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1. 发明申请

US20210340681A1 ELECTROCHEMICAL SYSTEM, APPARATUS AND METHOD TO GENERATE METAL HYDROXIDE IN THE PRESENCE OF METAL SILICATES 有权
公开(公告)号：US20210340681A1
公开(公告)日：2021-11-04
申请号：US17243499
申请日：2021-04-28
申请人： Planetary Hydrogen Inc.
发明人： Gregory Hudson Rau , Sadaf Tahmasebi , Clive Mervyn Hugh Brereton , Alexandru Vasile Mezei , Michael John Kelland
IPC分类号： C25B9/23 , C25B1/02 , C25B1/20 , C25B1/50 , C25B15/08 , C25B9/65 , B01D53/62
摘要： An apparatus and method are provided for the electrochemical production of hydrogen, oxygen and metal hydroxide wherein the metal is derived from a metal silicate. The process involves the electrolysis of a metal salt solution where hydrogen and a metal hydroxide are produced at the cathode, and oxygen, or chlorine, and an acid are produced at the anode. The acid is reacted with a metal silicate producing a soluble metal salt and water that is used in turn to make solid or dissolved metal hydroxide. The net CO2 and acid gas emissions of the invention and its products may therefore be significantly reduced or turned negative.

2. 发明授权

US10759671B2 Method for manufacturing lithium hydroxide and lithium carbonate, and device therefor 有权
公开(公告)号：US10759671B2
公开(公告)日：2020-09-01
申请号：US15570400
申请日：2016-04-29
申请人： RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE & TECHNOLOGY
发明人： Sung Kook Park , Kwang Seok Park , Sang Gil Lee , Woo Chul Jung , Ki Young Kim , Hyun Woo Lee
IPC分类号： B01D61/44 , B01D61/50 , C01D15/08 , C25B1/20 , C01D15/02 , C25B1/14 , B01D53/46 , C01D15/04
摘要： The present invention relates to a method for manufacturing lithium hydroxide and lithium carbonate, and a device therefor. The present invention provides a method for manufacturing lithium hydroxide, comprising: a step of dissolving lithium phosphate in an acid; a step of preparing a monovalent ion selective-type electrodialysis device disposed in the order of a cathode cell containing a cathode separator, a monovalent anion selective-type dialysis membrane for selectively permeating a monovalent anion, a monovalent cation selective-type dialysis membrane for selectively permeating a monovalent cation, and an anode cell containing an anode separator, injecting the lithium phosphate dissolved in the acid between the anode separator of the anode cell and the monovalent cation selective-type dialysis membrane, and between the cathode separator of the cathode cell and the monovalent anion selective-type dialysis membrane, respectively, and injecting water between the monovalent cation selective-type dialysis membrane and the monovalent anion selective-type dialysis membrane; a step of obtaining an aqueous lithium chloride solution, and at the same time, obtaining a phosphoric acid aqueous solution formed as a byproduct, by applying an electric current to the monovalent ion selective-type electrodialysis device; and a step of converting the obtained aqueous lithium chloride solution into an aqueous lithium hydroxide solution.

3. 发明授权

US09180424B2 Infrared assisted hydrogen generation 有权
标题翻译：红外辅助氢生成
公开(公告)号：US09180424B2
公开(公告)日：2015-11-10
申请号：US12930812
申请日：2011-01-18
申请人： Albert Chin-Tang Wey
发明人： Albert Chin-Tang Wey
IPC分类号： C25B1/20 , C01B3/02 , B01J19/12 , B01J19/08 , C25B1/00 , B01J19/24 , C25B1/02
CPC分类号： B01J19/087 , B01J19/128 , B01J19/2475 , C01B3/02 , C25B1/003 , C25B1/02
摘要： This invention relates to a system and a method for achieving efficient production of hydrogen in a hydrogen generator, comprising at least a hydrogen generator, a liquid in said hydrogen generator to produce hydrogen from, and a ceramic that emits infrared at wavelengths covering at least a portion of 3-20 micrometers range so that said liquid can be excited with infrared at said wavelengths before or during the production of hydrogen for improved hydrogen production efficiency. The use of infrared-excited electrolyte solution in a hydrogen generator helps reduce the energy consumption, lower operating voltage, and thus reduce the cost of the production of hydrogen.
摘要翻译：本发明涉及一种用于在氢发生器中实现氢的有效生产的系统和方法，所述系统和方法至少包括氢生成器，所述氢发生器中的液体，以产生氢气，以及陶瓷，所述陶瓷以波长覆盖至少一个部分3-20微米的范围，使得所述液体可以在生产氢气之前或期间用所述波长的红外线激发，以提高制氢效率。在氢气发生器中使用红外激发电解质溶液有助于降低能量消耗，降低工作电压，从而降低生产氢气的成本。

