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1. 发明授权

US09273020B2 Process for the production of chemical compounds from carbon dioxide 有权
标题翻译：从二氧化碳生产化学化合物的方法
公开(公告)号：US09273020B2
公开(公告)日：2016-03-01
申请号：US14394508
申请日：2013-04-11
申请人： Haldor Topsøe A/S
发明人： Niels Christian Schjødt , John Bøgild Hansen , Claus Friis Pedersen
IPC分类号： C07D305/00 , C07C69/96 , C07C51/14 , C07D305/12 , C07C67/38 , C07C68/00 , C07C201/02 , C07D301/04 , C25B1/02 , C25B15/08 , C25B1/00 , C07C67/035 , C07C68/04
CPC分类号： C07D305/12 , C07C51/14 , C07C67/035 , C07C67/38 , C07C68/005 , C07C68/04 , C07C201/02 , C07D301/04 , C25B1/00 , C25B1/02 , C25B15/08 , Y02E60/366 , Y02P20/133 , Y02P20/134 , Y02P20/582 , C07C203/04 , C07C69/96 , C07C53/124 , C07C69/24
摘要： Process for the production of a chemical compound from a carbon dioxide starting material, comprising the steps of a) providing a feed stream consisting mainly of carbon dioxide; b) electrolyzing in an electrolysis stage the carbon dioxide in the feed stream to a first gas stream containing carbon monoxide and a second gas stream containing oxygen, wherein the molar ratio between carbon monoxide and oxygen is about 1:0.5 in an electrolysis stage; c) adjusting the composition of the first gas stream or the second gas stream or both gas streams to include carbon dioxide, either by operating at less than full conversion of CO2 or by sweeping one or both gas streams with a gas containing CO2 or by at some stage between the electrolysis cell and the oxidative carbonylation reactor diluting one or both gas streams with a gas containing CO2; all while maintaining an overall molar ratio of carbon monoxide to oxygen of about 1:0.5; and d) introducing the first and second process stream into a reaction stage and reacting the first and second process stream combined or in succession with a substrate to the chemical compound by means of an oxidative carbonylation reaction with the carbon monoxide and oxygen contained in the process feed stream.
摘要翻译：用于从二氧化碳原料生产化合物的方法，包括以下步骤：a）提供主要由二氧化碳组成的进料流; b）在电解阶段中将进料流中的二氧化碳电解成含有一氧化碳和含有氧的第二气流的第一气流，其中在电解阶段一氧化碳和氧之间的摩尔比为约1:0.5; c）调节第一气流或第二气流或两种气流的组成以包括二氧化碳，或者通过以少于二氧化碳的全部转化率进行操作，或者通过用含有CO 2的气体或通过在在电解池和氧化羰基化反应器之间的某个阶段，用含CO 2的气体稀释一种或两种气流; 同时保持一氧化碳与氧的总摩尔比为约1:0.5; 和d）将第一和第二工艺流引入反应阶段，并通过与该方法中所含的一氧化碳和氧气进行氧化羰基化反应，将第一和第二工艺流与底物组合或连续地与化学化合物反应饲料流。

