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1. 发明授权

US09624318B2 Matting agent for UV varnishes 有权
公开(公告)号：US09624318B2
公开(公告)日：2017-04-18
申请号：US13498343
申请日：2010-08-20
申请人： Klaus Benner , Hans-Dieter Christian , Gottlieb Lindner , Karl Meier
发明人： Klaus Benner , Hans-Dieter Christian , Gottlieb Lindner , Karl Meier
IPC分类号： C08F2/48 , C08F2/44 , C01B33/143 , C01B33/146 , C01B33/187
CPC分类号： C08F2/48 , C01B33/143 , C01B33/146 , C01B33/187 , C01P2004/61 , C08F2/44
摘要： The invention relates to matted UV varnishes comprising silicon dioxide, the surface thereof having been modified by means of treatment with a multiple bond organopolysiloxane so as to be particularly well-suited for use as a matting material for UV varnishes, and to a method for producing same.

2. 发明申请

US20170051126A1 PROCESS FOR THE PREPARATION OF PRECIPITATED SILICAS, PRECIPITATED SILICAS AND THEIR USES, IN PARTICULAR FOR THE REINFORCEMENT OF POLYMERS 审中-公开
标题翻译：制备降解硅，沉淀硅和其用途的方法，特别是聚合物增强
公开(公告)号：US20170051126A1
公开(公告)日：2017-02-23
申请号：US15118683
申请日：2015-02-12
申请人： RHODIA OPERATIONS
发明人： Cédric BOIVIN , Laurent GUY , Eric PERIN , Kilani LAMIRI
IPC分类号： C08K3/36 , C09C1/30 , C01B33/187
摘要： The invention relates to a process for the preparation of a novel precipitated silica, wherein: a silicate is reacted with an acidifying agent, so as to obtain a silica suspension; said silica suspension is filtered, so as to obtain a filter cake; said filter cake is subjected to a liquefaction operation, optionally in the presence of an aluminium compound; wherein at least one polycarboxylic acid is added to the filter cake, during or after the liquefaction operation. It also relates to a novel precipitated silica and to its uses.
摘要翻译：本发明涉及一种制备新型沉淀二氧化硅的方法，其中：将硅酸盐与酸化剂反应，得到二氧化硅悬浮液; 将所述二氧化硅悬浮液过滤，得到滤饼; 所述滤饼任选在铝化合物存在下进行液化操作; 其中在液化操作期间或之后，将至少一种多元羧酸加入到滤饼中。它还涉及一种新型沉淀二氧化硅及其用途。

3. 发明授权

US08986642B2 Metal oxide or semimetal oxide spherical beads, a process for making, and a process for using 有权
标题翻译：金属氧化物或半金属氧化物球形珠，制造方法和使用方法
公开(公告)号：US08986642B2
公开(公告)日：2015-03-24
申请号：US13770577
申请日：2013-02-19
申请人： BASF SE
发明人： Angela Siegel , Tobias Eckardt , Andreas Braedikow , Thorsten Puvogel
IPC分类号： C03C11/00 , C01B33/193 , C08F4/02 , C08F4/00 , B01J21/08 , B01J35/02 , B01J35/08 , B01J35/10 , B01J37/03 , C01B13/32 , C01B33/16 , C01B33/187 , B01J23/24 , B01J23/40 , B01J23/70 , C08F110/02 , C08F110/06
CPC分类号： C01B33/193 , B01J21/08 , B01J23/24 , B01J23/40 , B01J23/70 , B01J35/023 , B01J35/08 , B01J35/1019 , B01J35/1023 , B01J37/031 , C01B13/328 , C01B33/166 , C01B33/187 , C01P2004/32 , C01P2004/52 , C01P2004/54 , C01P2004/61 , C01P2006/12 , C01P2006/14 , C08F4/00 , C08F4/02 , C08F110/02 , C08F110/06 , Y10T428/2982
摘要： The present invention relates to spherical beads comprising at least one metal and/or semimetal oxide, having a mean diameter in the range from 10 to 120 μm, a BET surface area in the range from 400 to 800 m2/g and a pore volume in the range from 0.3 to 3.0 cm3/g, wherein the diameter of a given bead at any one point of said bead deviates by less than 10% from the average diameter of said bead and the surface of said bead is substantially smooth, and also to a process for producing these spherical beads, to a particulate catalyst comprising the spherical beads and to the use of the spherical beads as catalysts or catalyst carriers.
摘要翻译：本发明涉及包含至少一种金属和/或半金属氧化物的球形珠粒，其平均直径为10至120μm，BET表面积为400-800m2 / g，孔体积为范围为0.3至3.0cm 3 / g，其中在所述珠的任何一点处的给定珠粒的直径与所述珠粒的平均直径相差小于10％，并且所述珠粒的表面基本上平滑，并且还用于制备这些球形珠粒的方法，包括球形珠粒的颗粒催化剂和使用球形珠粒作为催化剂载体。

