5/00 , C01B6/06
CPC分类号： B01J2/06 , C01B6/06 , D01D5/0007 , Y10T428/2982
摘要： The invention relates to methods of preparing α-alane by desolvating an alane-etherate complex. The methods include electrospraying or electrospinning the alane-etherate complex in order to remove solvent. Solid alane is obtained and can be in either fine particulate form or fiber form. The alane can be encapsulated with a stabilizing agent.
摘要翻译：本发明涉及通过脱乙醚 - 乙醚合物络合物制备α-烷烃的方法。所述方法包括电解喷雾或静电纺丝，以除去溶剂。获得固体异氰酸酯，可以是细颗粒形式或纤维形式。丙烯可以用稳定剂包封。

7. 发明申请

US20130026453A1 Methods of Polymerizing Silanes and Cyclosilanes Using N-Heterocyclic Carbenes, Metal Complexes Having N-Heterocyclic Carbene Ligands, and Lanthanide Compounds 有权
标题翻译：使用N-杂环碳烯，具有N-杂环碳烯配体的金属络合物和镧系化合物聚合硅烷和环硅烷的方法
公开(公告)号：US20130026453A1
公开(公告)日：2013-01-31
申请号：US13194472
申请日：2011-07-29
申请人： Klaus KUNZE , Gregory Nyce , Wenzhuo Guo
发明人： Klaus KUNZE , Gregory Nyce , Wenzhuo Guo
IPC分类号： H01L51/40 , H01L51/30 , H01B1/06 , C01B33/04 , C01B6/06
CPC分类号： C01B6/06 , C01B33/04 , H01B3/18 , H01L51/0094 , Y02E10/549 , Y02P70/521
摘要： Compositions and methods for controlled polymerization and/or oligomerization of silane (and optionally cyclosilane) compounds, including those of the general formulae SinH2n and SinH2n+2, as well as halosilanes and arylsilanes, to produce soluble polysilanes, polygermanes and/or polysilagermanes having low levels of carbon and metal contaminants, high molecular weights, low volatility, high purity, high solubility and/or high viscosity. The polysilanes, polygermanes and/or polysilagermanes are useful as a precursor to silicon- and/or germanium-containing conductor, semiconductor and dielectric films.
摘要翻译：包括通式SinH2n和SinH2n + 2的硅烷（和任选的环硅烷）化合物的受控聚合和/或低聚的组合物和方法，以及卤代硅烷和芳基硅烷，以产生具有低的可溶性聚硅烷，多晶硅和/或聚硅烷碳和金属污染物的水平，高分子量，低挥发性，高纯度，高溶解度和/或高粘度。聚硅烷，多晶硅和/或聚硅烷可用作含硅和/或锗的导体，半导体和介电膜的前体。

8. 发明申请

US20120217618A1 Silicon-Germanium Hydrides and Methods for Making and Using Same 失效
标题翻译：硅锗氢化物及其制备和使用方法
公开(公告)号：US20120217618A1
公开(公告)日：2012-08-30
申请号：US13407195
申请日：2012-02-28
申请人： John Kouvetakis , Cole J. Ritter, III
发明人： John Kouvetakis , Cole J. Ritter, III
IPC分类号： H01L29/24 , C30B25/02 , C23C16/28 , H01L21/20 , C01B33/00 , H01B1/06
CPC分类号： C01B6/06 , C23C16/22 , C30B25/02 , C30B29/52 , H01L21/0237 , H01L21/02381 , H01L21/02532 , H01L21/0262 , Y10T428/261 , Y10T428/265 , Y10T428/31663
摘要： The present invention provides novel silicon-germanium hydride compounds, methods for their synthesis, methods for their deposition, and semiconductor structures made using the novel compounds.
摘要翻译：本发明提供新的硅锗化合物，它们的合成方法，它们的沉积方法，以及使用这些新化合物制备的半导体结构。

9. 发明申请

US20090010836A1 HYDROGEN STORAGE MATERIALS, METAL HYDRIDES AND COMPLEX HYDRIDES PREPARED USING LOW-BOILING-POINT SOLVENTS 审中-公开
标题翻译：使用低沸点溶剂制备的氢储存材料，金属水合物和复合水合物
公开(公告)号：US20090010836A1
公开(公告)日：2009-01-08
申请号：US12143348
申请日：2008-06-20
申请人： Gerard Sean McGrady , Craig M. Jensen
发明人： Gerard Sean McGrady , Craig M. Jensen
IPC分类号： C01B6/04 , C01B6/24
CPC分类号： C01B6/243 , B01J20/0248 , B01J20/04 , C01B3/0026 , C01B3/0031 , C01B6/06 , C01B6/24 , Y02E60/327
摘要： The invention provides systems and methods for preparing hydrogen storage materials using low boiling point solvents or reaction media. Examples of such solvents or reaction media include dimethyl ether, ethyl methyl ether, epoxyethane, and trimethylamine. The synthesis of the hydrogen storage materials is conducted is a selected medium, and after synthesis is complete, the reaction medium is removed as necessary by moderate heating.
摘要翻译：本发明提供使用低沸点溶剂或反应介质制备储氢材料的系统和方法。这种溶剂或反应介质的实例包括二甲醚，乙基甲基醚，环氧乙烷和三甲胺。进行储氢材料的合成是选择的介质，合成完成后，根据需要通过适度加热除去反应介质。

10. 发明申请

US20080299037A1 Method for Purifying Germanium Hydrides 有权
标题翻译：纯化氢化锗的方法
公开(公告)号：US20080299037A1
公开(公告)日：2008-12-04
申请号：US11756114
申请日：2007-05-31
申请人： Mathias Tezock
发明人： Mathias Tezock
IPC分类号： C01B39/00 , C01G17/00
CPC分类号： C01B3/52 , C01B6/06 , C01B2203/0415 , C01B2203/0475 , C01B2203/0495 , Y10S55/15
摘要： An improved method for purifying gaseous mixtures of germanium hydrides and hydrogen is disclosed. In one aspect, the crude gas is contacted with a cold caustic solution to reduce levels of carbon dioxide and water. The partially purified gas is chilled in direct-contact with a hydrogen refrigerant to induce homogenous condensation of water impurity. Liquid and ice particles formed by lower temperatures are removed across an aerosol phase separating medium to produce a cooled and partially purified gas mixture which is further dried and de-carbonated across a zeolitic molecular sieve adsorbent to achieve very low concentrations of moisture and carbon dioxide in the bulk gas. In one aspect, the purified gas mixture obtained is partially liquefied, phase-separated and distilled to obtain germanium hydride, digermanium hexahydride and hydrogen gas as products. A portion of the hydrogen product can be compressed, chilled and re-used as a direct-contact refrigerant in the purification process.
摘要翻译：公开了一种用于纯化氢化锗和氢气的气态混合物的改进方法。在一个方面，粗气体与冷苛性溶液接触以降低二氧化碳和水的含量。部分纯化的气体与氢制冷剂直接接触而冷却，以引起水杂质的均匀冷凝。通过气溶胶相分离介质去除由较低温度形成的液体和冰颗粒，以产生冷却和部分纯化的气体混合物，该气体混合物进一步在沸石分子筛吸附剂上干燥和脱碳，以实现非常低浓度的水分和二氧化碳大量气体。一方面，将获得的纯化气体混合物部分液化，分相分离并蒸馏，得到氢化锗，六氢六氢呋喃和氢气作为产物。在纯化过程中，氢产物的一部分可以被压缩，冷却并重新用作直接接触制冷剂。

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