4. 发明申请

US20150183653A1 METHOD FOR PREPARING ALKALI METAL CARBONATES FROM INORGANIC MATERIALS INCLUDING ALKALI METAL IONS USING ELECTROLYSIS SYSTEM 审中-公开
标题翻译：从无机材料制备碱金属碳酸盐的方法，包括使用电解质体系的碱金属离子
公开(公告)号：US20150183653A1
公开(公告)日：2015-07-02
申请号：US14585936
申请日：2014-12-30
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Kwang Deog JUNG , Heung Yong HA , Jun Woo OH , Sung Min LEE , Ho Yong JO
IPC分类号： C01F11/18 , C22B26/20 , C25B9/08 , C22B7/00 , C25B1/20 , C25B1/22
CPC分类号： C22B26/20 , C01D7/07 , C01D7/12 , C01F11/181 , C01P2002/72 , C01P2004/03 , C01P2004/10 , C01P2004/38 , C01P2004/39 , C01P2004/62 , C01P2006/80 , C22B7/007 , C25B1/20 , C25B1/22 , C25B9/08 , C25B15/08
摘要： The present invention relates to a method for preparing a carbonate of an alkali ion using an electrolysis system, more particularly to an improved method for preparing a carbonate of an alkali ion, including eluting an alkali ion from an inorganic material containing the alkali ion and converting the eluted alkali ion to a carbonate, using an electrolysis system which generates an eluting agent and a quick precipitating agent used for the elution of the alkali ion and the conversion to the carbonate at the same time.
摘要翻译：本发明涉及一种使用电解系统制备碱金属碳酸盐的方法，更具体地说，涉及一种制备碱金属碳酸盐的改进方法，该方法包括从含有碱金属的无机材料中洗脱出碱金属离子，使用产生洗脱剂的电解系统和用于碱性离子洗脱的快速沉淀剂和同时转化为碳酸盐的碳酸盐洗脱的碱离子。

5. 发明授权

US08894830B2 CO2 utilization in electrochemical systems 有权
标题翻译：电化学系统中的CO2利用率
公开(公告)号：US08894830B2
公开(公告)日：2014-11-25
申请号：US13540992
申请日：2012-07-03
申请人： Ryan J. Gilliam , Thomas A. Albrecht , Nikhil Jalani , Nigel Antony Knott , Valentin Decker , Michael Kostowskyj , Bryan Boggs , Alexander Gorer , Kasra Farsad
发明人： Ryan J. Gilliam , Thomas A. Albrecht , Nikhil Jalani , Nigel Antony Knott , Valentin Decker , Michael Kostowskyj , Bryan Boggs , Alexander Gorer , Kasra Farsad
IPC分类号： C25B1/20 , C25B15/08 , C01F5/24 , C01F11/18 , B01D61/44
CPC分类号： C25B1/14 , B01D53/326 , B01D61/422 , B01D61/44 , B01D61/46 , B01D2257/504 , B01D2313/08 , B01D2313/16 , B01D2313/26 , C01B7/01 , C01D1/40 , C01D7/07 , C01F5/24 , C01F11/18 , C02F1/46109 , C02F1/68 , C02F2001/46166 , C02F2201/46115 , C02F2201/4613 , C02F2201/46135 , C02F2201/46185 , C02F2209/06 , C02F2301/046 , C25B1/00 , C25B1/02 , C25B1/04 , C25B1/16 , C25B1/20 , C25B1/26 , C25B15/08 , Y02C10/04 , Y02E60/366 , Y02P20/152
摘要： A low-voltage, low-energy electrochemical system and method of removing protons and/or producing a base solution comprising hydroxide and carbonate/bicarbonate ions, utilizing carbon dioxide in a cathode compartment that is partitioned into a first cathode electrolyte compartment and a second cathode electrolyte compartment such that liquid flow between the cathode electrolyte compartments is possible, but wherein gaseous communication between the cathode electrolyte compartments is restricted. Carbon dioxide gas in one cathode electrolyte compartment is utilized with the cathode electrolyte in both compartments to produce the base solution with less that 3V applied across the electrodes.
摘要翻译：一种低电压，低能量的电化学系统和消除质子和/或产生包含氢氧化物和碳酸盐/碳酸氢根离子的碱性溶液的方法，其利用分隔成第一阴极电解质隔室和第二阴极的阴极室中的二氧化碳电解质隔室，使得阴极电解质隔室之间的液体流动是可能的，但是其中阴极电解质隔室之间的气体连通被限制。一个阴极电解质室中的二氧化碳气体与两个隔室中的阴极电解质一起使用，以产生较少3V施加在电极上的碱溶液。