4. 发明申请

US20130156674A1 NOVEL METHOD FOR PREPARING PRECIPITATED SILICAS CONTAINING ALUMINIUM 有权
标题翻译：用于制备包含铝的预制硅的新方法
公开(公告)号：US20130156674A1
公开(公告)日：2013-06-20
申请号：US13636995
申请日：2011-03-25
申请人： Laurent Guy , Dominique Dupuis , Eric Perin
发明人： Laurent Guy , Dominique Dupuis , Eric Perin
IPC分类号： C01B33/187
CPC分类号： C01B33/187 , C01B33/193
摘要： A method for preparing precipitated silicas is described. A precipitation reaction between a silicate and an acidifying agent is also described, wherein a precipitated silica suspension is produced, and, subsequently, separation and drying of the suspension is conducted, in which, inter alia, one of the following three operations (a, b or c) is performed: (a) simultaneously adding a compound of aluminium and a basic agent, (b) simultaneously adding a silicate and a compound of aluminium, (c) simultaneously adding the acidifying agent, a silicate and a compound of aluminium.
摘要翻译：描述了制备沉淀二氧化硅的方法。还描述了硅酸盐和酸化剂之间的沉淀反应，其中制备沉淀二氧化硅悬浮液，随后进行悬浮液的分离和干燥，其中尤其是以下三种操作之一（a， b或c）：（a）同时加入铝和碱性试剂的化合物，（b）同时加入硅酸盐和铝化合物，（c）同时加入酸化剂，硅酸盐和铝化合物。

5. 发明授权

US6013234A Silica pigment particulates 失效
标题翻译：二氧化硅颜料颗粒
公开(公告)号：US6013234A
公开(公告)日：2000-01-11
申请号：US479530
申请日：1995-06-07
申请人： Jean-Louis Ray , Maurice Coudurier
发明人： Jean-Louis Ray , Maurice Coudurier
IPC分类号： C08L7/00 , C01B33/113 , C01B33/18 , C01B33/187 , C08K3/36 , C08K9/00 , C08L21/00 , C08L23/00 , C08L101/00 , C09C1/00 , C09C1/28 , C09C1/30 , C09C1/42
CPC分类号： C09C1/42 , C08K3/36 , C09C1/28 , C09C1/30 , C09C1/309 , C01P2004/01 , C01P2004/60 , C01P2006/11 , C01P2006/12 , C01P2006/22
摘要： Dry, freely-flowing, water-insoluble but readily dispersible, solid and homogeneous silica pigment particulates essentially spheroidal in geometrical configuration and having a mean particle size in excess of 80.mu., preferably in excess of 150.mu., are prepared by atomizing to dryness a pulverulent aqueous suspension of silica having a solids contact in excess of 18%. Such silica pigment particulates, advantageously comprised of precipitated silica, are well adapted as reinforcing fillers for elastomeric matrices.
摘要翻译：干燥，自由流动的水不溶性但易于分散的固体和均匀的二氧化硅颜料颗粒，其几何构型基本上是球形的，并且具有超过80μm，优选超过150μm的平均粒度通过雾化至干具有超过18％的固体接触的二氧化硅的粉末水性悬浮液。有利地由沉淀二氧化硅组成的这种二氧化硅颜料颗粒很适合作为弹性体基体的增强填料。

