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1. 发明授权

US06964813B2 Ultraviolet curable resin composition and photo solder resist including the same 有权
标题翻译：紫外线固化型树脂组合物及含有它的光阻焊剂
公开(公告)号：US06964813B2
公开(公告)日：2005-11-15
申请号：US10450464
申请日：2001-12-06
申请人： Soichi Hashimoto
发明人： Soichi Hashimoto
IPC分类号： C08F8/08 , C08F283/06 , C08F290/12 , C08F290/14 , C08F299/00 , C08F299/02 , C08G59/14 , C08G59/42 , C08L63/10 , G03F7/038 , H05K3/28 , B32B27/38 , C08L63/00
CPC分类号： C08G59/1494 , C08F8/00 , C08F283/06 , C08F290/126 , C08F290/142 , C08F299/00 , C08F2800/20 , C08F2810/30 , C08G59/4292 , C08L63/10 , G03F7/038 , G03F7/0388 , H05K3/287 , Y10S428/901 , Y10T428/31511 , C08L2666/22 , C08F8/14 , C08F2220/325
摘要： An ultraviolet curable resin composition is provided, which is excellent in developing width and resolution, and exhibits good solder heat resistance and resistance to gold plating. This resin composition comprises (A) an ultraviolet curable resin obtained by reacting an epoxy-group containing polymer (a), which is prepared by polymerizing an ethylenically unsaturated monomer component including an ethylenically unsaturated monomer (i) having an epoxy group, with an ethylenically unsaturated monomer (b) having a carboxyl group to obtain an intermediate product, and then reacting the intermediate product with a saturated or unsaturated polybasic acid anhydride (c); (B) an epoxy compound having at least two epoxy groups in its molecule; (C) a photo-polymerization initiator; (D) a diluent; and (E) an ultraviolet curable resin obtained by reacting a novolac epoxy compound (e) with the ethylenically unsaturated monomer (b) having a carboxyl group, and then reacting a resultant intermediate product with the saturated or unsaturated polybasic acid anhydride (c). The ultraviolet curable resin (E) has an acid value of 10 mgKOH/g or more and less than 45 mgKOH/g.
摘要翻译：提供了紫外线固化树脂组合物，其显影宽度和分辨率优异，并且具有良好的焊料耐热性和耐镀金性。该树脂组合物包含（A）通过将包含具有环氧基的烯属不饱和单体（i）的烯键式不饱和单体组分与烯属不饱和单体（i）聚合而制备的含环氧基的聚合物（a）具有羧基的不饱和单体（b）以获得中间产物，然后使中间产物与饱和或不饱和多元酸酐（c）反应; （B）分子中具有至少两个环氧基的环氧化合物; （C）光聚合引发剂; （D）稀释剂; 和（E）通过使酚醛清漆环氧化合物（e）与具有羧基的烯键式不饱和单体（b）反应得到的紫外线固化树脂，然后使得到的中间产物与饱和或不饱和多元酸酐（c）反应。紫外线固化性树脂（E）的酸值为10mgKOH / g以上且小于45mgKOH / g。

