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1. 发明授权

US08987526B2 Partially halogenated, hydroxylated fullerene and allergen adsorbent using the same 有权
标题翻译：部分卤化，羟基化富勒烯和过敏原吸附剂使用
公开(公告)号：US08987526B2
公开(公告)日：2015-03-24
申请号：US14495438
申请日：2014-09-24
申请人： Osaka University , Totai Co., Ltd.
发明人： Ken Kokubo , Takeshi Noguchi
IPC分类号： C07C35/23 , B01J20/22 , C01B31/02 , C07C17/02 , C07C25/22 , C07C35/52 , C07C29/48 , C07C29/62 , C07C29/124 , B82Y30/00 , B82Y40/00
CPC分类号： B01J20/22 , B82Y30/00 , B82Y40/00 , C01B32/152 , C07C17/02 , C07C25/22 , C07C29/124 , C07C29/48 , C07C29/62 , C07C35/52 , C07C2604/00 , Y10S977/734 , Y10S977/735 , Y10S977/736 , Y10S977/74
摘要： Provided are a novel fullerene derivative which can adsorb quickly and efficiently an allergen which may cause a pollen allergy without releasing the allergen again, does not contain a metal or the like which may cause a harmful effect to a human body, and is easily applicable, impregnable, or chemically bondable onto surface of various materials: and a process for producing the same. The fullerene derivative is characterized in that a halogen group and many hydroxyl groups are bonded directly to a fullerene nucleus. In the case that the halogen group is chlorine, the fullerene derivative can be synthesized by a partial hydroxylation of a chlorinated fullerene or a partial chlorination of a hydroxylated fullerene.
摘要翻译：提供一种新颖的富勒烯衍生物，其可以快速且有效地吸附可能引起花粉过敏的过敏原，而不会再次释放过敏原，不含可能对人体产生有害影响的金属等，并且易于应用，可浸渍或化学粘合到各种材料的表面上的方法及其制备方法。富勒烯衍生物的特征在于卤素基团和许多羟基直接键合到富勒烯核上。在卤素基团为氯的情况下，富勒烯衍生物可以通过氯化富勒烯的部分羟基化或羟基化富勒烯的部分氯化来合成。

2. 发明授权

US08957261B2 Method for producing partially halogenated, hydroxylated fullerene 有权
标题翻译：部分卤化的羟基化富勒烯的制备方法
公开(公告)号：US08957261B2
公开(公告)日：2015-02-17
申请号：US13577868
申请日：2011-01-31
申请人： Ken Kokubo , Takeshi Noguchi
发明人： Ken Kokubo , Takeshi Noguchi
IPC分类号： C07C35/23 , C07C25/22 , C01B31/02 , C07C17/02 , C07C35/52 , C07C29/48 , C07C29/62 , C07C29/124 , B82Y30/00 , B82Y40/00
CPC分类号： B01J20/22 , B82Y30/00 , B82Y40/00 , C01B32/152 , C07C17/02 , C07C25/22 , C07C29/124 , C07C29/48 , C07C29/62 , C07C35/52 , C07C2604/00 , Y10S977/734 , Y10S977/735 , Y10S977/736 , Y10S977/74
摘要： Provided are a novel fullerene derivative which can adsorb quickly and efficiently an allergen which may cause a pollen allergy without releasing the allergen again, does not contain a metal or the like which may cause a harmful effect to a human body, and is easily applicable, impregnable, or chemically bondable onto surface of various materials; and a process for producing the same. The fullerene derivative is characterized in that a halogen group and many hydroxyl groups are bonded directly to a fullerene nucleus. In the case that the halogen group is chlorine, the fullerene derivative can be synthesized by a partial hydroxylation of a chlorinated fullerene or a partial chlorination of a hydroxylated fullerene.
摘要翻译：提供一种新颖的富勒烯衍生物，其可以快速且有效地吸附可能引起花粉过敏的过敏原，而不会再次释放过敏原，不含可能对人体产生有害影响的金属等，并且易于应用，可浸渍或化学粘合到各种材料的表面上; 及其制造方法。富勒烯衍生物的特征在于卤素基团和许多羟基直接键合到富勒烯核上。在卤素基团为氯的情况下，富勒烯衍生物可以通过氯化富勒烯的部分羟基化或羟基化富勒烯的部分氯化来合成。