2. 发明授权

US08987446B2 Bimetallic complexes and the use thereof in producing diaryl carbonate 有权
标题翻译：双金属络合物及其在制备碳酸二芳酯中的用途
公开(公告)号：US08987446B2
公开(公告)日：2015-03-24
申请号：US13515710
申请日：2010-12-09
申请人： Christoph Gürtler , Thomas Ernst Müller , Pieter Ooms , Johann Rechner , Friedhelm Risse , Angelina Prokofieva , Franco Doro , Burkhard Köhler , Walter Leitner , Aurel Wolf
发明人： Christoph Gürtler , Thomas Ernst Müller , Pieter Ooms , Johann Rechner , Friedhelm Risse , Angelina Prokofieva , Franco Doro , Burkhard Köhler , Walter Leitner , Aurel Wolf
IPC分类号： C07D241/46 , C07F15/00 , C07C68/00
CPC分类号： C07F15/0066 , C07C68/005 , C07C69/96
摘要： The invention relates to bimetallic complexes in which the ligand contains a salophen unit which complexes copper, manganese or cobalt and a phenanthroline unit which complexes palladium and the two systems are linked by a continuous conjugated system. The invention further relates to the use of these bimetallic complexes as catalysts for the oxidative carbonylation of aromatic hydroxy compounds to form diaryl carbonates, a process for preparing diaryl carbonates using the bimetallic complex as catalyst and also diaryl carbonates prepared by oxidative carbonylation of aromatic hydroxy compounds using the bimetallic complexes of the invention as catalysts.
摘要翻译：本发明涉及双金属络合物，其中配体包含络合铜，锰或钴的盐酸单体和络合钯并且两种体系通过连续共轭体系连接的菲咯啉单元。本发明还涉及这些双金属络合物作为用于芳族羟基化合物的氧化羰基化以形成碳酸二芳基酯的催化剂的使用，使用双金属络合物作为催化剂制备碳酸二芳基酯的方法，以及通过芳族羟基化合物的氧化羰基化制备的碳酸二芳基酯使用本发明的双金属络合物作为催化剂。

3. 发明申请

US20150057458A1 PROCESS FOR THE PRODUCTION OF CHEMICAL COMPOUNDS FROM CARBON DIOXIDE 有权
标题翻译：从二氧化碳生产化学化合物的方法
公开(公告)号：US20150057458A1
公开(公告)日：2015-02-26
申请号：US14394508
申请日：2013-04-11
申请人： Haldor Topsøe A/S
发明人： Niels Christian Schjødt , John Bøgild Hansen , Claus Friis Pedersen
IPC分类号： C07D305/12 , C25B1/02 , C25B1/00 , C07C68/04 , C07C67/035
CPC分类号： C07D305/12 , C07C51/14 , C07C67/035 , C07C67/38 , C07C68/005 , C07C68/04 , C07C201/02 , C07D301/04 , C25B1/00 , C25B1/02 , C25B15/08 , Y02E60/366 , Y02P20/133 , Y02P20/134 , Y02P20/582 , C07C203/04 , C07C69/96 , C07C53/124 , C07C69/24
摘要： Process for the production of a chemical compound from a carbon dioxide starting material, comprising the steps of a) providing a feed stream consisting mainly of carbon dioxide; b) electrolysing in an electrolysis stage the carbon dioxide in the feed stream to a first gas stream containing carbon monoxide and a second gas stream containing oxygen, wherein the molar ratio between carbon monoxide and oxygen is about 1:0.5 in an electrolysis stage; c) adjusting the composition of the first gas stream or the second gas stream or both gas streams to include carbon dioxide, either by operating at less than full conversion of CO2 or by sweeping one or both gas streams with a gas containing CO2 or by at some stage between the electrolysis cell and the oxidative carbonylation reactor diluting one or both gas streams with a gas containing CO2; all while maintaining an overall molar ratio of carbon monoxide to oxygen of about 1:0.5; and d) introducing the first and second process stream into a reaction stage and reacting the first and second process stream combined or in succession with a substrate to the chemical compound by means of an oxidative carbonylation reaction with the carbon monoxide and oxygen contained in the process feed stream.
摘要翻译：用于从二氧化碳原料生产化合物的方法，包括以下步骤：a）提供主要由二氧化碳组成的进料流; b）在电解阶段将电解中的二氧化碳电解成含有一氧化碳和含有氧的第二气流的第一气流，其中一氧化碳与氧之间的摩尔比在电解阶段为约1:0.5; c）调节第一气流或第二气流或两种气流的组成以包括二氧化碳，或者通过以少于二氧化碳的全部转化率进行操作，或者通过用含有CO 2的气体或通过在在电解池和氧化羰基化反应器之间的某个阶段，用含CO 2的气体稀释一种或两种气流; 同时保持一氧化碳与氧的总摩尔比为约1:0.5; 和d）将第一和第二工艺流引入反应阶段，并通过与该方法中所含的一氧化碳和氧气进行氧化羰基化反应，将第一和第二工艺流与底物组合或连续地与化学化合物反应饲料流。

