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1. 发明授权

US10336670B2 Method for producing high-octane components from olefins from catalytic cracking 有权
公开(公告)号：US10336670B2
公开(公告)日：2019-07-02
申请号：US16061080
申请日：2016-11-29
申请人： AKTSIONERNOE OBSCHESTVO “GAZPROMNEFT—MOSKOVSKY NPZ” (AO “GAZPROMNEFT-MNPZ”)
发明人： Aleksandr Sergeevich Haritonov , Konstantin Aleksandrovich Dubkov , Mihail Vladimirovich Parfenov , Aleskandr Stepanovich Noskov , Valery Aleksandrovich Golovachev , Andrei Vladimirovich Kleimenov , Dmitry Olegovich Kondrashev , Valentina Dmitrievna Miroshkina , Dmitrii Petrovich Ivanov , Sergey Vladimirovich Semikolenov , Valery Sergeevich Chernyavsky , Larisa Vladimirovna Piryutko , Kristina Andreevna Rusetskaya , Sergey Evgenyevich Kuznetsov
IPC分类号： C07C45/28 , C07C1/22 , C07C27/16 , C07C29/136 , C07C45/73 , C10L1/185 , C10L1/16 , C10L1/182 , C10L10/10 , C07C29/141 , C07C29/145 , C07C45/45 , B01J21/04 , B01J21/06 , B01J21/08 , B01J23/42 , B01J23/44 , B01J23/52 , B01J23/72 , B01J23/75 , B01J23/755 , B01J29/035 , B01J29/06
摘要： The invention relates to the field of petrochemistry, and specifically to a method for synthesizing high-octane oxygen containing components of motor fuel. The objects of the invention consist in variants of a method for synthesizing high-octane oxygen-containing components of motor fuel from olefin-containing gas mixtures via oxidative non-catalytic conversions using nitrous oxide, and the subsequent condensation and hydrogenation of the produced oxygenates using heterogeneous catalysts. The high-octane components according to the proposed method consist in a mixture of carbonyl compounds (ketones, aldehydes, hydroxy ketones, hydroxy aldehydes) C2-C9 and/or branched hydrocarbons C5-C9 and/or alcohols in different ratios. Depending on the production method variant, the octane number of a mixture of the proposed high-octane components consists in a value between 100 and 130 RON. The technical result consists in broadening the resource base for the production of high-octane gasolines and of a variety of environmentally-friendly high-octane additives.

2. 发明授权

US09975114B2 Metal organic frameworks as catalysts and hydrocarbon oxidation methods thereof 有权
公开(公告)号：US09975114B2
公开(公告)日：2018-05-22
申请号：US15458437
申请日：2017-03-14
申请人： KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
发明人： Abiola Azeez Jimoh , Abdul Malik Peedikakkal
IPC分类号： C07F5/00 , B01J31/12 , B01J35/10 , C07C45/29 , C07C27/16 , C07C51/285 , C07F15/02 , C07F3/06 , C07F1/08
CPC分类号： B01J31/123 , B01J35/002 , B01J35/1023 , B01J35/1028 , B01J35/1057 , B01J35/1061 , C07C27/16 , C07C29/48 , C07C45/28 , C07C45/294 , C07C51/285 , C07C2101/14 , C07C2601/14 , C07F1/08 , C07F3/06 , C07F15/025 , C07C35/08 , C07C49/403 , C07C47/54 , C07C63/06
摘要： A metal organic framework comprising zinc (II) ions and second metal ions, such as iron (II) ions, cobalt (II) ions, and copper (II) ions as nodes or clusters and coordinated 1,3,5-benzenetricarboxylic acid struts or linkers between them forming a porous coordination network in the form of polyhedral crystals that are isostructural to HKUST-1. Transmetallation processes for producing the metal organic frameworks, as well as methods for applications of the metal organic frameworks as catalysts, specifically catalysts for the oxidation of cyclic hydrocarbons, such as toluene, cyclohexane, and methylcyclohexane.