3. 发明申请

US20130102812A1 WATER-SOLUBLE FLUORESCENT FULLERENE DERIVATIVE, AND PREPARATION METHOD THEREOF 有权
标题翻译：水溶性氟化物衍生物及其制备方法
公开(公告)号：US20130102812A1
公开(公告)日：2013-04-25
申请号：US13643292
申请日：2011-04-25
申请人： Bong Hyun Chung , Jin Young Jeong
发明人： Bong Hyun Chung , Jin Young Jeong
IPC分类号： C07C41/06
CPC分类号： C07C41/06 , B82Y30/00 , C07C2604/00 , C09K11/06 , C09K2211/1011 , Y10S977/74 , Y10S977/847 , C07C43/196
摘要： The present invention relates to a water-soluble fluorescent fullerene derivative and a preparation method thereof, and more particularly to a method of preparing a fullerene derivative having excellent fluorescence in a simple manner by mixing fullerene and a ligand containing a terminal hydroxyl group in a first solvent and reacting the mixture in the presence of a catalyst, and to a water-soluble fluorescent fullerene derivative prepared by the method.According to the method of preparing a water-soluble fluorescent fullerene derivative the present invention, a fullerene derivative having strong fluorescence and hydrophilicity is prepared in a simple and easy manner. In addition, the preparation method enables the intensity and wavelength of fluorescence to be easily controlled depending on the amount of fullerene and the kind of catalyst. The prepared fluorescent fullerene derivative contains a biocompatible ligand, and thus is useful as a biological fluorescent dye. In addition, the fluorescent fullerene derivative has not only fluorescence, but also excellent solubility in a solvent, and thus is useful in the biological field, the medical field, the nanotechnology field, etc.
摘要翻译：本发明涉及一种水溶性荧光富勒烯衍生物及其制备方法，更具体地涉及一种通过在富勒烯中首先混合富勒烯和含有末端羟基的配位体，以简单的方式制备具有优异荧光的富勒烯衍生物的方法溶剂，并在催化剂存在下使混合物反应，并通过该方法制备的水溶性荧光富勒烯衍生物。根据本发明的水溶性荧光富勒烯衍生物的制备方法，以简单易行的方式制备具有强荧光性和亲水性的富勒烯衍生物。此外，该制备方法能够根据富勒烯的量和催化剂的种类容易地控制荧光的强度和波长。制备的荧光富勒烯衍生物含有生物相容性配体，因此可用作生物荧光染料。此外，荧光富勒烯衍生物不仅具有荧光，而且在溶剂中的溶解性优异，因此可用于生物领域，医疗领域，纳米技术领域等。