2. 发明申请

US20050043490A1 Polymerizable compounds and compositions 审中-公开
标题翻译：可聚合的化合物和组合物
公开(公告)号：US20050043490A1
公开(公告)日：2005-02-24
申请号：US10938459
申请日：2004-09-10
申请人： Joachim Klee , Uwe Walz
发明人： Joachim Klee , Uwe Walz
IPC分类号： A61K6/00 , A61K6/083 , A61K6/087 , A61K6/09 , C08F283/02 , C08F290/06 , C08G18/83 , C08G59/10 , C08G59/12 , C08G59/14 , C08G59/17 , C08G59/42 , C08G63/02 , C08F267/04
CPC分类号： A61K6/0017 , A61K6/0032 , A61K6/083 , A61K6/087 , A61K6/09 , C08F283/02 , C08F290/06 , C08F290/061 , C08F290/064 , C08G18/835 , C08G59/10 , C08G59/12 , C08G59/1466 , C08G59/1494 , C08G59/4292 , C08G2270/00 , C08L63/00 , C08L33/00 , C08L75/16
摘要： An esterified macromonomer within the scope of the general formula: wherein Z is an organic moiety, R1 is hydrogen or a substituted or unsubstituted alkyl having from 1 to 12 carbon atoms, oxyalkyl having from 1 to 12 carbon atoms, alkenyl having from 2 to 12 carbon atoms, cycloalkyl having from 5 to 12 carbon atoms, aryl having from 6 to 12 carbon atoms or aralkyl having from 7 to 12 carbon atoms, each E independently is a hydroxyl group, an organic ester moiety or an inorganic ester containing moiety and at least one E is an ester containing moiety, n and m each independently is an integer from 2 to 12. The esterified macromonomer is obtainable by esterification of at least a portion of the —OH groups of a macromonomer having at least one terminal double bond with at least one derivative of an inorganic or organic acid which introduces pendant groups exhibiting at least one acid moiety selected from the group of consisting of —COOH, —PO3H2, —SO3H, —BO2H or salts thereof. The number of the acid moieties is chosen such that a polymer obtained by polymerizing those monomers has an adhesive strength to dentine of at least 2 MPa.
摘要翻译：在通式范围内的酯化大分子单体：其中Z是有机部分，R 1是氢或具有1至12个碳原子的取代或未取代的烷基，具有1至12个碳原子的烷氧基，具有2至12个的烯基碳原子，具有5至12个碳原子的环烷基，具有6至12个碳原子的芳基或具有7至12个碳原子的芳烷基，每个E独立地是羟基，有机酯部分或含无机酯的部分，至少一个E是含酯部分，n和m各自独立地为2至12的整数。酯化的大分子单体可通过至少一部分具有至少一个末端双键的大分子单体的-OH基团酯化得到引入具有至少一个选自-COOH，-PO 3 H 2，-SO 3 H，-BO 2 H或其盐的至少一个酸基部分的侧基的无机或有机酸的至少一种衍生物。选择酸部分的数目使得通过聚合这些单体获得的聚合物对牙本质的粘合强度至少为2MPa。

3. 发明申请

US20030082355A1 Photocurable/thermosetting composition for forming matte film 有权
标题翻译：用于形成无光泽膜的光固化/热固性组合物
公开(公告)号：US20030082355A1
公开(公告)日：2003-05-01
申请号：US10216802
申请日：2002-08-13
发明人： Satoru Iwaida , Yoshihiro Ohno , Masayuki Isono , Akio Sekimoto
IPC分类号： C08F002/46 , C08J003/28 , C08K003/00 , B32B003/00 , B32B007/00 , B32B015/00
CPC分类号： G03F7/0388 , C08G59/4246 , C08G59/4292 , C09D163/00 , G03F7/032 , G03F7/038 , H05K3/287 , Y10T428/24917 , C08L2666/02
摘要： A photocurable and thermosetting composition which is useful in forming a matte film and can be developed with an aqueous alkaline solution is provided. The composition comprises (A) a photosensitive prepolymer obtained by causing a saturated or unsaturated polybasic acid anhydride to react with a hydroxyl group of an esterification product of a novolak type epoxy compound and an unsaturated monocarboxylic acid, (B) a carboxyl group-containing copolymer resin, (C) a photopolymerization initiator, (D) a diluent, (E) a polyfunctional epoxy compound having at least two epoxy groups in its molecule, and, when necessary, (F) an inorganic filler. The composition may further comprise (G) an epoxy resin curing agent. This composition can be advantageously used for the formation of a solder resist on a printed circuit board.
摘要翻译：提供了可用于形成无光泽膜并且可以用碱性水溶液显影的光固化和热固性组合物。组合物包含（A）通过使饱和或不饱和多元酸酐与酚醛清漆型环氧化合物和不饱和一元羧酸的酯化产物的羟基反应获得的光敏预聚物，（B）含羧基的共聚物树脂，（C）光聚合引发剂，（D）稀释剂，（E）分子中具有至少两个环氧基的多官能环氧化合物，必要时，（F）无机填料。组合物还可以包含（G）环氧树脂固化剂。该组合物可有利地用于在印刷电路板上形成阻焊剂。