4. 发明授权

US08212088B2 Efficient and selective chemical recycling of carbon dioxide to methanol, dimethyl ether and derived products 有权
标题翻译：二氧化碳对甲醇，二甲醚和衍生产物的高效选择性化学回收
公开(公告)号：US08212088B2
公开(公告)日：2012-07-03
申请号：US12537647
申请日：2009-08-07
申请人： George A. Olah , G. K. Surya Prakash
发明人： George A. Olah , G. K. Surya Prakash
IPC分类号： C07C29/51 , C07C29/15 , C07C29/132
CPC分类号： C07C29/136 , C07C1/20 , C07C29/04 , C07C29/14 , C07C29/141 , C07C29/149 , C07C41/09 , C07C51/15 , C07C67/08 , C07C67/38 , C07C68/005 , C07C68/02 , C25B3/04 , C07C31/08 , C07C31/04 , C07C31/10 , C07C11/02 , C07C53/02 , C07C69/06 , C07C69/96 , C07C43/043
摘要： An efficient and environmentally beneficial method of recycling and producing methanol from varied sources of carbon dioxide including flue gases of fossil fuel burning powerplants, industrial exhaust gases or the atmosphere itself. Converting carbon dioxide by chemical or electrochemical reduction seconardy treatment to produce essentially methanol, dimethyl ether and derived products.
摘要翻译：一种从不同来源的二氧化碳回收和生产甲醇的有效和环保的方法，包括化石燃料燃烧发电厂，工业废气或大气本身的烟道气。通过化学或电化学还原仲胺处理来转化二氧化碳，主要生产甲醇，二甲醚和衍生产物。

5. 发明申请

US20110152558A1 PROCESS FOR PRODUCING DIARYL CARBONATES 有权
标题翻译：生产二氧化碳的方法
公开(公告)号：US20110152558A1
公开(公告)日：2011-06-23
申请号：US12813185
申请日：2010-06-10
申请人： Zhen Wei HUANG , Chih Wei CHANG , Chia Jung TSAI
发明人： Zhen Wei HUANG , Chih Wei CHANG , Chia Jung TSAI
IPC分类号： C07C68/00
CPC分类号： C07C68/005 , C07C69/96
摘要： The present invention relates to a process for producing diaryl carbonates, which is to synthesize diaryl carbonates by oxidative carbonylation of phenols with carbon monoxide and oxygen, and in particular, to synthesize diphenyl carbonate from phenol. The present invention is characterized in that a catalytic system comprising a metal halide catalyst and one or more cocatalysts of nitrogenous heterocyclic compounds is used to increase the convertibility, selectivity and yield of this catalytic reaction.
摘要翻译：本发明涉及一种碳酸二芳基酯的制备方法，该方法是通过苯酚与一氧化碳和氧的氧化羰基化合成碳酸二芳基酯，特别是合成苯酚碳酸二苯酯。本发明的特征在于，使用包含金属卤化物催化剂和一种或多种含氮杂环化合物的助催化剂的催化体系来提高该催化反应的可转换性，选择性和产率。

