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1. 发明申请

US20180079667A1 PROCESS FOR THE TREATMENT OF WATER 审中-公开
公开(公告)号：US20180079667A1
公开(公告)日：2018-03-22
申请号：US15710782
申请日：2017-09-20
申请人： William Whitney Burch
发明人： William Whitney Burch
IPC分类号： C02F1/70
CPC分类号： C02F1/705 , C01B3/08 , C01D1/04 , C01D7/00 , C01F11/18 , C02F1/04 , C25C3/02
摘要： Waste water is treated by contacting it with sodium to form hydrogen which is then contacted with air in a combustion chamber to produce clean water and heat.

2. 发明授权

US09856569B2 Apparatus and method of producing metal in a nasicon electrolytic cell 有权
公开(公告)号：US09856569B2
公开(公告)日：2018-01-02
申请号：US13935035
申请日：2013-07-03
申请人： FIELD UPGRADING LIMITED
发明人： Sai Bhavaraju
IPC分类号： C25C1/22 , C25C1/06 , C25C3/06 , C25C3/28 , C25B1/14 , C25C1/02 , C25C3/02 , C25C3/24 , C25C3/34
CPC分类号： C25C1/22 , C25B1/14 , C25C1/02 , C25C1/06 , C25C3/02 , C25C3/06 , C25C3/24 , C25C3/28 , C25C3/34
摘要： A process of producing metal that includes adding a quantity of a alkoxide (M(OR)x) or another metal salt to a cathode compartment of an electrolytic cell and electrolyzing the cell. This electrolyzing causes a quantity of alkali metal ions to migrate into the cathode compartment and react with the metal alkoxide, thereby producing metal and an alkali metal alkoxide. In some embodiments, the alkali metal is sodium such that the sodium ions will pass through a sodium ion selective membrane, such as a NaSICON membrane, into the cathode compartment.

3. 发明申请

US20170016128A1 PROCESS FOR RECOVERING ALKALI METALS AND SULFUR FROM ALKALI METAL SULFIDES AND POLYSULFIDES 审中-公开
标题翻译：从碱金属硫化物和聚合物中回收碱金属和硫的方法
公开(公告)号：US20170016128A1
公开(公告)日：2017-01-19
申请号：US15279926
申请日：2016-09-29
申请人： Ceramatec, Inc.
发明人： John Howard Gordon
IPC分类号： C25C1/02 , C25C3/02 , C10G32/02 , C25B1/00 , C01B17/22 , C01B17/34
CPC分类号： C25C1/02 , C01B17/22 , C01B17/34 , C10G32/02 , C10G2300/202 , C25B1/00 , C25C3/02 , C25C7/06
摘要： Alkali metals and sulfur may be recovered from alkali monosulfide and polysulfides in an electrolytic process that utilizes an electrolytic cell having an alkali ion conductive membrane. An anolyte includes an alkali monosulfide, an alkali polysulfide, or a mixture thereof and a solvent that dissolves elemental sulfur. A catholyte includes molten alkali metal. Applying an electric current oxidizes sulfide and polysulfide in the anolyte compartment, causes alkali metal ions to pass through the alkali ion conductive membrane to the catholyte compartment, and reduces the alkali metal ions in the catholyte compartment. Liquid sulfur separates from the anolyte and may be recovered. The electrolytic cell is operated at a temperature where the formed alkali metal and sulfur are molten.
摘要翻译：碱金属和硫可以在利用具有碱离子导电膜的电解池的电解方法中从单硫化物和多硫化物中回收。阳极电解液包括碱金属一硫化物，碱性多硫化物或其混合物和溶解元素硫的溶剂。阴极电解液包括熔融碱金属。施加电流在阳极电解液室中氧化硫化物和多硫化物，导致碱金属离子通过碱离子导电膜到阴极电解液室，并减少阴极电解液室中的碱金属离子。液态硫与阳极电解液分离，可以回收。电解池在形成的碱金属和硫熔融的温度下运行。