4. 发明授权

US06555592B2 Photothermosetting composition comprising acrylated epoxy resin 有权
标题翻译：含有丙烯酸酯化环氧树脂的光热固化组合物
公开(公告)号：US06555592B2
公开(公告)日：2003-04-29
申请号：US09793631
申请日：2001-02-27
申请人： Chao-Hui Tseng , Fu-Lung Chen
发明人： Chao-Hui Tseng , Fu-Lung Chen
IPC分类号： G03F7004
CPC分类号： G03F7/032 , C08F283/10 , C08G59/4292 , C08L63/10 , G03F7/0388 , H05K3/287
摘要： A photothermosetting composition is described which contains a base resin (A), a photopolymerizable photomonomer or photooligomer (B), a photoinitiator (C), an epoxide compound containing at least two epoxy groups (D), and an organic solvent. The base resin (A) an epoxide compound (a) containing at least two epoxy groups, an unsaturated monobasic acid (b), a saturated or unsaturated dibasic acid (c), and a saturated or unsaturated acid anhydride (d) according to the ratio of (a)/(b)/(c) of 1:0.90˜0.95:0.025˜0.050 and the acid value of the base resin is in the range of 40˜49 mg KOH/g. This photothermosetting component was coating on the substrate, and then dried by baking, exposed by light, developed, irradiated by ultraviolet light or heated, and cured to form a solder mask.
摘要翻译：描述了含有基础树脂（A），光聚合性单体或光致抗体（B），光引发剂（C），含有至少两个环氧基的环氧化合物（D）和有机溶剂的光热固化组合物。基础树脂（A）含有至少两个环氧基，不饱和一元酸（b），饱和或不饱和二元酸（c）和饱和或不饱和酸酐（d）的环氧化合物（a）根据（a）/（b）/（c）的比例为1:0.90〜0.95:0.025〜0.050，基础树脂的酸值在40〜49mg KOH / g的范围内。将该光热固化成分涂布在基板上，然后通过烘烤干燥，通过光照射，显影，紫外线照射或加热，并固化形成焊接掩模。

5. 发明申请

US20020143108A1 Polymerizable compounds and compositions 审中-公开
标题翻译：可聚合的化合物和组合物
公开(公告)号：US20020143108A1
公开(公告)日：2002-10-03
申请号：US10054360
申请日：2002-01-22
发明人： Joachim E. Klee , Uwe Walz
IPC分类号： C08F267/04
CPC分类号： C08L67/07 , A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/087 , A61K6/09 , C08F283/02 , C08F290/06 , C08F290/061 , C08F290/064 , C08G18/835 , C08G59/10 , C08G59/12 , C08G59/1466 , C08G59/1494 , C08G59/4292 , C08G63/52 , C08G2270/00 , Y10S525/922 , C08L33/00 , C08L43/02 , C08L63/00 , C08L75/16
摘要： An esterified macromonomer within the scope of the general formula: 1 wherein Z is an organic moiety, R1 is hydrogen or a substituted or unsubstituted alkyl having from 1 to 12 carbon atoms, oxyalkyl having from 1 to 12 carbon atoms, alkenyl having from 2 to 12 carbon atoms, cycloalkyl having from 5 to 12 carbon atoms, aryl having from 6 to 12 carbon atoms or aralkyl having from 7 to 12 carbon atoms, each E independently is a hydroxyl group, an organic ester moiety or an inorganic ester containing moiety and at least one E is an ester containing moiety, n and m each independently is an integer from 2 to 12. The esterified macromonomer is obtainable by esterification of at least a portion of the nullOH groups of a macromonomer having at least one terminal double bond with at least one derivative of an inorganic or organic acid which introduces pendant groups exhibiting at least one acid moiety selected from the group of consisting of nullCOOH, nullPO3H2, nullSO3H, nullBO2H or salts thereof. The number of the acid moieties is chosen such that a polymer obtained by polymerizing those monomers has an adhesive strength to dentine of at least 2 MPa.
摘要翻译：在通式范围内的酯化大分子单体：其中Z是有机部分，R 1是氢或具有1至12个碳原子的取代或未取代的烷基，具有1至12个碳原子的烷氧基，具有2至12个的烯基碳原子，具有5至12个碳原子的环烷基，具有6至12个碳原子的芳基或具有7至12个碳原子的芳烷基，每个E独立地是羟基，有机酯部分或含无机酯的部分，至少一个E是含酯部分，n和m各自独立地为2至12的整数。酯化的大分子单体可通过至少一部分具有至少一个末端双键的大分子单体的-OH基团酯化得到引入具有至少一个选自-COOH，-PO 3 H 2，-SO 3 H，-BO 2 H或其盐的至少一个酸基部分的侧基的无机或有机酸的至少一种衍生物。选择酸部分的数量使得通过聚合这些单体获得的聚合物对牙本质的粘合强度至少为2MPa