4. 发明授权

US08084505B2 Substance-containing carbon nanohorn composite having polyamine plug and process for producing the same 有权
标题翻译：含有多胺栓塞的含物质碳纳米复合材料及其制造方法
公开(公告)号：US08084505B2
公开(公告)日：2011-12-27
申请号：US12307473
申请日：2007-07-03
申请人： Ryota Yuge , Hideki Yorimitsu , Masako Yudasaka , Sumio Iijima
发明人： Ryota Yuge , Hideki Yorimitsu , Masako Yudasaka , Sumio Iijima
IPC分类号： A61K9/14 , A61K31/13 , A61K31/16 , A01N33/00 , A01N33/02
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/18 , Y10S977/734 , Y10S977/736 , Y10S977/74 , Y10S977/744 , Y10S977/748 , Y10S977/75
摘要： The present invention provides: a carbon nanohorn composite including a carbon nanohorn, a substance encapsulated in the carbon nanohorn, and a polyamine adsorbed by chemical reaction firmly to a surface functional group present on the opening part on the surface of the carbon nanohorn, wherein the release amount and release rate of the encapsulated substance can be controlled using the difference in size, substituent or three-dimensional structure of the polyamine, which is used as a plug; a method of controlling the release of the encapsulated substance; and a process for producing the carbon nanohorn composite. The release amount and release rate of the substance encapsulated in the carbon nanohorn composite is controlled by selecting a polyamine molecule, which plugs the opening part formed in the carbon nanohorn by oxidation, by its size, substituent or three-dimensional structure.
摘要翻译：本发明提供了一种碳纳米角复合材料，其包含碳纳米角，包封在碳纳米角中的物质，以及通过化学反应吸附的多胺与存在于碳纳米角表面上的开口部分上的表面官能团，其中，可以使用用作塞子的多胺的尺寸，取代基或三维结构的差异来控制包封物质的释放量和释放速率; 控制包封物质释放的方法; 以及生产碳纳米复合材料的方法。通过选择通过其尺寸，取代基或三维结构通过氧化将形成在碳纳米角中的开口部分堵塞的多胺分子来控制包封在碳纳米角复合材料中的物质的释放量和释放速率。

5. 发明申请

US20110071202A1 ANTI-HEPATITIS C VIRUS AGENTS AND ANTI-HIV AGENTS 有权
标题翻译：抗病毒药物C病毒和抗艾滋病毒药物
公开(公告)号：US20110071202A1
公开(公告)日：2011-03-24
申请号：US12956505
申请日：2010-11-30
申请人： Tadahiko Mashino , Kumiko Shimotohno
发明人： Tadahiko Mashino , Kumiko Shimotohno
IPC分类号： A61K31/415 , A61K31/40 , A61P31/12 , A61P31/18
CPC分类号： C07D487/04 , A61K31/194 , A61K31/403 , A61K31/407 , A61K31/4439 , C07D209/56 , Y10S977/734 , Y10S977/738 , Y10S977/74
摘要： An anti-hepatitis C virus agent or anti-HIV agent comprising, as an active ingredient, a fullerene derivative which has a nitrogen atom forming a ring together with adjacent bonded carbon atom pairs constituting the carbon cluster skeleton of the fullerene or a quaternary amine salt thereof is provided.
摘要翻译：一种抗丙型肝炎病毒剂或抗HIV剂，其特征在于，作为活性成分，具有形成环的氮原子的富勒烯衍生物与构成所述富勒烯的碳簇骨架的相邻键合碳原子对或季胺盐提供。

6. 发明申请

US20060205589A1 Method for producing a palladium-containing hydrogenation catalyst 失效
标题翻译：含钯氢化催化剂的制造方法
公开(公告)号：US20060205589A1
公开(公告)日：2006-09-14
申请号：US10564019
申请日：2004-07-06
申请人： Valery Ukainlsev , Anatolievich Khokhryakov , Nikolai Zakharovich , Georgy Andreevich , Gregory Dyuzhev , Vladimir Kofiev
发明人： Valery Ukainlsev , Anatolievich Khokhryakov , Nikolai Zakharovich , Georgy Andreevich , Gregory Dyuzhev , Vladimir Kofiev
IPC分类号： B01J21/18
CPC分类号： B82Y30/00 , B01J21/18 , B01J23/44 , B01J37/031 , B01J37/16 , Y10S423/39 , Y10S423/40 , Y10S977/734 , Y10S977/735 , Y10S977/74 , Y10S977/742 , Y10S977/748
摘要： The invention relates to physical chemistry and can be used for adjusting the rate of autocatalytic hydrogenation reactions. The method for producing a palladium-containing hydrogenation catalyst consists in reducing divalent palladium from the initial compound thereof and precipitating the thus reduced palladium on a carbon material, wherein, according to said invention, the initial compound is embodied in the form of tetra aqua-palladium (II) perchlorate. The reduced palladium is precipitated on a nano-carbon material which can be embodied in the form of fullerene C60, carbon nanotubes, cathodic deposit and the mixture of C60 and C70 fullerenes at the following ratio thereof: 60-80 mass % fullerene C60 and 20-40 mass % fluorine C70. The invention makes it possible to develop the method for producing a palladium-containing hydrogenation catalyst which exhibits a higher catalytic activity and operates in softer conditions (at a room temperature and a normal (atmospheric) pressure).
摘要翻译：本发明涉及物理化学，可用于调节自催化氢化反应的速率。含钯氢化催化剂的制备方法在于从其初始化合物中还原二价钯，并将如此还原的钯沉淀在碳材料上，其中根据本发明，初始化合物以四水合物形式体现，高氯酸钯（II）。还原的钯在纳米碳材料上沉淀，纳米碳材料可以以富勒烯C 60，碳纳米管，阴极沉积物和C 60 C和C的混合物的形式体现 70％富勒烯按以下比例：60-80质量％富勒烯C 60和20-40质量％氟C 70 70。本发明使得可以开发出具有较高催化活性并在较软条件（室温和正常（大气压））下操作的含钯氢化催化剂的方法。