6. 发明授权

US07799940B2 Process for manufacturing dimethyl carbonate 有权
标题翻译：碳酸二甲酯的制造方法
公开(公告)号：US07799940B2
公开(公告)日：2010-09-21
申请号：US12032149
申请日：2008-02-15
申请人： Ignacio Vic Fernandez , Benoit Fillion , Vutukuru Murthy , Vinod Sankaran Nair , Mario Perez Collado
发明人： Ignacio Vic Fernandez , Benoit Fillion , Vutukuru Murthy , Vinod Sankaran Nair , Mario Perez Collado
IPC分类号： C07C69/96
CPC分类号： C07C68/005 , C07C69/96
摘要： The present invention provides methods of forming dialkyl carbonate wherein catalyst buildup in the reaction equipment, the separation equipment, and transfer lines there between is reduced and even eliminated. In one embodiment, the method includes introducing alkanol, carbon monoxide, oxygen, and a catalyst to a reactor having a gaseous head space and a liquid body space. The reactor is operated under conditions to form dialkyl carbonate and water. A product stream containing dialkyl carbonate, water, and residual reactants is removed from the head space of the reactor and introduced to a cyclone with a flushing stream. A liquid bottom stream is captured from the cyclone and introduced to the reactor. The gaseous top stream contains product dialkyl carbonate.
摘要翻译：本发明提供形成碳酸二烷基酯的方法，其中反应设备中的催化剂积聚，分离设备和其间的输送管线减少甚至消除。在一个实施方案中，该方法包括将链烷醇，一氧化碳，氧和催化剂引入到具有气体顶部空间和液体体空间的反应器中。反应器在形成碳酸二烷基酯和水的条件下操作。从反应器的顶部空间除去含有碳酸二烷基酯，水和残余反应物的产物流，并将其引入具有冲洗流的旋风分离器。从旋风分离器捕获液体底部流并将其引入反应器。气态顶部流含有碳酸二烷基酯。

7. 发明授权

US07622602B2 Method for preparing a dialkyl carbonate, and its use in the preparation of diaryl carbonates and polycarbonates 有权
标题翻译：制备碳酸二烷基酯的方法及其在制备碳酸二芳基酯和聚碳酸酯中的用途
公开(公告)号：US07622602B2
公开(公告)日：2009-11-24
申请号：US11248390
申请日：2005-10-12
申请人： Thodla Ramgopal , Mario Perez Collado , Vijaya Kumar Narasaiah , Ignacio Vic Fernandez
发明人： Thodla Ramgopal , Mario Perez Collado , Vijaya Kumar Narasaiah , Ignacio Vic Fernandez
IPC分类号： C07C69/96
CPC分类号： C08G64/30 , C07C68/005 , C07C68/06 , C07C69/96
摘要： A method of making a dialkyl carbonate comprises: reacting, in a reactor comprising tantalum, an alkanol, oxygen, and carbon monoxide, in the presence of a catalyst. The reaction occurs in a mixture comprising a liquid phase wherein the liquid phase comprises about 4 to about 12 weight percent water based on the total weight of the liquid phase.
摘要翻译：制备碳酸二烷基酯的方法包括：在包含钽的反应器中，在催化剂存在下，使烷醇，氧和一氧化碳反应。该反应发生在包含液相的混合物中，其中基于液相的总重量，液相包含约4至约12重量％的水。

8. 发明申请

US20080200713A1 Process for Manufacturing Dimethyl Carbonate 有权
标题翻译：制造碳酸二甲酯的方法
公开(公告)号：US20080200713A1
公开(公告)日：2008-08-21
申请号：US12032149
申请日：2008-02-15
申请人： Ignacio Vic Fernandez , Benoit Fillion , Vutukuru Murthy , Vinod Sankaran Nair , Mario Perez Collado
发明人： Ignacio Vic Fernandez , Benoit Fillion , Vutukuru Murthy , Vinod Sankaran Nair , Mario Perez Collado
IPC分类号： C07C69/96
CPC分类号： C07C68/005 , C07C69/96
摘要： The present invention provides methods of forming dialkyl carbonate wherein catalyst buildup in the reaction equipment, the separation equipment, and transfer lines there between is reduced and even eliminated. In one embodiment, the method includes introducing alkanol, carbon monoxide, oxygen, and a catalyst to a reactor having a gaseous head space and a liquid body space. The reactor is operated under conditions to form dialkyl carbonate and water. A product stream containing dialkyl carbonate, water, and residual reactants is removed from the head space of the reactor and introduced to a cyclone with a flushing stream. A liquid bottom stream is captured from the cyclone and introduced to the reactor. The gaseous top stream contains product dialkyl carbonate.
摘要翻译：本发明提供形成碳酸二烷基酯的方法，其中反应设备中的催化剂积聚，分离设备和其间的输送管线减少甚至消除。在一个实施方案中，该方法包括将链烷醇，一氧化碳，氧和催化剂引入到具有气体顶部空间和液体体空间的反应器中。反应器在形成碳酸二烷基酯和水的条件下操作。从反应器的顶部空间除去含有碳酸二烷基酯，水和残余反应物的产物流，并将其引入具有冲洗流的旋风分离器。从旋风分离器捕获液体底部流并将其引入反应器。气态顶部流含有碳酸二烷基酯。