6. 发明授权

US5780005A Method for manufacturing spherical silica from olivine 失效
标题翻译：从橄榄石制造球形二氧化硅的方法
公开(公告)号：US5780005A
公开(公告)日：1998-07-14
申请号：US602772
申请日：1996-03-04
申请人： Svein Olerud
发明人： Svein Olerud
IPC分类号： C01B33/18 , C01B33/187 , C01B33/12
CPC分类号： B82Y30/00 , C01B33/187 , C01P2004/32 , C01P2004/50 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/60 , C01P2006/80
摘要： In a method for manufacturing silica a leaching of natural silicates is performed with hydrochloric acid or other mineral acids, draining, drying and possibly a grinding up of the residue of the product obtained. In order to obtain a spherical silica with a controlled particle size and surface characteristics a mineral olivine with the highest possible degree of purity is employed as the basic material. This raw material is reduced to a grain size between 0.05 and 5 mm. The particles are pretreated and washed for the removal of dust on the grain surfaces and heavy materials such as spinel and at least a part of the foliar and stem-like minerals such as serpentine, talc and pyroxene are removed. The olivine particles are then leached in a controlled leaching process where the acid concentration, leaching temperature and leaching time are controlled in order to achieve the desired primary particle size, specific surface and pore volume measured according to the BET method on the extracted silica. The particle agglomerate of spherical particles thus formed with a grain size between 30 and 70 nanometers are washed and dried in the conventional manner, whereupon the agglomerate is divided into the spherical particles.
摘要翻译： PCT No.PCT / NO94 / 00145 Sec。 371日期：1996年3月4日 102（e）1996年3月4日PCT 1994年9月1日PCT PCT。公开号WO95 / 07235 日期：1995年3月16日在二氧化硅的制造方法中，天然硅酸盐的浸出是用盐酸或其他无机酸进行的，排出，干燥和可能磨碎所得产品的残余物。为了获得具有受控粒度和表面特性的球形二氧化硅，采用具有最高纯度的矿物橄榄石作为基础材料。将该原料还原成0.05〜5mm的粒径。颗粒被预处理并洗涤以去除颗粒表面上的灰尘，并且重要材料如尖晶石和至少一部分叶面和茎状矿物如蛇纹石，滑石和辉石被去除。然后在受控浸出过程中浸出橄榄石颗粒，其中控制酸浓度，浸出温度和浸出时间，以获得根据提取的二氧化硅上的BET法测量的所需的一次粒径，比表面积和孔体积。将由此形成的粒径在30和70纳米之间的球形颗粒的颗粒聚集体以常规方式洗涤和干燥，由此将附聚物分成球形颗粒。

