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1. 发明授权

US11046637B2 Process for the manufacture of 1,1,1-trifluoro-2-chloroethaneand/or trifluoroethylamine 有权
公开(公告)号：US11046637B2
公开(公告)日：2021-06-29
申请号：US16517547
申请日：2019-07-20
申请人： Fujian Yongjing Technology Co., Ltd.
发明人： Hongjun Du , Wenting Wu
IPC分类号： C07C209/08 , C07C211/15 , B01J27/06
摘要： The invention relates to a new process for the manufacture of fluoroaryl compounds and derivatives thereof, in particular of fluorobenzenes and derivatives thereof, and especially wherein said manufacture relates to an environmentally friendly production of the said compounds. Thus, the present invention overcomes the disadvantages of the prior art processes, and in a surprisingly simple and beneficial manner, and as compared to the prior art processes, in particular, the invention provides a more efficient and energy saving processes, and also provides a more environmentally friendly process, for the manufacture of nuclear fluorinated aromatics, and preferably of nuclear fluorinated fluorobenzenes. Accordingly, in one aspect of the invention, an industrially beneficial process for preparing fluorobenzenes from halobenzene precursors using HF to form hydrogen halide is provided by the present invention. A beneficial and surprisingly simple use of chlorobenzene as an industrially interesting starting material in the manufacture of fluorobenzene is provided.

2. 发明申请

US20190300473A1 COMPOSITION COMPRISING 1-CHLORO-2,2-DIFLUOROETHANE 审中-公开
公开(公告)号：US20190300473A1
公开(公告)日：2019-10-03
申请号：US16336305
申请日：2017-09-25
申请人： Arkema France
发明人： Dominique GARRAIT , Charlotte HERDT , Camille SCHERPEREEL
IPC分类号： C07C211/15 , C07C19/12 , C07C21/18
摘要： Compositions including 1-chloro-2,2-difluoroethane, and the uses thereof. A composition including 1-chloro-2,2-difluoroethane and at least one additional compound selected from 1,1-difluoroethylene, 1,1,1-trifluoroethane, chlorotrifluoroethylene, 1-chloro-1-fluoroethylene, 1,1-difluoroethane, trans-1-chloro-2-fluoroethylene, 1-chloro-2,2,2-trifluoroethane, 1-chloro-1,2,2-trifluoroethane, cis-1-chloro-2-fluoroethylene, 2,2-dichloro-1,1,1-trifluoroethane, 1,1-dichloro-1-fluoroethane, 1,1-dichloroethylene, 1,2-dichloro-1-fluoroethylene, 1,1-dichloro-2-fluoroethylene, 1,2-dichloro-1,1-difluoroethane, 1,1-dichloro-2,2-difluoroethane, cis-1,2-dichloroethylene, 1,2,2-trichloro-1,1-difluoroethane, 1,1,1-trichloroethane, 1,1-dichloroethane, 1,1,2-trichloro-1-fluoroethane, trichloroethylene, 1,1,2-trichloro-2-fluoroethane, 1,1,2-trichloroethane, 1,1,2,2-tetrachloro-1-fluoroethane, tetrachloroethylene, 1,1,1,2-tetrachloroethane, 1,1,2,2-tetrachloroethane, 1,1,1,2,2-pentachloroethane, tetrachloromethane, 1,2,2-trichloro-1-fluoroethylene, isomers of chloropropene, 1,2-dichloro-1-fluoroethylene, 1-chloro-2-fluoroethane, 1-chloro-1-fluoroethane, 1,1-chloro-2,2,2-trifluoroethane, 1,1,1-trichloro-2,2-difluoroethane, 1-chloroethylene, 1-fluoroethylene, H2O and HCl; the composition including at least 30% by weight of 1-chloro-2,2-difluoroethane, based on the total weight of the composition.

3. 发明授权

US10100000B2 Method for synthesizing 1,1-diamino-2,2-dinitroethylene (FOX-7) or a salt thereof 有权
公开(公告)号：US10100000B2
公开(公告)日：2018-10-16
申请号：US15636934
申请日：2017-06-29
申请人： DIEHL DEFENCE GMBH & CO. KG
发明人： Oliver Pham-Schoenwetter , Bjoern Donner , Arno Hahma
IPC分类号： C07C209/68 , C07C211/09 , C07C211/15 , C07C267/00 , C07C209/60 , C07C211/24
摘要： In a method for synthesizing 1,1-diamino-2,2-dinitroethylene (FOX-7) or an N-substituted diamino derivative thereof or a salt of 1,1-diamino-2,2-dinitroethylene or of the N-substituted diamino derivative, a carbodiimide is reacted with a dinitromethane anion. The reaction of the carbodiimide with the dinitromethane anion takes place in a solution.