7. 发明申请

US20030013861A1 E-isomeric fullerene derivatives 失效
标题翻译： E-异构富勒烯衍生物
公开(公告)号：US20030013861A1
公开(公告)日：2003-01-16
申请号：US10202567
申请日：2002-07-24
发明人： Long Y. Chiang , Vijayaraj Anantharaj
IPC分类号： C07D209/96 , C07F009/02
CPC分类号： C07D209/56 , C07C2604/00 , Y10S977/74 , Y10S977/775 , Y10S977/915 , Y10S977/926 , Y10S977/95 , Y10S977/954
摘要： An E-isomeric fulleropyrrolidine compound of formula (I): 1 is disclosed. Also disclosed is a method for preparing and polymers prepared from such a compound.
摘要翻译：公开了式（I）的E-异构的富勒烯吡咯烷化合物：还公开了一种制备由这种化合物制备的聚合物的方法。

8. 发明申请

US20030009036A1 E-isomeric fullerene derivatives 有权
公开(公告)号：US20030009036A1
公开(公告)日：2003-01-09
申请号：US10201798
申请日：2002-07-24
发明人： Long Y. Chiang , Vijayaraj Anantharaj
IPC分类号： C07D29/54 , C07F007/02 , C07F009/547
CPC分类号： C07D209/56 , C07C2604/00 , Y10S977/74 , Y10S977/775 , Y10S977/915 , Y10S977/926 , Y10S977/95 , Y10S977/954
摘要： An E-isomeric fulleropyrrolidine compound of formula (I): 1 is disclosed. Also disclosed is a method for preparing and polymers prepared from such a compound.