7. 发明授权

US5453260A Amorphous silica or silica-alumina spherical particles and process for preparation thereof 失效
标题翻译：无定形二氧化硅或二氧化硅 - 氧化铝球形颗粒及其制备方法
公开(公告)号：US5453260A
公开(公告)日：1995-09-26
申请号：US014777
申请日：1993-02-08
申请人： Tadahisa Nakazawa , Masahide Ogawa , Kiyoshi Abe , Kazuhiko Suzuki , Takashi Tokita , Toshio Ito
发明人： Tadahisa Nakazawa , Masahide Ogawa , Kiyoshi Abe , Kazuhiko Suzuki , Takashi Tokita , Toshio Ito
IPC分类号： A61K8/25 , A61K8/26 , A61Q1/02 , C01B33/187 , C01B39/28 , C08K7/18 , C09C1/30 , C09C1/40 , C10M171/00 , C01B33/12 , B01J21/12
CPC分类号： C01B33/187 , A61K8/25 , A61K8/26 , A61Q1/02 , C01B39/28 , C08K7/18 , C09C1/30 , C09C1/405 , C10M171/001 , A61K2800/43 , C01P2002/02 , C01P2002/72 , C01P2002/82 , C01P2004/03 , C01P2004/32 , C01P2004/50 , C01P2004/51 , C01P2004/52 , C01P2004/61 , C01P2004/62 , C01P2004/82 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/19 , C01P2006/60 , C01P2006/80 , C01P2006/82 , C01P2006/90
摘要： Disclosed are amorphous silica or silica-alumina spherical particles composed of X-ray diffractometrically substantially amorphous silica or silica-alumina, wherein individual particles have a definite spherical shape and a notched surface, the circularity (A) represented by the following formula: ##EQU1## wherein r1 stands for the radius of the circumcircle of the profile of the particle in an electron microscope photo thereof and r2 stands for the radius of the inscribed circle of the profile of the particle in the electron microscope photo, is in the range of from 0.90 to 1, the notching degree (B) represented by the formula: ##EQU2## wherein .DELTA.t stands for the depth between the peak and trough in the radial direction of notches on the profile of the particle in the electron microscope photo and r1 is as defined above, is in the range of from 1 to 10%, and the primary particle size (2r1) determined by the electron microscope method is in the range of from 0.1 to 20 .mu.m.
摘要翻译：公开了由X射线衍射法基本上无定形二氧化硅或二氧化硅 - 氧化铝组成的无定形二氧化硅或二氧化硅 - 氧化铝球形颗粒，其中单个颗粒具有确定的球形和缺口表面，由下式表示的圆形度（A）：f 电子显微镜照片中的颗粒轮廓的外接圆，r2表示电子显微镜照片中的颗粒轮廓的内切圆的半径在0.90〜1的范围内，切口度（B ）由下式表示：其中DELTA t代表电子显微镜照片中颗粒轮廓上凹口径向方向上的峰和谷之间的深度，r1如上所定义，在 1〜10％的范围和通过电子显微镜法测定的一次粒径（2r1）在0.1〜20μm的范围内。

8. 发明授权

US5418273A Aqueous suspensions of precipitated silica with anionic dispersant and aluminum compound 失效
标题翻译：沉淀二氧化硅与阴离子分散剂和铝化合物的水悬浮液
公开(公告)号：US5418273A
公开(公告)日：1995-05-23
申请号：US1399
申请日：1993-01-07
申请人： Adrien Dromard , Claude Richard
发明人： Adrien Dromard , Claude Richard
IPC分类号： C01B33/187 , B01F17/52 , C01B33/141 , D21H19/40 , D21H19/58 , C08K3/36 , C08K3/22 , C08K3/32
CPC分类号： C01B33/1417 , D21H19/40 , D21H19/58
摘要： Stable aqueous suspensions of precipitated silica, well adopted as coatings for the papermaking industry, include an aqueous suspension of a slaked precipitated silica filter cake and an effective amount of a stabilizer therefor, which stabilizer contains (a) aluminum or an aluminum compound, and (b) an anionic dispersing agent.
摘要翻译：沉淀二氧化硅的稳定的水性悬浮液，被良好地用作造纸工业的涂料，包括熟化的沉淀二氧化硅滤饼和有效量的稳定剂的水悬浮液，该稳定剂包含（a）铝或铝化合物和（ b）阴离子分散剂。