4. 发明申请

US20170283365A1 NITROGEN CONTAINING HYDROFLUOROETHERS AND METHODS OF USING SAME 审中-公开
公开(公告)号：US20170283365A1
公开(公告)日：2017-10-05
申请号：US15511259
申请日：2015-09-18
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： William M. Lamanna , Michael J. Bulinski , Kiah A. Smith , Michael G. Costello , Georgiy Teverovskiy
IPC分类号： C07C217/26 , C07C211/15 , C07D241/04 , C09K5/04 , C09K5/10 , C09K3/00 , C10M107/38 , C09D7/00 , A62D1/00 , C11D3/43 , C08J9/00 , H01M10/0525 , H01M10/0569 , H01L23/46 , C07D265/30
CPC分类号： C07C217/26 , A62D1/0028 , C07C211/15 , C07D207/10 , C07D211/38 , C07D223/04 , C07D241/04 , C07D265/30 , C08J9/0028 , C08J9/14 , C08J2323/04 , C08J2325/04 , C08J2327/06 , C08J2371/10 , C08J2375/04 , C09D7/20 , C09K3/00 , C09K5/048 , C09K5/10 , C10M107/38 , C10M2213/0606 , C11D3/43 , H01B3/24 , H01B3/56 , H01L23/46 , H01M10/0525 , H01M10/0569 , H01M2300/0034
摘要： A hydrofluoroether compound is represented by the following general formula (1): wherein n is 1-2.

5. 发明申请

US20140094495A1 Antimicrobial Haloalkyl Heterocycle Compounds 失效
标题翻译：抗菌卤烷基杂环化合物
公开(公告)号：US20140094495A1
公开(公告)日：2014-04-03
申请号：US13676922
申请日：2012-11-14
申请人： NovaBay Pharmaceuticals, Inc.
发明人： Timothy K. Shiau , Charles Francavilla , Eddy Low , Eric Douglas Turtle , Donogh John Roger O'Mahony , Rakesh K. Jain
IPC分类号： C07D263/22 , C07D233/20 , A01N43/50 , A01N37/18 , A01N43/36 , C07C211/15 , A01N37/44 , C07C313/06 , A01N43/76 , C07D207/46
CPC分类号： C07D263/22 , A01N37/18 , A01N37/44 , A01N43/36 , A01N43/50 , A01N43/76 , A01N59/00 , C07C211/15 , C07C313/06 , C07D207/46 , C07D233/20 , C07D263/26
摘要： This application describes compounds useful as anti-microbial agents, including as antibacterial, disinfectant, antifungal, germicidal or antiviral agents.
摘要翻译：本申请描述了可用作抗微生物剂的化合物，包括作为抗细菌剂，消毒剂，抗真菌剂，杀菌剂或抗病毒剂。

6. 发明申请

US20130123513A1 Adhesive Compositions for Bonding Composites 有权
标题翻译：粘合复合材料的粘合剂组合物
公开(公告)号：US20130123513A1
公开(公告)日：2013-05-16
申请号：US13627335
申请日：2012-09-26
申请人： Georgia-Pacific Chemicals LLC
发明人： Bobby Lee Williamson , Richard M. Rammon
IPC分类号： C07C213/04 , C07D205/04 , C07C209/00 , C07C211/15 , C07C215/08 , C07C213/00 , C07D303/02 , C07D301/00
CPC分类号： C07C213/04 , C07C209/00 , C07C211/15 , C07C213/00 , C07C215/08 , C07D205/04 , C07D301/00 , C07D303/02 , C08L61/06 , C08L61/24 , C08L61/28 , C08L77/00 , C08L79/02 , C08L2205/02 , C08L2666/02 , C08L2666/16 , C08L2666/20 , C09J179/02
摘要： The present invention relates to a non-thermosetting composition made by reacting epichlorohydrin and a primary amine, to the use of that composition for making thermosetting (curable) adhesives suitable for bonding composites, to a method of preparing composites using the thermosetting (curable) adhesives, and to the related composites bonded with the thermosetting (curable) adhesives.
摘要翻译：本发明涉及通过使表氯醇和伯胺反应制备的非热固性组合物，以使用该组合物制备适用于粘合复合材料的热固性（可固化）粘合剂，使用该热固性（可固化）粘合剂制备复合材料的方法以及与热固性（可固化）粘合剂结合的相关复合材料。

