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1. 发明申请

US20210322967A1 EMISSION CONTROL DURING CATALYST REGENERATION 有权
公开(公告)号：US20210322967A1
公开(公告)日：2021-10-21
申请号：US17361357
申请日：2021-06-29
申请人： Monsanto Technology LLC
发明人： Kam-To Wan
IPC分类号： B01J38/02 , B01J21/06 , B01J23/22 , B01J29/076 , B01J29/90 , B01J38/06 , B01J38/50 , C07C37/00 , C07C37/60 , F01N9/00 , B01J38/16 , B01J38/12 , B01J38/14 , B01D53/86 , C07C17/358
摘要： Catalyst regeneration processes that include measures for controlling emissions generated during the regeneration are described. The present invention further relates to catalytic processes for producing various chlorinated aromatic compounds that include provisions for controlling emissions during catalyst regeneration.

2. 发明申请

US20210229085A1 METHOD FOR MANUFACTURING MODIFIED ALUMINOSILICATE, MODIFIED ALUMINOSILICATE, AND METHOD FOR MANUFACTURING AROMATIC DIHYDROXY COMPOUND USING THE SAME 有权
公开(公告)号：US20210229085A1
公开(公告)日：2021-07-29
申请号：US17053603
申请日：2019-05-20
申请人： MITSUI CHEMICALS, INC.
发明人： Yoshiya MATSUKAWA , Nobuhiko HORIUCHI , Akihiro OKABE , Yoshihiro KUBOTA , Satoshi INAGAKI
IPC分类号： B01J37/08 , C01B39/48 , C01B39/06 , B01J29/89 , C07C37/60
摘要： There are provided a method for manufacturing a modified aluminosilicate by which a hydroquinone is highly selectively manufactured by reaction of a phenol with hydrogen peroxide, a modified aluminosilicate, and a method for manufacturing an aromatic dihydroxy compound by using the modified aluminosilicate, under industrially advantageous conditions. The method for manufacturing a modified aluminosilicate of the present invention includes a first step of treating an aluminosilicate with an acid, a second step of primarily calcining the treated material obtained in the first step at 550° C. to 850° C., and a third step of contacting the calcined material obtained in the second step with a liquid. containing one or more elements selected from the group consisting of Group 4 elements and. Group 5 elements on. the periodic table, and then drying and secondarily calcining the resultant. The modified aluminosilicate included in the present invention. includes one or more elements selected from the group consisting of Group 4 elements and Group 5 elements on the periodic table, and exhibits an absorbance at 300 nm (A[300]) in an ultraviolet visible spectrum of 1.0 or higher. The method for manufacturing aromatic dihydroxy compounds of the present invention includes a step of reacting a phenol with hydrogen peroxide in the presence of a specific modified. aluminosilicate.

3. 发明申请

US20190248723A1 CONTINUOUS PROCESS FOR THE OZONOLYSIS OF LIGNIN TO YIELD AROMATIC MONOMERS 审中-公开
公开(公告)号：US20190248723A1
公开(公告)日：2019-08-15
申请号：US16317173
申请日：2017-07-13
申请人： UNIVERSITY OF KANSAS
发明人： Bala SUBRAMANIAM , Andrew M. DANBY , Michael D. LUNDIN
IPC分类号： C07C45/40 , C07C37/60 , C07C45/78 , C07G1/00 , C08H7/00 , C07C37/70
摘要： A method for processing lignin may comprise flowing a lignin composition comprising a lignin polymer and a solvent through a reaction chamber of a continuous flow reactor, the lignin polymer comprising hydroxycinnamic groups bound to a polymeric backbone; flowing ozone through the reaction chamber containing the lignin composition under conditions to maximize oxidative cleavage of the hydroxycinnamic groups to produce one or more types of aromatic monomers while minimizing oxidative cleavage of the polymeric backbone; and collecting the one or more types of aromatic monomers, e.g., by a size-selective membrane separation device.