6. 发明申请

US20020120031A1 Photothermosetting component 有权
标题翻译：光热组件
公开(公告)号：US20020120031A1
公开(公告)日：2002-08-29
申请号：US09793631
申请日：2001-02-27
发明人： Fu-Lung Chen
IPC分类号： C08G002/00
CPC分类号： G03F7/032 , C08F283/10 , C08G59/4292 , C08L63/10 , G03F7/0388 , H05K3/287
摘要： This invention is to provide a kind of photothermosetting component, which was composed of a base resin (A), a photopolymerizable photomonomer or photooligomer (B), a photoinitiator (C), an epoxide compound containing at least two epoxy groups (D), and an organic solvent. A base resin (A) is composed of containing at least two epoxy groups of epoxide compound (a), containing at least two double bonds of unsaturated monobasic acid (b), a saturated or unsaturated dibasic acid (c), and a saturated or unsaturated acid anhydride (d) according to the typical ratio. This photothermosetting component was coating on the substrate, and then dried by baking, exposed by light, developed, irradiated by ultraviolet light or heated, and cured to form a solder mask.
摘要翻译：本发明提供一种由基础树脂（A），光聚合性单色
剂或光引发剂（B），光引发剂（C），含有至少两个环氧基（D）的环氧化合物组成的光热组分，和有机溶剂。基础树脂（A）由含有至少两个环氧化合物（a）的环氧基组成，含有至少两个不饱和一元酸（b）的双键，饱和或不饱和二元酸（c）和饱和或不饱和二元酸不饱和酸酐（d）根据典型比例。将该光热固化成分涂布在基板上，然后通过烘烤干燥，通过光照射，显影，紫外线照射或加热，并固化形成焊接掩模。

7. 发明授权

US06359082B1 Process for the preparation of epoxy (meth) acrylates reacting epoxy compounds with anhydride and oh-functional (meth)acrylic-polyetherpolyol 失效
标题翻译：制备环氧（甲基）丙烯酸酯的方法使环氧化合物与酸酐和欧姆官能（甲基）丙烯酸 - 聚醚多元醇反应
公开(公告)号：US06359082B1
公开(公告)日：2002-03-19
申请号：US08878159
申请日：1997-06-18
申请人： Jürgen Meixner
发明人： Jürgen Meixner
IPC分类号： C08G5917
CPC分类号： C08G59/4284 , C08F20/32 , C08G59/4292 , C08L63/10 , Y10S525/922
摘要： The present invention relates to a process for the preparation of epoxy(meth)acrylates by simultaneously reacting 1 equivalent of organic compounds containing epoxide groups with A) 0.8 to 1.2 moles of organic dicarboxylic anhydrides having a molecular weight from 98 to 166 and B) 0.8 to 1.2 OH equivalents of OH group-containing reaction products, which are prepared at a COOH/OH equivalent ratio of 0.6:1 to 0.95:1, of a) (meth)acrylic acid and b) tri- or tetrahydric ether alcohols having a molecular weight of 180 to 1000 and containing at least two ethylene and/or propylene oxide units as part of an ether structure.
摘要翻译：本发明涉及一种制备环氧（甲基）丙烯酸酯的方法，它同时使1当量含有环氧基的有机化合物与A）0.8至1.2摩尔的分子量为98至166和B = 0.8至1.2的有机二羧酸酐反应 OH等价的OH基的反应产物，它们是以（a）（甲基）丙烯酸和b）分子量为180的三或四元醚醇的COOH / OH当量比为0.6:1至0.95:1制备的至1000，并含有至少两个乙烯和/或环氧丙烷单元作为醚结构的一部分。