9. 发明申请

US20070254969A1 EFFICIENT AND SELECTIVE CHEMICAL RECYCLING OF CARBON DIOXIDE TO METHANOL, DIMETHYL ETHER AND DERIVED PRODUCTS 有权
标题翻译：二氧化碳对甲醇，二甲醚和衍生产物的有效和选择性化学回收
公开(公告)号：US20070254969A1
公开(公告)日：2007-11-01
申请号：US11766408
申请日：2007-06-21
申请人： George Olah , G.K. Prakash
发明人： George Olah , G.K. Prakash
IPC分类号： C07C27/00
CPC分类号： C07C29/136 , C07C1/20 , C07C29/04 , C07C29/14 , C07C29/141 , C07C29/149 , C07C41/09 , C07C51/15 , C07C67/08 , C07C67/38 , C07C68/005 , C07C68/02 , C25B3/04 , C07C31/08 , C07C31/04 , C07C31/10 , C07C11/02 , C07C53/02 , C07C69/06 , C07C69/96 , C07C43/043
摘要： An efficient and environmentally beneficial method of recycling and producing methanol from varied sources of carbon dioxide including flue gases of fossil fuel burning powerplants, industrial exhaust gases or the atmosphere itself. Converting carbon dioxide by chemical or electrochemical reduction secondary treatment to produce essentially methanol, dimethyl ether and derived products.
摘要翻译：一种从不同来源的二氧化碳回收和生产甲醇的有效和环保的方法，包括化石燃料燃烧发电厂，工业废气或大气本身的烟道气。通过化学或电化学还原二次处理将二氧化碳转化为基本上产生甲醇，二甲醚和衍生产物。

10. 发明申请

US20070083059A1 Method for preparing a dialkyl carbonate, and its use in the preparation of diaryl carbonates and polycarbonates 有权
标题翻译：制备碳酸二烷基酯的方法及其在制备碳酸二芳基酯和聚碳酸酯中的用途
公开(公告)号：US20070083059A1
公开(公告)日：2007-04-12
申请号：US11248390
申请日：2005-10-12
申请人： Thodla Ramgopal , Mario Collado , Vijaya Narasaiah , Ignacio Fernandez
发明人： Thodla Ramgopal , Mario Collado , Vijaya Narasaiah , Ignacio Fernandez
IPC分类号： C07C69/96
CPC分类号： C08G64/30 , C07C68/005 , C07C68/06 , C07C69/96
摘要： A method of making a dialkyl carbonate comprises: reacting, in a reactor comprising tantalum, an alkanol, oxygen, and carbon monoxide, in the presence of a catalyst. The reaction occurs in a mixture comprising a liquid phase wherein the liquid phase comprises about 4 to about 12 weight percent water based on the total weight of the liquid phase
摘要翻译：制备碳酸二烷基酯的方法包括：在包含钽的反应器中，在催化剂存在下，使烷醇，氧和一氧化碳反应。反应发生在包含液相的混合物中，其中液相包含约4至约12重量％的水，基于液相的总重量

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