7. 发明申请

US20110275805A1 METHOD FOR PREPARING LINEZOLID AND INTERMEDIATES THEREOF 有权
标题翻译：制备线粒体的方法及其中间体
公开(公告)号：US20110275805A1
公开(公告)日：2011-11-10
申请号：US13144242
申请日：2010-01-08
申请人： Ping Wang , Qiangbiao Pan , Yangzhou Li , Daoliang Zheng
发明人： Ping Wang , Qiangbiao Pan , Yangzhou Li , Daoliang Zheng
IPC分类号： C07D413/10 , C07C211/15
CPC分类号： C07D263/20
摘要： A method for preparing the linezolid (compound 1), which comprises the steps of: (1) carrying out the debenzyl reaction of compound 4 in solvent, to obtain the compound 5 or its acetate; (2) carrying out the acetylation reaction in the amino of the compound 5 or its acetate obtained in step (1) in solvent to obtain the compound 1. The intermediates to prepare the compound 1 and the acetate of compound 5. The present preparation method is easy to obtain the chiral materials and the chiral materials are cheap, the process and the post treatment are simple, the intermediate products and the end product are easy to be purified, the total yield is high, their purities are also high, this preparation method is easy to be used in the industry manufacture.
摘要翻译：一种制备利奈唑胺（化合物1）的方法，包括以下步骤：（1）在溶剂中进行化合物4的脱苄基反应，得到化合物5或其乙酸酯; （2）在溶剂中在步骤（1）中得到的化合物5或其乙酸的氨基进行乙酰化反应，得到化合物1.制备化合物1和化合物5的乙酸酯的中间体。本制备方法手性材料易于获得，手性材料便宜，工艺和后处理简单，中间产品和最终产品易于纯化，总产率高，纯度高，该制剂方法易于在工业制造中使用。

8. 发明申请

US20080319228A1 Method of fluorination 失效
标题翻译：氟化方法
公开(公告)号：US20080319228A1
公开(公告)日：2008-12-25
申请号：US12068481
申请日：2008-02-07
申请人： Shoji Hara , Tsuyoshi Fukuhara
发明人： Shoji Hara , Tsuyoshi Fukuhara
IPC分类号： C07C211/15
CPC分类号： C07D239/30 , C07B39/00 , C07B2200/09 , C07C17/093 , C07C17/16 , C07C17/18 , C07C29/64 , C07C51/60 , C07C67/307 , C07C2601/14 , C07C2601/16 , C07C2601/18 , C07C2601/20 , C07C2603/74 , C07H1/00 , C07H9/04 , C07H13/04 , C07H13/08 , C07H19/06 , C07C22/08 , C07C21/18 , C07C19/08 , C07C23/38 , C07C23/02 , C07C23/10 , C07C63/10 , C07C69/63 , C07C35/52 , C07C35/48
摘要： A method of fluorination comprising reacting monosaccharides, oligosaccharides, polysaccharides, composite saccharides formed by bonding of these saccharides with proteins and lipids and saccharides having polyalcohols, aldehydes, ketones and acids of the polyalcohols, and derivatives and condensates of these compounds with a fluorinating agent represented by general formula (I) thermally or under irradiation with microwave or an electromagnetic wave having a wavelength around the microwave region. In accordance with the method, the fluorination at a selected position can be conducted safely at a temperature in the range of 150 to 200° C. where the reaction is difficult in accordance with conventional methods. The above method comprising the irradiation with microwave or an electromagnetic wave having a wavelength around the microwave region can be applied to substrates other than saccharides. When a complex compound comprising HF and a base is reacted under irradiation with microwave, fluorination at a specific position which is difficult in accordance with conventional methods proceeds highly selectively, efficiently in a short time and safely.
摘要翻译：一种氟化方法，包括使单糖，寡糖，多糖，这些糖与蛋白质和脂质结合形成的复合糖和多元醇的多元醇，醛，酮和酸的糖，以及这些化合物的衍生物和缩合物与氟化剂的代表性反应通过通式（I）热或照射微波或具有波长在微波区域周围的波长的电磁波。根据该方法，可以根据常规方法在150〜200℃的范围内的温度下安全地进行选择位置的氟化。包含微波照射或微波周围波长的电磁波的上述方法可以应用于除糖以外的基材。当包含HF和碱的络合物在微波照射下反应时，根据常规方法困难的特定位置的氟化在高速选择性地进行，在短时间内和安全地进行。