4. 发明申请

US20170009358A1 METHOD FOR SIMULTANEOUSLY RECOVERING COBALT AND MANGANESE FROM LITHIUM BASED BATTERY 审中-公开
标题翻译：从锂离子电池同时回收钴和锰的方法
公开(公告)号：US20170009358A1
公开(公告)日：2017-01-12
申请号：US15121212
申请日：2015-01-23
申请人： KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCE (KIGAM)
发明人： Shun-Myung SHIN , Sung-Ho JU , Dong-Ju SHIN , Jei-Pil WANG
IPC分类号： C25C7/02 , H01M6/52 , C25C1/10 , C25C1/08 , C22C11/06 , C22B47/00 , C22B3/00 , C22B7/00 , C22B1/02 , C22B1/248 , H01M10/54 , C25C7/00
CPC分类号： C25C7/02 , C22B1/02 , C22B1/248 , C22B7/007 , C22B23/043 , C22B23/0461 , C22B47/00 , C22B47/0009 , C22C11/06 , C25C1/08 , C25C1/10 , C25C3/02 , C25C7/007 , H01M6/52 , H01M10/54 , Y02P10/234 , Y02W30/84
摘要： The present invention relates to a method of simultaneously recovering cobalt (Co) and manganese (Mn) from lithium-based BATTERY, and more particularly, to a method that is capable of simultaneously recovering cobalt and manganese from lithium-based BATTERY, i.e., recycled resources that contain large amounts of cobalt and manganese, with high purities using multistage leaching and electrowinning methods. According to the method of the present invention, cobalt and manganese can be simultaneously recovered from lithium-based BATTERY as recycled resources, and a recovery method that is cost-effective compared to conventional methods can be provided.
摘要翻译：本发明涉及从锂基电池同时回收钴（Co）和锰（Mn）的方法，更具体地说，涉及一种能够从锂基电池中同时回收钴和锰的方法，即再循环含有大量钴和锰的资源，具有使用多级浸出和电解提取方法的高纯度。根据本发明的方法，可以从锂基电池中同时回收钴和锰作为循环资源，并且可以提供与常规方法相比成本有效的回收方法。

5. 发明申请

US20140328740A1 METHODS FOR PRODUCING SILANE 有权
标题翻译：生产硅烷的方法
公开(公告)号：US20140328740A1
公开(公告)日：2014-11-06
申请号：US14335531
申请日：2014-07-18
申请人： SunEdison LLC
发明人： Puneet Gupta , Henry F. Erk , Alexis Grabbe
IPC分类号： C01B33/029 , C01B33/04
CPC分类号： C01B33/029 , C01B33/043 , C25B1/003 , C25C3/02
摘要： Methods and systems for producing silane that use electrolysis to regenerate reactive components therein are disclosed. The methods and systems may be substantially closed-loop with respect to halogen, an alkali or alkaline earth metal and/or hydrogen.
摘要翻译：公开了用于生产使用电解以再生其中的反应性组分的硅烷的方法和系统。所述方法和系统可以相对于卤素，碱金属或碱土金属和/或氢基本上是闭环的。

6. 发明授权

US08858677B2 Method and apparatus for recovering valuable substance from lithium secondary battery 有权
标题翻译：从锂二次电池中回收有价物质的方法和装置
公开(公告)号：US08858677B2
公开(公告)日：2014-10-14
申请号：US12084705
申请日：2006-02-02
申请人： Toshiya Kakuta , Seiichiro Yamazaki
发明人： Toshiya Kakuta , Seiichiro Yamazaki
IPC分类号： C22B26/12 , C22B1/00 , C25C3/02
CPC分类号： H01M10/54 , C25C3/02 , C25C7/005 , H01M4/131 , H01M10/052 , Y02W30/84
摘要： A valuable-substance recovery method according to the present invention includes: a solvent peeling step (S3) of dissolving a resin binder included in an electrode material by immersing crushed pieces of a lithium secondary battery into a solvent, so as to peel off the electrode material containing valuable substances from a metal foil constituting the electrode; a filtering step (S4) of filtering a suspension of the solvent, so as to separate and recover the electrode material containing the valuable substances and a carbon material; a heat treatment step (S5) of heating the recovered electrode material containing the valuable substances and the carbon material, under an oxidative atmosphere, so as to burn and remove the carbon material; and a reducing reaction step (S6) of immersing the resultant electrode material containing the valuable substances into a molten salt of lithium chloride containing metal lithium, so as to perform a reducing reaction.
摘要翻译：根据本发明的有价值的物质回收方法包括：通过将锂二次电池的碎片浸入溶剂中来溶解包含在电极材料中的树脂粘合剂的溶剂剥离步骤（S3），以剥离电极含有构成电极的金属箔的有价值物质的材料; 对溶剂的悬浮液进行过滤的过滤工序（S4），分离回收含有有价物质的电极材料和碳材料; 在氧化气氛下加热含有有价物质和碳材料的回收电极材料的热处理步骤（S5），以便燃烧和除去碳材料; 以及将含有有价物质的所得电极材料浸入含有金属锂的氯化锂的熔融盐中的还原反应步骤（S6），以进行还原反应。