4. 发明授权

US09469580B2 Dehydrogenation process 有权
标题翻译：脱氢工艺
公开(公告)号：US09469580B2
公开(公告)日：2016-10-18
申请号：US14435670
申请日：2013-11-18
申请人： ExxonMobil Chemical Patents Inc.
发明人： Tan-Jen Chen , Christopher L. Becker , Hari Nair , Francisco M. Benitez , Charles Morris Smith
IPC分类号： C07C45/00 , C07C37/60 , C07C2/74 , C07C5/367 , C07C45/29 , C07C37/08 , C07C45/53 , C07C407/00 , B01J23/62
CPC分类号： C07C5/367 , B01J23/626 , C07C2/74 , C07C37/08 , C07C37/60 , C07C45/294 , C07C45/53 , C07C407/00 , C07C2101/14 , C07C2521/08 , C07C2523/14 , C07C2523/42 , C07C2523/62 , C07C2601/14 , Y02P20/52 , C07C409/14 , C07C49/403 , C07C39/04 , C07C13/28 , C07C15/04
摘要： Disclosed herein is a process for dehydrogenating a hydrocarbon with a dehydrogenation catalyst comprising a step of activating the catalyst precursor in a H2-containing atmosphere. A particularly advantageous activation process includes heating the catalyst precursor to a temperature in a range from 400° C. to 600° C. The process of the present disclosure is particularly advantageous for dehydrogenating cyclohexane to make benzene.
摘要翻译：本文公开了一种用脱氢催化剂使烃脱氢的方法，包括在含H2气氛中活化催化剂前体的步骤。特别有利的活化方法包括将催化剂前体加热至400℃至600℃的温度。本公开的方法对于使环己烷脱氢以制备苯是特别有利的。

5. 发明申请

US20120129736A1 HIGHLY OXIDIZED GRAPHENE OXIDE AND METHODS FOR PRODUCTION THEREOF 有权
标题翻译：高度氧化的氧化石墨及其生产方法
公开(公告)号：US20120129736A1
公开(公告)日：2012-05-24
申请号：US13321623
申请日：2010-05-14
申请人： James M. Tour , Dmitriy V. Kosynkin
发明人： James M. Tour , Dmitriy V. Kosynkin
IPC分类号： C09K8/03 , C07C67/00 , C07C39/12 , C01B31/00 , C01B31/04 , C07C37/60 , C07C245/20 , B82B3/00 , B82B1/00
CPC分类号： C01B31/0476 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/23 , C09K8/032
摘要： A highly oxidized form of graphene oxide and methods for production thereof are described in various embodiments of the present disclosure. In general, the methods include mixing a graphite source with a solution containing at least one oxidant and at least one protecting agent and then oxidizing the graphite source with the at least one oxidant in the presence of the at least one protecting agent to form the graphene oxide. Graphene oxide synthesized by the presently described methods is of a high structural quality that is more oxidized and maintains a higher proportion of aromatic rings and aromatic domains than does graphene oxide prepared in the absence of at least one protecting agent. Methods for reduction of graphene oxide into chemically converted graphene are also disclosed herein. The chemically converted graphene of the present disclosure is significantly more electrically conductive than is chemically converted graphene prepared from other sources of graphene oxide.
摘要翻译：在本公开的各种实施方案中描述了高度氧化形式的石墨烯氧化物及其生产方法。通常，所述方法包括将石墨源与含有至少一种氧化剂和至少一种保护剂的溶液混合，然后在至少一种保护剂存在下用至少一种氧化剂氧化石墨源以形成石墨烯氧化物。通过目前描述的方法合成的石墨烯氧化物具有比在不存在至少一种保护剂时制备的氧化石墨烯更高氧化并且维持更高比例的芳香环和芳族结构域的高结构质量。将氧化石墨烯还原成化学转化的石墨烯的方法也在本文中公开。本公开的化学转化的石墨烯比由其他氧化石墨烯源生产的化学转化的石墨烯显着更具导电性。