9. 发明授权

US5716549A Fluoroiodocarbon blends as CFC and halon replacements 失效
公开(公告)号：US5716549A
公开(公告)日：1998-02-10
申请号：US701669
申请日：1996-08-22
申请人： Jonathan Shelley Nimitz , Lance Harrell Lankford
发明人： Jonathan Shelley Nimitz , Lance Harrell Lankford
IPC分类号： A62D1/00 , A62D1/08 , C07C19/16 , C07C43/12 , C07C211/15 , C08J9/14 , C09K3/00 , C09K3/30 , C09K5/04 , C11D7/30 , C11D7/32 , C11D7/50 , C23G5/028 , C09K5/00
CPC分类号： C08J9/149 , A62D1/0057 , C09K3/30 , C09K5/044 , C09K5/045 , C08J2203/12 , C08J2203/14 , C08J2203/142 , C08J2203/146 , C08J2207/04 , C09K2205/11 , C09K2205/112 , C09K2205/12 , C09K2205/122 , C09K2205/128 , C09K2205/32 , Y10S264/05 , Y10S422/90 , Y10S521/909 , Y10S521/91
摘要： A new set of effective, environmentally safe, nonflammable, low-toxicity refrigerants, solvents, foam blowing agents, propellants, and firefighting agents is disclosed. The agents are clean, electrically nonconductive, and have short atmospheric lifetimes, zero ozone-depletion potential, and low global warming potentials. The agents comprise at least one fluoroiodocarbon agent satisfying the general formula C.sub.a H.sub.b Br.sub.c Cl.sub.d F.sub.e I.sub.f N.sub.g O.sub.h, wherein a is between and including 1 and 8; b is between and including 0 and 2; c, d, g, and h are each between and including 0 and 1; e is between and including 1 and 18; and f is between and including 1 and 2, either neat or mixed with additives selected from the group consisting of: alcohols, esters, ethers, fluoroethers, hydrocarbons, hydrofluorocarbons, and perfluorocarbons.

10. 发明授权

US5695688A Fluoroiodocarbon blends as CFC and halon replacements 失效
公开(公告)号：US5695688A
公开(公告)日：1997-12-09
申请号：US707960
申请日：1996-09-10
申请人： Jonathan Shelly Nimitz , Lance Harrell Lankford
发明人： Jonathan Shelly Nimitz , Lance Harrell Lankford
IPC分类号： A62D1/00 , A62D1/08 , C07C19/16 , C07C43/12 , C07C211/15 , C08J9/14 , C09K3/00 , C09K3/30 , C09K5/04 , C11D7/30 , C11D7/32 , C11D7/50
CPC分类号： C08J9/149 , A62D1/0057 , C09K3/30 , C09K5/044 , C09K5/045 , C08J2203/12 , C08J2203/14 , C08J2203/142 , C08J2203/146 , C08J2207/04 , C09K2205/11 , C09K2205/112 , C09K2205/12 , C09K2205/122 , C09K2205/128 , C09K2205/32 , Y10S264/05 , Y10S422/90 , Y10S521/909 , Y10S521/91
摘要： A new set of effective, environmentally safe, nonflammable, low-toxicity refrigerants, solvents, foam blowing agents, propellants, and firefighting agents is disclosed. The agents are clean, electrically nonconductive, and have short atmospheric lifetimes, zero ozone-depletion potential, and low global warming potentials. The agents comprise at least one fluoroiodocarbon agent satisfying the general formula C.sub.a H.sub.b Br.sub.c Cl.sub.d F.sub.e I.sub.f N.sub.g O.sub.h, wherein a is between and including 1 and 8; b is between and including 0 and 2; c, d, g, and h are each between and including 0 and 1; e is between and including 1 and 18; and f is between and including 1 and 2, either neat or mixed with additives selected from the group consisting of: alcohols, esters, ethers, fluoroethers, hydrocarbons, hydrofluorocarbons, and perfluorocarbons.

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