8. 发明授权

US4866134A Laminate with layer of rubber-modified vinyl ester and unsaturated polyester 失效
标题翻译：层压橡胶改性乙烯基酯和不饱和聚酯层
公开(公告)号：US4866134A
公开(公告)日：1989-09-12
申请号：US184373
申请日：1988-04-21
申请人： Hidekazu Takano , Tetsuo Kunitomi , Shigehiro Okada , Toshio Awaji , Katsuaki Shindo , Daisuke Atobe
发明人： Hidekazu Takano , Tetsuo Kunitomi , Shigehiro Okada , Toshio Awaji , Katsuaki Shindo , Daisuke Atobe
IPC分类号： C08F299/00 , C08C19/30 , C08F283/10 , C08F290/00 , C08F299/02 , C08G59/00 , C08G59/14 , C08G59/40 , C08G59/42 , C08G59/56 , C08K5/04 , C08L15/00 , C08L33/00 , C08L33/02 , C08L63/00 , C08L63/10 , C08L67/00 , H05K1/03
CPC分类号： C08G59/56 , C08C19/30 , C08F283/10 , C08G59/4292 , C08L63/10 , H05K1/0326 , Y10T428/2826 , Y10T428/31522 , Y10T428/31696
摘要： An electric metal foil-plated laminate sheet which is obtained by laminating a cured layer of a thermosetting resin composition with electroconductive foils, said thermosetting resin composition comprising 30-85% by weight of (A) a rubber-modified vinyl ester obtained by reacting,(a) an epoxy resin,(b) a carboxyl group containing rubbery polymer derived from a conjugated diene, and(c) at least one unsaturated monocarboxylic acid selected from the group consisting of acrylic acid and methacrylic acid to react one another in amounts such that, based on 100 parts by weight of (a) the epoxy resin, (b) the carboxyl group containing rubbery polymer accounts for a proportion in the range of 5 to 80 parts by weight and that the total number of carboxylic group contained in (b) the rubbery polymer and (c) the unsaturated monocarboxylic acid falls in the range of 1.3 to 1.5 per each of the epoxy groups contained in (a) the epoxy resin at a temperature of 90.degree. to 120.degree. C., 5-30% weight of (B) a specific unsaturated polyester, and 10-60% by weight of (C) a radically polymerizable unsaturated monomer, wherein (A)+(B)+(C) equals 100% by weight.
摘要翻译：一种通过将热固性树脂组合物的固化层与导电箔层压而获得的电镀金属箔层压片，所述热固性树脂组合物包含30-85重量％的（A）通过使（a）环氧树脂，（b）由共轭二烯衍生的含羧基的橡胶状聚合物，和（c）至少一种选自丙烯酸和甲基丙烯酸的不饱和一元羧酸，基于100重量份的（a）环氧树脂，（b）含羧基的橡胶状聚合物的比例在5-80重量份的范围内，并且（ b）橡胶状聚合物和（c）不饱和一元羧酸在环氧树脂（a）中包含的每个环氧基中的温度在90℃至120℃的范围内为1.3至1.5，5-30 ％重量（B）特定的不饱和聚酯和10-60重量％的（C）可自由基聚合的不饱和单体，其中（A）+（B）+（C）等于100重量％。

9. 发明授权

US4764430A Crosslinkable compositions containing polyepoxides and polyacid curing agents 失效
标题翻译：含有聚环氧化物和多元酸固化剂的交联组合物
公开(公告)号：US4764430A
公开(公告)日：1988-08-16
申请号：US1304
申请日：1987-01-08
申请人： William P. Blackburn , Debra L. Singer
发明人： William P. Blackburn , Debra L. Singer
IPC分类号： C08G59/18 , B05D7/00 , C08G59/32 , C08G59/42 , C09D163/00 , B05D1/36 , B32B27/38 , C08G59/40
CPC分类号： B05D7/536 , C08G59/3209 , C08G59/4276 , C08G59/4292 , C09D163/00 , Y10T428/31511
摘要： Curable, liquid coating compositions based on polyepoxides and polyacid curing agents are disclosed. The compositions also contain volatile components such as solvent or curing agents which release volatile components upon curing. Also present is a relatively long chain aliphatic monocarboxylic acid which is present to improve the appearance of the coatings. The compositions are useful as coating compositions particularly as clear coats in color-plus-clear automotive coatings.
摘要翻译：公开了基于聚环氧化物和多元酸固化剂的可固化的液体涂料组合物。组合物还含有挥发性成分，例如在固化时释放挥发性组分的溶剂或固化剂。还存在一种相对长链的脂族单羧酸，其用于改善涂层的外观。该组合物可用作涂料组合物，特别是作为透明涂料在彩色汽车涂料中。

10. 再颁专利

USRE31310E Impact resistant vinyl ester resin and process for making same 失效
标题翻译：耐冲击乙烯基酯树脂及其制造方法
公开(公告)号：USRE31310E
公开(公告)日：1983-07-12
申请号：US124055
申请日：1980-02-25
申请人： Daniel J. Najvar
发明人： Daniel J. Najvar
IPC分类号： C08F8/00 , C08F8/08 , C08G8/02 , C08G59/42
CPC分类号： C08F8/00 , C08F8/08 , C08G59/4292 , C08G8/02
摘要： Vinyl ester resins with improved impact resistance and other benefits and advantages may be obtained by a process modification wherein up to 20 percent of the unsaturated monocarboxylic acid, which is reacted with a polyepoxide, is replaced by an equivalent amount of a liquid carboxy terminated polydiene rubber capable of reacting with epoxy groups to form a chemically bound molecule. .Iadd.

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