6. 发明授权

US06911563B2 Reaction method utilizing diaphram type catalyst and apparatus therefor 有权
标题翻译：利用二价型催化剂的反应方法及其设备
公开(公告)号：US06911563B2
公开(公告)日：2005-06-28
申请号：US10451624
申请日：2001-12-27
申请人： Fujio Mizukami , Shuichi Niwa , Makoto Toba , Naotsugu Itoh , Tomonari Saito , Takemi Nanba , Hiroshi Shoji , Kazuhiko Haba
发明人： Fujio Mizukami , Shuichi Niwa , Makoto Toba , Naotsugu Itoh , Tomonari Saito , Takemi Nanba , Hiroshi Shoji , Kazuhiko Haba
IPC分类号： B01J8/00 , B01J10/00 , B01J12/00 , B01J14/00 , B01J19/24 , B01J23/44 , B01J35/06 , C07C29/50 , C07C37/58 , C07C37/60 , C07C39/04 , C07C39/07 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C45/40 , C07D213/63 , C07L37/00
CPC分类号： C07D213/63 , B01J8/009 , B01J10/007 , B01J12/007 , B01J14/005 , B01J19/2475 , B01J23/44 , B01J35/065 , B01J2219/00063 , B01J2219/00094 , B01J2219/00099 , C07C29/50 , C07C37/58 , C07C37/60 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C45/40 , C07C2601/14 , Y02P20/52 , C07C49/08 , C07C47/22 , C07C35/08 , C07C39/04 , C07C39/07 , C07C39/14 , C07C35/36
摘要： A method for carrying out a reaction of one substance capable of being activated by a catalyst with another substance capable of reacting with said one substance activated, characterized in that the substance capable of being activated is activated by passing the substance through a diaphragm type catalyst and the reaction is thus performed in one reaction step; a method for producing an aromatic alcohol utilizing the above method; and a reaction apparatus suitable for these reactions. In the method, one substance is activated by passing through a diaphragm type catalyst and an objective reaction is carried out by using the activated substance, and the reaction can be performed in one reaction step and with safety. Moreover, the contact of the above activated substance with a compound to be reacted therewith can be freely controlled, and therefore, over-reaction can be prevented and an objective product can be produced in high yield. The method is thus markedly advantageous from an economical view point as a commercial process for producing oxygen-containing organic compounds such as an aromatic alcohol, a ketone, an aldehyde, a carboxylic acid and an epoxide.
摘要翻译：一种能够使一种能够被催化剂活化的物质与能够与所述一种活化物质反应的物质进行反应的方法，其特征在于，通过使该物质通过隔膜型催化剂而活化，因此在一个反应步骤中进行反应; 利用上述方法制备芳族醇的方法; 和适用于这些反应的反应装置。在该方法中，通过隔膜型催化剂活化一种物质，并通过使用活性物质进行目标反应，反应可以在一个反应步骤和安全性下进行。此外，可以自由地控制上述活性物质与其反应的化合物的接触，因此可以防止过度反应，并且可以高产率制备目标产物。因此，作为用于生产含氧有机化合物如芳族醇，酮，醛，羧酸和环氧化物的商业方法，从经济角度看，该方法显着是有利的。

7. 发明申请

US20050070744A1 PROCESS FOR CONVERSION OF PHENOL TO HYDROQUINONE AND QUINONES 失效
标题翻译：苯酚转化为氢醌和喹啉的方法
公开(公告)号：US20050070744A1
公开(公告)日：2005-03-31
申请号：US10671871
申请日：2003-09-29
申请人： Gajanan Dewkar , Vinay Thakur , Sanjeevani Pardhy , Arumugam Sudalai , Sukumar Devotta
发明人： Gajanan Dewkar , Vinay Thakur , Sanjeevani Pardhy , Arumugam Sudalai , Sukumar Devotta
IPC分类号： B01J21/06 , B01J37/03 , C07C37/60 , C07C39/08 , C07C46/06 , C07C37/58
CPC分类号： B01J21/063 , B01J37/033 , C07C37/60 , C07C46/06 , C07C50/24 , C07C50/04 , C07C50/02 , C07C39/08
摘要： The present invention relates to a process for the conversion of phenol to hydroquinone and quinones. More particularly this invention relates to a process for the oxidation of phenol to a mixture of 1,4-benzoquinone and hydroquinone using an oxidant in the presence of titanium superoxide as a reusable catalyst in a liquid phase condition.
摘要翻译：本发明涉及一种将苯酚转化为氢醌和醌的方法。更具体地说，本发明涉及在液相条件下，在超氧化钛作为可重复使用的催化剂存在下，使用氧化剂将苯酚氧化为1,4-苯醌和氢醌的混合物的方法。