6. 发明申请

US20130034489A1 ELECTROCHEMICAL HYDROXIDE SYSTEM AND METHOD USING FINE MESH CATHODE 审中-公开
标题翻译：电化学氢氧化物系统和使用精细网状阴极的方法
公开(公告)号：US20130034489A1
公开(公告)日：2013-02-07
申请号：US13365440
申请日：2012-02-03
申请人： RYAN J. GILLIAM , Bryan Boggs , Michael Kostowskyj , Nigel Antony Knott , Rebecca Lynne King , Alexander Gorer
发明人： RYAN J. GILLIAM , Bryan Boggs , Michael Kostowskyj , Nigel Antony Knott , Rebecca Lynne King , Alexander Gorer
IPC分类号： C01B31/24 , C01F5/24 , C25B9/00 , C01F11/18 , C25B1/20 , C25B13/00
CPC分类号： C25B1/20 , C01B32/60 , C01F5/24 , C01F11/18 , C25B9/08 , C25B15/08
摘要： Provided herein are methods and systems including contacting an anode electrolyte with an anode; contacting a cathode electrolyte with a cathode where cathode is a fine mesh cathode; and applying voltage across the anode and the cathode. The methods and systems further may include treating hydroxide ions produced at the cathode with carbon from a source of carbon.
摘要翻译：本文提供了包括使阳极电解质与阳极接触的方法和系统; 使阴极电解质与阴极是细网状阴极的阴极接触; 并在阳极和阴极上施加电压。所述方法和系统还可包括用来自碳源的碳处理在阴极处产生的氢氧根离子。

7. 发明授权

US08021536B2 Method and apparatus for achieving maximum yield in the electrolytic preparation of group IV and V hydrides 有权
标题翻译：在IV族和V型氢化物的电解制备中获得最大产率的方法和装置
公开(公告)号：US08021536B2
公开(公告)日：2011-09-20
申请号：US11687947
申请日：2007-03-19
申请人： Reinaldo Mario Machado , Christopher L. Hartz , James E. Hollen , Rebecca J. Mohr , George L. Ryals
发明人： Reinaldo Mario Machado , Christopher L. Hartz , James E. Hollen , Rebecca J. Mohr , George L. Ryals
IPC分类号： C25B7/00 , C25B1/00 , C25B1/20
CPC分类号： C25B1/00 , C23C16/4488 , C25B15/08
摘要： A method for generating a hydride gas of metal M1 in an electrochemical cell comprising a cathode comprising metal M1, a sacrificial anode comprising metal M2, an initial concentration of aqueous electrolyte solution comprising a metal hydroxide, M3OH, wherein the sacrificial metal anode electrochemically oxidizes in the presence of the aqueous electrolyte solution comprising M3OH to form a metal salt, and the hydride gas of metal M1 is formed by reducing the metal M1 of the cathode. The method comprises the steps of determining solubility profile curves of the metal salt as the M3OH is consumed and the metal oxide is formed by the oxidation reaction at various concentrations of M3OH; determining a maximum concentration of M3OH that, as it is consumed, does not yield a concentration of metal salt that precipitates out of the electrolyte solution; and choosing a concentration of M3OH that is in the range of at and within 5% less than the maximum concentration of M3OH to be the initial concentration of M3OH.
摘要翻译：一种用于在电化学电池中产生金属M1的氢化物气体的方法，包括：包含金属M1的阴极，包含金属M2的牺牲阳极，包含金属氢氧化物的初始浓度的电解质水溶液，M3OH，其中牺牲金属阳极电化学氧化含有M3OH的电解质水溶液的存在形成金属盐，通过还原阴极的金属M1形成金属M1的氢化物气体。该方法包括以下步骤：测定当M3OH被消耗时金属盐的溶解度曲线曲线，并且通过在不同浓度的M3OH下的氧化反应形成金属氧化物; 确定在消耗时不会产生从电解液中析出的金属盐浓度的M3OH的最大浓度; 并选择在M3OH的最大浓度以下且小于5％的范围内的M3OH浓度成为M3OH的初始浓度。