9. 发明授权

US5763719A Thermally stable fullerene derivatives and process for producing the same 失效
标题翻译：热稳定的富勒烯衍生物及其制备方法
公开(公告)号：US5763719A
公开(公告)日：1998-06-09
申请号：US492021
申请日：1995-09-15
申请人： Andreas Gugel , Pavel Belik , Klaus Mullen
发明人： Andreas Gugel , Pavel Belik , Klaus Mullen
IPC分类号： C07C13/32 , C07C13/62 , C07C13/64 , C07C13/70 , C07C23/46 , C07C25/22 , C07C43/21 , C07C43/215 , C07C69/00 , C07C69/12 , C07C69/157 , C07C69/22 , C07C69/63 , C07C69/78 , C07C69/96 , C07C205/45 , C07C205/58 , C07C225/22 , C07D213/55 , C07D213/79 , C07C5/22
CPC分类号： C07D213/79 , C07C13/32 , C07C13/70 , C07C205/58 , C07C225/22 , C07C43/215 , C07C69/00 , C07C2103/00 , C07C2104/00 , Y10S977/737 , Y10S977/738 , Y10S977/74 , Y10S977/833 , Y10S977/84
摘要： A fullerene derivative of the formula I ##STR1## where the symbols and indices have the following meanings: F is a fullerene radical of the formula (C.sub.20+2m), where m is a number from 1 to 50 R.sup.1 to R.sup.8 are identical or different and are each H, CO.sub.2 R.sup.9, CN, COR.sup.10, Cl, Br, I, F, OR.sup.11, C.sub.1 -C.sub.20 -alkyl, phenyl or H, R.sup.1 -R.sup.4 and/or R.sup.5, R.sup.7 can also be part of a cycloalipathic, cycloaromatic or cycloheteroaromatic system which in turn is substituted by C.sub.1 -C.sub.20 -alkyl, aryl, carboxyl, carbonyl, alkoxy, aryloxy, halogen, nitro, alcohol or amine, or R.sup.1 and R.sup.2, R.sup.2 and R.sup.3, R.sup.3 and R.sup.4 can together be ##STR2## where R.sup.15 -R.sup.18 are each H, C.sub.1 -C.sub.20 -alkyl, F, Cl, Br, I or phenyl, and AR is the radical of a fused cyclo-aromatic system, and n is from 1 to 20 and a process for its preparation.
摘要翻译： PCT No.PCT / EP93 / 03658 371 1995年9月15日第 102（e）日期1995年9月15日PCT 1993年12月22日PCT公布。出版物WO94 / 17018 日期1994年8月4日具有式I的富勒烯衍生物其中符号和指数具有以下含义：+ E，crc F + EE是式（C20 + 2m）的富勒烯基，其中m是数 1至50个R 1至R 8相同或不同，各自为H，CO 2 R 9，CN，COR 10，Cl，Br，I，F，OR 11，C 1 -C 20烷基，苯基或H，R 1 -R 4和/或R 5， R7也可以是环脂族，环芳族或环杂芳族体系的一部分，其又被C 1 -C 20烷基，芳基，羧基，羰基，烷氧基，芳氧基，卤素，硝基，醇或胺取代，或者R 1和R 2，R 2和 R 3，R 3和R 4可以一起为，其中R 15 -R 18各自为H，C 1 -C 20 - 烷基，F，Cl，Br，I或苯基，+ E，crc AR + EE为稠环 - 芳族体系，n为1〜20，其制备方法为。

10. 发明授权

US09079837B2 Water-soluble fluorescent fullerene derivative, and preparation method thereof 有权
标题翻译：水溶性荧光富勒烯衍生物及其制备方法
公开(公告)号：US09079837B2
公开(公告)日：2015-07-14
申请号：US13643292
申请日：2011-04-25
申请人： Bong Hyun Chung , Jin Young Jeong
发明人： Bong Hyun Chung , Jin Young Jeong
IPC分类号： C07C41/06 , C09K11/06 , B82Y30/00
CPC分类号： C07C41/06 , B82Y30/00 , C07C2604/00 , C09K11/06 , C09K2211/1011 , Y10S977/74 , Y10S977/847 , C07C43/196
摘要： A simple and easy method is described for preparing a water-soluble fluorescent fullerene derivative with strong fluorescence and hydrophilicity, by mixing fullerene and a ligand containing a terminal hydroxyl group in a first solvent and reacting the mixture in the presence of a catalyst. Such preparation method enables the intensity and wavelength of fluorescence to be easily controlled depending on the amount of fullerene and the type of catalyst that are utilized. The prepared fluorescent fullerene derivative contains a biocompatible ligand, and thus is useful as a biological fluorescent dye. As a result of its fluorescence and excellent solubility in solvent, the fluorescent fullerene derivative is useful in biological, medical, nanotechnology, and other fields.
摘要翻译：通过将富勒烯和含有末端羟基的配位体在第一溶剂中混合并在催化剂存在下反应来描述制备具有强荧光和亲水性的水溶性荧光富勒烯衍生物的简便方法。这样的制备方法能够根据富勒烯的量和使用的催化剂的种类容易地控制荧光的强度和波长。制备的荧光富勒烯衍生物含有生物相容性配体，因此可用作生物荧光染料。荧光富勒烯衍生物由于其荧光和在溶剂中的溶解性优异，可用于生物，医学，纳米技术等领域。

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