3. 发明授权

US08242300B2 Process for selective, partial, substantially solvent-free, oxidation of methane to methanol and/or a methanol derivative with a heterogeneous catalyst and sulfur trioxide 有权
标题翻译：使用多相催化剂和三氧化硫将甲烷选择性，部分，基本上无溶剂氧化成甲醇和/或甲醇衍生物的方法
公开(公告)号：US08242300B2
公开(公告)日：2012-08-14
申请号：US12670431
申请日：2008-07-01
申请人： Michael A. Gonzalez , Daniel R. Henton , David C. Molzahn
发明人： Michael A. Gonzalez , Daniel R. Henton , David C. Molzahn
IPC分类号： C07C27/16 , C07C303/06 , B01J21/06 , B01J27/12 , B01J39/04
CPC分类号： C07C29/48 , Y02P20/52 , C07C31/04
摘要： The present invention relates to selective partial oxidation of methane in the absence of a solvent such as sulfuric acid or oleum.
摘要翻译：本发明涉及在不存在溶剂如硫酸或发烟硫酸的情况下甲烷的选择性部分氧化。

4. 发明授权

US08227647B2 Method of producing alcohols 有权
标题翻译：醇的生产方法
公开(公告)号：US08227647B2
公开(公告)日：2012-07-24
申请号：US12927936
申请日：2010-11-30
申请人： Jorge Miller , Luisa Kling Miller
发明人： Jorge Miller , Luisa Kling Miller
IPC分类号： C07C29/48 , C07C27/16
CPC分类号： C07C29/095 , C07C17/10 , C07C67/11 , C07C19/075 , C07C31/04 , C07C69/06
摘要： A method comprising reacting an alkane gas with a halogen gas in a halogenations reactor to form a halogenation reaction product mixture comprising alkane halide and hydrogen halide mixture; mixing the halogenations reaction product mixture with a countercurrent flow of a metal organic salt thereby forming an extractor product mixture of a metal halide, organic salt, and organic acid separating the organic ester and organic acid mixture from the metal halide; oxygenating the metal halide to form a metal oxide and halide containing gasses; separating the metal oxide from the halide containing gasses; mixing the metal oxide with water to form a metal oxide slurry; mixing the metal oxide slurry with a countercurrent flow of the organic ester and organic acid mixture to form a raw product comprising alkanol, a metal organic salt is provided.
摘要翻译：一种方法，包括在卤化反应器中使烷烃气体与卤素气体反应以形成卤化反应产物混合物，其包含烷烃卤化物和卤化氢混合物; 将卤化反应产物混合物与金属有机盐的逆流混合，从而形成金属卤化物，有机盐和有机酸的萃取产物混合物，从有机酯和有机酸混合物中分离出金属卤化物; 使金属卤化物氧化以形成金属氧化物和含卤气的气体; 从含卤化物气体中分离金属氧化物; 将金属氧化物与水混合以形成金属氧化物浆料; 将金属氧化物浆料与有机酯和有机酸混合物的逆流混合以形成包含链烷醇，金属有机盐的粗产物。

5. 发明申请

US20090105356A1 PROCESS AND PLANT FOR PRODUCING SYNTHESIS GAS 有权
标题翻译：生产合成气的工艺和设备
公开(公告)号：US20090105356A1
公开(公告)日：2009-04-23
申请号：US12300683
申请日：2007-05-10
申请人： Andreas Bormann , Dierk Muller
发明人： Andreas Bormann , Dierk Muller
IPC分类号： C07C27/16 , C10J3/48
CPC分类号： C01B3/382 , C01B2203/0233 , C01B2203/0244 , C01B2203/061 , C01B2203/068 , C01B2203/1241 , C01B2203/127 , C01B2203/141 , C01B2203/143
摘要： When producing synthesis gas from a starting material containing hydrocarbons, in particular natural gas, a feed stream of the starting material is divided into a first partial stream and a second partial stream. The first partial stream is supplied to a steam reformer (4), in which together with steam it is catalytically converted to a gas stream containing carbon oxides. Then, the first partial stream is again combined with the second partial stream and the combined gas stream is supplied to an autothermal reformer (7), in which together with gas rich in oxygen it is autothermally reformed to a synthesis gas in the presence of a cracking catalyst. Processing a starting material with a high content of higher hydrocarbons is made possible in that before the steam reformer (4) and before the autothermal reformer (7) the entire starting material is supplied to a pre-reformer (2) in which the starting material largely is liberated from higher hydrocarbons.
摘要翻译：当从含有烃，特别是天然气的原料生产合成气时，原料的进料流被分成第一部分流和第二部分流。将第一部分流供应到蒸汽重整器（4），其中蒸汽与蒸汽一起被催化转化成含有碳氧化物的气流。然后，将第一部分流再次与第二部分流合并，将合并的气流供应至自热重整器（7），其中与富含氧气的气体一起，在有气体的情况下自动重整成合成气裂化催化剂。加工具有高含量高烃的原料是可能的，因为在蒸汽重整器（4）之前和自热重整器（7）之前，将整个起始原料供应到预重整器（2），其中原料主要是从高级碳氢化合物中释放出来的。