7. 发明申请

US20140008239A1 Apparatus and Method of Producing Metal in a Nasicon Electrolytic Cell 有权
标题翻译：在纳斯康斯电解池中生产金属的装置和方法
公开(公告)号：US20140008239A1
公开(公告)日：2014-01-09
申请号：US13935035
申请日：2013-07-03
申请人： Ceramatec, Inc.
发明人： Sai Bhavaraju
IPC分类号： C25C1/22
CPC分类号： C25C1/22 , C25B1/14 , C25C1/02 , C25C1/06 , C25C3/02 , C25C3/06 , C25C3/24 , C25C3/28 , C25C3/34
摘要： A process of producing metal that includes adding a quantity of a alkoxide (M(OR)x) or another metal salt to a cathode compartment of an electrolytic cell and electrolyzing the cell. This electrolyzing causes a quantity of alkali metal ions to migrate into the cathode compartment and react with the metal alkoxide, thereby producing metal and an alkali metal alkoxide. In some embodiments, the alkali metal is sodium such that the sodium ions will pass through a sodium ion selective membrane, such as a NaSICON membrane, into the cathode compartment.
摘要翻译：一种生产金属的方法，包括向电解池的阴极室加入一定数量的醇盐（M（OR）x）或另一种金属盐，并对该电池进行电解。这种电解使一定量的碱金属离子迁移到阴极室并与金属醇盐反应，从而产生金属和碱金属醇盐。在一些实施方案中，碱金属是钠，使得钠离子将通过钠离子选择性膜，例如NaSICON膜进入阴极室。

8. 发明授权

US07897028B2 Process for the recovery of materials from a desulfurization reaction 有权
标题翻译：从脱硫反应中回收材料的方法
公开(公告)号：US07897028B2
公开(公告)日：2011-03-01
申请号：US10905782
申请日：2005-01-20
申请人： John H. Gordon , Ashok V. Joshi
发明人： John H. Gordon , Ashok V. Joshi
IPC分类号： C10G25/12
CPC分类号： C10G25/12 , C10G19/08 , C22B1/08 , C22B3/045 , C22B7/002 , C22B7/007 , C22B23/00 , C22B26/12 , C25B1/24 , C25C3/02 , Y02P10/234
摘要： Disclosed herein is an improved method for regenerating materials from a desulfurization/demetallation reaction. The desulfurization/demetallation reaction preferably has products including one or more of an alkali sulfide, polysulfide or hydrosulfide, or alkali earth sulfide, polysulfide, or hydrosulfide. The method includes the steps of reacting the desulfurization/demetallation products with a halogen, liberating and removing sulfur from the product, and then electrolyzing the halogenated products to separate the halogen from the alkali metal or alkali earth metal.
摘要翻译：本文公开了一种用于从脱硫/脱金属反应再生材料的改进方法。脱硫/脱金属反应优选具有包括碱金属硫化物，多硫化物或氢硫化物或碱土金属硫化物，多硫化物或氢硫化物中的一种或多种的产物。该方法包括以下步骤：使脱硫/脱金属产物与卤素反应，从产物中释放和除去硫，然后电解卤化产物以将卤素与碱金属或碱土金属分离。