8. 发明授权

US5891320A Soluble magnesium hydroxide 失效
标题翻译：可溶性氢氧化镁
公开(公告)号：US5891320A
公开(公告)日：1999-04-06
申请号：US701777
申请日：1996-08-26
申请人： Stephen R. Wurzburger , James M. Overton
发明人： Stephen R. Wurzburger , James M. Overton
IPC分类号： C01F5/22 , C01F11/46 , C02F1/44 , C02F1/461 , C02F1/48 , C02F1/66 , C02F9/00 , C25B1/20 , C01F1/00 , C01F5/40
CPC分类号： C01F5/22 , C01F11/46 , C02F1/461 , C02F1/488 , C02F1/66 , C02F9/00 , C01P2004/61 , C02F1/441 , C02F1/48 , C02F2101/20 , C02F2103/023 , C02F2103/10
摘要： A clear solution and a method for preparing the solution which has a pH in the range of from 10 to 13.9 and containing sulfate ions in a concentration range less than 500 parts per million. The solution is prepared by mixing two solutions in which one solution has one equivalent of magnesium sulfate and an equivalent of sulfuric acid and the second solution has an equivalent of Ca (OH).sub.2 and two equivalents of K.sub.2 OH. It is believed that CaSO.sub.4 precipitates in the mixed solution and causes coprecipitation of potassium, perhaps as double salt with the Ca leaving OH stabilized by hydration and magnesium ions.
摘要翻译：一种澄清溶液和一种制备溶液的方法，其pH为10-13.9，含有浓度范围小于500ppm的硫酸根离子。该溶液通过混合两种溶液制备，其中一种溶液具有一当量硫酸镁和当量的硫酸，第二溶液具有当量的Ca（OH）2和两当量的K 2 OH。据信CaSO 4在混合溶液中沉淀，并引起钾的共沉淀，可能是与通过水合和镁离子稳定的Ca离去的双重盐。

9. 发明授权

US5599436A Process for the preparation of manganese(III)-containing nickel hydroxide 失效
标题翻译：制备含锰（III）的氢氧化镍的方法
公开(公告)号：US5599436A
公开(公告)日：1997-02-04
申请号：US547802
申请日：1995-10-25
申请人： Peter Axmann
发明人： Peter Axmann
IPC分类号： C01G53/00 , H01M4/50 , H01M4/52 , C25B1/20 , C01G1/00 , C01G45/00 , C01G49/00
CPC分类号： C01G53/00 , H01M4/50 , H01M4/52 , C01P2006/40
摘要： The present invention relates to a process for the preparation of manganese(III)-containing nickel(II) hydroxide powders, more than 50 mole % of the manganese being present in the trivalent oxidation state, by co-precipitation of nickel(II) and manganese salt solutions with alkali liquors.
摘要翻译：本发明涉及一种制备含有锰（III）的氢氧化镍（II）粉末的方法，其中超过50摩尔％的锰以三价氧化态存在，通过共沉淀镍（II）和锰盐溶液与碱液。

10. 发明授权

US5286354A Method for preparing organic and inorganic hydroxides and alkoxides by electrolysis 失效
标题翻译：通过电解制备有机和无机氢氧化物和醇盐的方法
公开(公告)号：US5286354A
公开(公告)日：1994-02-15
申请号：US45819
申请日：1993-04-09
申请人： Allen I. Bard , Hossein Sharifian
发明人： Allen I. Bard , Hossein Sharifian
IPC分类号： C25B1/00 , C25B1/16 , C25B1/20 , C25B1/24 , C25B1/26 , C25B3/00
CPC分类号： C25B3/00 , C25B1/00
摘要： An electrolytic process for making hydroxides or alkoxides from the corresponding halide salts in a divided cell where the desired compounds are formed in the catholyte while the accumulation of halogen in the anolyte is effectively prevented throught the action of a reducing agent added to the acidic anolyte.
摘要翻译：通过加入到酸性阳极电解液中的还原剂的作用，有效地防止在阴极电解液中形成所需化合物的分隔池中相应卤化物盐中的氢氧化物或醇盐的电解方法。

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