6. 发明授权

US5705705A Oxidation of alkylaromatic compounds 失效
标题翻译：烷基芳族化合物的氧化
公开(公告)号：US5705705A
公开(公告)日：1998-01-06
申请号：US619507
申请日：1996-03-26
申请人： Scott William Brown , Kevin Auty
发明人： Scott William Brown , Kevin Auty
IPC分类号： C07B41/00 , C07C27/16 , C07C29/48 , C07C33/20 , C07C45/28 , C07C67/00 , C07C45/27
CPC分类号： C07C45/28 , C07B41/00 , C07C27/16 , C07C29/48 , C07C33/20 , C07C67/00
摘要： A process for the oxidation of alkylaromatic compounds is provided. The process comprises oxidizing a substrate alkylaromatic compound with a peroxygen compound in the presence of a source of cerium (III) or (IV), a source of bromide and a carboxylic acid or anhydride solvent. Preferably, the source of cerium is cerium (III) acetate, the source of bromide is sodium bromide and the solvent is acetic or propionic acid. The process is particularly suited to the selective oxidation of methylaromatic compounds to the corresponding aldehydes.
摘要翻译： PCT No.PCT / GB94 / 02080 Sec。 371日期：1996年3月26日 102（e）1996年3月26日PCT 1994年9月26日PCT公布。公开号WO95 / 09139 日期1995年4月6日提供了烷基芳族化合物的氧化方法。该方法包括在铈（III）或（IV）源，溴化物源和羧酸或酸酐溶剂的存在下用过氧化合物氧化底物烷基芳族化合物。优选地，铈源是乙酸铈（III），溴化物源是溴化钠，溶剂是乙酸或丙酸。该方法特别适用于将甲基芳族化合物选择性氧化成相应的醛。

7. 发明授权

US4647707A Hydroformylation of olefins 失效
标题翻译：烯烃的加氢甲酰化
公开(公告)号：US4647707A
公开(公告)日：1987-03-03
申请号：US803090
申请日：1985-11-27
申请人： Arie van Vliet
发明人： Arie van Vliet
IPC分类号： C07C27/20 , B01J23/00 , B01J23/74 , C07B61/00 , C07C27/00 , C07C27/16 , C07C29/14 , C07C29/156 , C07C29/16 , C07C31/125 , C07C45/27 , C07C45/50 , C07C67/00
CPC分类号： C07C45/50 , C07C29/16
摘要： The higher alcohol yield of a hydroformylation process including hydroformylation, catalyst removal, hydrogenation and higher alcohol separation stages is improved by subjecting the Heavy Oxo Fraction (HOF) obtained following higher alcohol separation to steam cracking in the presence of a catalyst system comprising a dehydration-catalytic metal on an acidic support. The resultant cracked HOF mixture comprising a major proportion of olefin and saturated hydrocarbon is recycled to the hydroformylation stage.
摘要翻译：通过使含有高级醇分离得到的重质氧化物馏分（HOF）在含有脱水 - 脱水的催化剂体系的存在下进行蒸汽裂化，改进了加氢甲酰化方法（包括加氢甲酰化，催化剂除去，氢化和高级醇分离）催化金属在酸性载体上。将包含主要比例的烯烃和饱和烃的所得裂解HOF混合物再循环至加氢甲酰化阶段。