9. 发明申请

US20090152122A1 Method for electrolyzing molten salt, electrolytic cell, and process for producing ti using said method 审中-公开
标题翻译：使用所述方法电解熔融盐，电解池和制造方法的方法
公开(公告)号：US20090152122A1
公开(公告)日：2009-06-18
申请号：US11991072
申请日：2006-08-22
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Toru Uenishi , Masahiko Hori , Kazuo Takemura , Katsunori Dakeshita
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Toru Uenishi , Masahiko Hori , Kazuo Takemura , Katsunori Dakeshita
IPC分类号： C25B1/26 , C25B9/00 , C25C3/28
CPC分类号： C22B34/129 , C22B5/04 , C22B34/1268 , C25C3/02 , C25C7/005
摘要： The present invention provides a method for electrolyzing molten salt that can enhance the concentration of metal-fog forming metal in the molten salt by carrying out the electrolysis under conditions that the molten salt containing the chloride of metal-fog forming metal is supplied from one end of an electrolytic cell to a space between an anode and a cathode in a continuous or intermittent manner to provide a flow rate in one direction to the molten salt in the vicinity of the surface of the cathode and thus to allow the molten salt to flow in one direction in the vicinity of the surface of the cathode. According to the present invention, while high current efficiency is maintained, only the molten salt enriched with metal-fog forming metal such as Ca can be effectively taken out. Further, this method can easily be carried out by using the electrolytic cell according to the present invention. Furthermore, the application of the method for electrolyzing molten salt according to the present invention to the production of Ti by Ca reduction can realize the production of metallic Ti with high efficiency. Thus, the method for electrolyzing molten salt, the electrolytic cell, and the process for producing Ti, each according to the present invention, can be effectively utilized in the production of Ti by Ca reduction.
摘要翻译：本发明提供了一种电解熔融盐的方法，该方法可以通过在从一端供给含有金属雾形成金属的氯化物的熔融盐的条件下进行电解，从而提高熔融盐中金属雾形成金属的浓度的电解池以连续或间歇的方式连接到阳极和阴极之间的空间，以在阴极表面附近向熔融盐提供沿一个方向的流速，从而允许熔融盐流入在阴极表面附近的一个方向。根据本发明，在保持高电流效率的同时，仅有效地除去富含金属雾形成金属如Ca的熔盐。此外，该方法可以通过使用根据本发明的电解槽容易地进行。另外，通过将本发明的熔盐电解方法应用于通过Ca还原生产Ti，可以实现高效率地生产金属Ti。因此，根据本发明的电解熔融盐，电解槽和制造Ti的方法的方法可以有效地用于通过Ca还原生产Ti。

10. 发明申请

US20080110765A1 Method For Producing Metal 审中-公开
标题翻译：生产金属的方法
公开(公告)号：US20080110765A1
公开(公告)日：2008-05-15
申请号：US11792954
申请日：2005-12-09
申请人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi
发明人： Tadashi Ogasawara , Makoto Yamaguchi , Masahiko Hori , Toru Uenishi
IPC分类号： C25C3/02 , C25C1/22
CPC分类号： C25C5/04 , C25B1/26 , C25C3/02 , C25C3/34 , C25C7/04
摘要： A method for producing a metal by an electrolytic process using an yttria-containing porous ceramic body as a diaphragm is provided; the calcium formed by electrolysis cannot pass through the diaphragm, hence the back reaction can be effectively inhibited. Preferably, to be used is a diaphragm comprising a porous ceramic body having a purity of yttrium of 90 mass % or more (more preferably, 99% or more), a porosity of 1% or more and a pore diameter of 20 μm or less, and having a thickness of 0.05-50 mm and a metal halide is used as the electrolytic bath. The method can be utilized for producing metals such as calcium or rare earth elements, in particular. For example, when the method is applied to the production of calcium, metallic calcium can be produced with ease and at low cost without the need for enormous heat energy.
摘要翻译：提供了使用含有氧化钇的多孔陶瓷体作为隔膜的电解法制造金属的方法。通过电解形成的钙不能通过隔膜，因此可以有效地抑制背部反应。优选使用的是具有钇的纯度为90质量％以上（更优选为99％以上），孔隙率为1％以上，孔径为20μm以下的多孔陶瓷体的隔膜，并且具有0.05-50mm的厚度，并且使用金属卤化物作为电解浴。该方法特别可用于生产诸如钙或稀土元素的金属。例如，当将该方法应用于钙的生产时，可以容易且低成本地生产金属钙，而不需要巨大的热能。

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