8. 发明授权

US6166268A Selective oxidation and the synthesis of hydroxyl-containing aromatic compounds 失效
标题翻译：选择性氧化和合成含羟基的芳族化合物
公开(公告)号：US6166268A
公开(公告)日：2000-12-26
申请号：US301574
申请日：1999-04-29
申请人： Adolf Kuehnle , Mark Duda
发明人： Adolf Kuehnle , Mark Duda
IPC分类号： B01J23/745 , C07C37/60 , C07C37/00
CPC分类号： C07C37/60 , Y02P20/52 , C07C39/04
摘要： The invention relates to a process for preparing hydroxyl-containing aromatic compounds by catalytic oxidation.
摘要翻译：本发明涉及通过催化氧化制备含羟基芳族化合物的方法。

9. 发明授权

US6156939A Process for the hydroxylation of aromatic hydrocarbons 有权
标题翻译：芳烃羟基化方法
公开(公告)号：US6156939A
公开(公告)日：2000-12-05
申请号：US542457
申请日：2000-04-04
申请人： Rodolfo Vignola , Ezio Battistel , Daniele Bianchi , Rossella Bortolo , Roberto Tassinari
发明人： Rodolfo Vignola , Ezio Battistel , Daniele Bianchi , Rossella Bortolo , Roberto Tassinari
IPC分类号： B01J31/28 , B01J23/745 , B01J31/04 , C07B41/02 , C07B61/00 , C07C37/60 , C07C39/04 , C07C39/06 , C07C69/96 , C07C37/00
CPC分类号： B01J31/403 , B01J23/745 , B01J31/04 , B01J31/181 , B01J31/2208 , C07B41/02 , C07C37/60 , B01J2531/842 , Y02P20/52 , Y02P20/584
摘要： The invention relates to a process for the hydroxylation of aromatic hydrocarbons by direct oxidation with hydrogen peroxide. The process is carried out in the presence of a catalyst comprising:iron, administered as inorganic salt;iron ligand, consisting of carboxylic acids of ether-aromatic compounds containing nitrogen, in particular pyrazin-2-carboxylic acid and derivatives;acidifying agent, especially trifluoracetic acid, and a solvent system comprising an organic phase consisting of a substrate and acetonitrile and an aqueous phase containing the catalyst and hydrogen peroxide.
摘要翻译：本发明涉及通过用过氧化氢直接氧化来芳族烃的羟基化的方法。该方法在催化剂的存在下进行，所述催化剂包含：作为无机盐施用的铁; 铁配体，由含氮的醚 - 芳族化合物的羧酸组成，特别是吡嗪-2-羧酸及其衍生物; 酸化剂，特别是三氟乙酸，以及包含由底物和乙腈组成的有机相和含有催化剂和过氧化氢的水相的溶剂体系。

10. 发明授权

US5932773A Process for the preparation of .alpha. and .beta. napthol by hydroxylation of naphthalene using organotransition metal complex 失效
标题翻译：通过使用有机过渡金属络合物萘的羟基化制备α和β-萘酚的方法
公开(公告)号：US5932773A
公开(公告)日：1999-08-03
申请号：US829400
申请日：1997-03-31
申请人： Paul Ratnasamy , Robert Raja , Pramod Prabhakar Moghe , Madhav Gopal Kotasthane , Ashwini Vinayak Pol , Prakash Kondiba Bahirat
发明人： Paul Ratnasamy , Robert Raja , Pramod Prabhakar Moghe , Madhav Gopal Kotasthane , Ashwini Vinayak Pol , Prakash Kondiba Bahirat
IPC分类号： C07C37/60 , C07C37/00
CPC分类号： C07C37/60
摘要： This invention relates to a process for the hydroxylation of napthalene to .varies. and .beta. naphthols which comprises reacting napthalene with hydrogen peroxide in the presence of a solid catalyst containing an organotransition metal complex wherein some or all of the hydrogen atoms of the said organotransition metal complex have been substituted by one or more electron withdrawing group in the presence of solvents, with or without promoter and isolating the naphthols formed by conventional methods.
摘要翻译：本发明涉及一种将萘羟基化成比例和β-萘酚的方法，其包括在含有有机过渡金属络合物的固体催化剂存在下使萘与过氧化氢反应，其中所述有机过渡金属络合物的一些或全部氢原子具有在有或没有促进剂的溶剂存在下被一个或多个吸电子基团取代，并分离由常规方法形成的萘酚。

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