8. 发明授权

US3946077A Process for oxidating hydrocarbons 失效
标题翻译：氧化烃的方法
公开(公告)号：US3946077A
公开(公告)日：1976-03-23
申请号：US439689
申请日：1974-02-04
申请人： Reinhard Thiel , Heinz Jorg Rosenbaum , Karl Heinz Heller
发明人： Reinhard Thiel , Heinz Jorg Rosenbaum , Karl Heinz Heller
IPC分类号： C07C27/12 , C07C27/00 , C07C29/52 , C07C67/00 , C07C27/16 , C07C29/00 , C07C45/02
CPC分类号： C07C29/52 , C07C2101/14 , C07C2101/20
摘要： Hydrocarbons containing from 4 to 20 carbon atoms are oxidized with a gas containing molecular oxygen in the presence of a catalyst and/or auxiliary agents. The resulting reaction mixture is saponified with an aqueous alkaline solution and the resulting alkaline solution containing organic impurities is subjected to liquid phase oxidation with a gas containing molecular oxygen in at least a stoichiometric quantity sufficient for completely burning the organic ingredients, the oxidation taking place in a reaction zone heated to at least 200.degree.C under a pressure sufficient to keep at least some of the water in the liquid phase. The alkali carbonate/bicarbonate solution formed is recycled to the hydrolysis stage.
摘要翻译：含有4至20个碳原子的烃在催化剂和/或助剂的存在下用含有分子氧的气体氧化。将所得反应混合物用碱性水溶液皂化，并将含有有机杂质的所得碱溶液用至少化学计量的含分子氧的气体进行液相氧化，以使其完全燃烧有机成分，氧化发生在在足以使至少一些水保持液相的压力下加热至至少200℃的反应区。形成的碱金属碳酸盐/碳酸氢盐溶液被循环到水解阶段。

9. 发明授权

US3488395A Oxidation process 失效
公开(公告)号：US3488395A
公开(公告)日：1970-01-06
申请号：US3488395D
申请日：1966-09-28
申请人： ICI LTD
发明人： HOOPER GEORGE WALLACE
IPC分类号： C07C37/60 , C07C45/28 , C07C27/16 , C07C39/00
CPC分类号： C07C37/60 , C07C45/28 , C07C39/04 , C07C39/14 , C07C39/07

10. 发明申请

US20170326536A1 METAL ORGANIC FRAMEWORKS AS CATALYSTS AND HYDROCARBON OXIDATION METHODS THEREOF 有权
公开(公告)号：US20170326536A1
公开(公告)日：2017-11-16
申请号：US15458437
申请日：2017-03-14
申请人： KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
发明人： Abiola Azeez JIMOH , Abdul Malik Peedikakkal
IPC分类号： B01J31/12 , C07F3/06 , C07F1/08 , C07C51/285 , C07C45/29 , C07C27/16 , B01J35/10 , C07F15/02
CPC分类号： B01J31/123 , B01J35/002 , B01J35/1023 , B01J35/1028 , B01J35/1057 , B01J35/1061 , C07C27/16 , C07C29/48 , C07C45/28 , C07C45/294 , C07C51/285 , C07C2101/14 , C07C2601/14 , C07F1/08 , C07F3/06 , C07F15/025 , C07C35/08 , C07C49/403 , C07C47/54 , C07C63/06
摘要： A metal organic framework comprising zinc (II) ions and second metal ions, such as iron (II) ions, cobalt (II) ions, and copper (II) ions as nodes or clusters and coordinated 1,3,5-benzenetricarboxylic acid struts or linkers between them forming a porous coordination network in the form of polyhedral crystals that are isostructural to HKUST-1. Transmetallation processes for producing the metal organic frameworks, as well as methods for applications of the metal organic frameworks as catalysts, specifically catalysts for the oxidation of cyclic hydrocarbons, such as toluene, cyclohexane, and methylcyclohexane.

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