9. 发明授权

US5412018A Silicone rubber reinforced with reinforced precipitated silica 失效
标题翻译：硅橡胶用增强沉淀二氧化硅增强
公开(公告)号：US5412018A
公开(公告)日：1995-05-02
申请号：US741921
申请日：1991-08-08
申请人： Thomas G. Krivak , Timothy A. Okel , Melvin P. Wagner
发明人： Thomas G. Krivak , Timothy A. Okel , Melvin P. Wagner
IPC分类号： C01B33/12 , C01B33/187 , C01B33/193 , C08K3/36 , C08L83/04 , C09C1/30 , C08J5/10 , C08K3/34
CPC分类号： B82Y30/00 , C01B33/193 , C08K3/36 , C09C1/30 , C09C1/3081 , C01P2002/02 , C01P2004/04 , C01P2004/50 , C01P2004/61 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C01P2006/80 , C01P2006/82 , C01P2006/90
摘要： Elastomeric compositions contain crosslinked poly(diorganosiloxane) and reinforced precipitated silica having, on a coating-free and impregnant-free basis, a surface area of from about 220 to about 340 square meters per gram, a pore diameter at the maximum of the volume pore size distribution function of from about 9 to about 20 nanometers, and a total intruded volume of from about 2.6 to about 4.4 cubic centimeters per gram.
摘要翻译：弹性组合物含有交联的聚（二有机硅氧烷）和增强的沉淀二氧化硅，其以无涂层和无浸剂的形式具有约220至约340平方米/克的表面积，体积孔的最大孔径尺寸分布函数为约9至约20纳米，总入侵体积为约2.6至约4.4立方厘米/克。

10. 发明授权

US5236680A Preparation of amorphous silica-alumina particles by acid-treating spherical P-type zeolite particles crystallized from a sodium aluminosilicate gel 失效
标题翻译：通过酸处理由硅铝酸钠凝胶结晶的球形P型沸石颗粒制备无定形二氧化硅 - 氧化铝颗粒
公开(公告)号：US5236680A
公开(公告)日：1993-08-17
申请号：US716905
申请日：1991-06-18
申请人： Tadahisa Nakazawa , Masahide Ogawa , Kiyoshi Abe , Kazuhiko Suzuki , Takashi Tokita , Toshio Ito
发明人： Tadahisa Nakazawa , Masahide Ogawa , Kiyoshi Abe , Kazuhiko Suzuki , Takashi Tokita , Toshio Ito
IPC分类号： A61K8/25 , A61K8/26 , A61Q1/02 , C01B33/187 , C01B39/28 , C08K7/18 , C09C1/30 , C09C1/40 , C10M171/00
CPC分类号： A61K8/26 , A61K8/25 , A61Q1/02 , C01B33/187 , C01B39/28 , C08K7/18 , C09C1/30 , C09C1/405 , C10M171/001 , A61K2800/43 , C01P2002/02 , C01P2002/72 , C01P2002/82 , C01P2004/03 , C01P2004/32 , C01P2004/50 , C01P2004/51 , C01P2004/52 , C01P2004/61 , C01P2004/62 , C01P2004/82 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/19 , C01P2006/60 , C01P2006/80 , C01P2006/82 , C01P2006/90
摘要： The invention is a process for preparing amorphous silica alumina spherical particles by mixing sodium silicate or silicic acid gel with sodium aluminate and sodium hydroxide in an aqueous solution to form a gel, homogenizing the formed gel, crystallizing this intermediate product at 85.degree. C. to 200.degree. under atmospheric pressure or under hydrothermal conditions to form spherical zeolite particles with an x-ray diffraction pattern inherent to P-type zeolites and with a notched surface, treating the zeolite particles with acid to remove the sodium, thereby rendering the particles amorphous.
摘要翻译：本发明是一种通过在水溶液中将硅酸钠或硅酸凝胶与铝酸钠和氢氧化钠混合以形成凝胶来制备无定形二氧化硅氧化铝球形颗粒的方法，使形成的凝胶均质化，将该中间产物在85℃下结晶至在大气压下或在水热条件下200°以形成具有P型沸石固有的x射线衍射图案和缺口表面的球形沸石颗粒，用酸处理沸石颗粒以除去钠，从而使颗粒无定形。

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