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81. 发明授权

US4440670A Method of synthesizing high surface area unagglomerated noble metal pyrochlore compounds 失效
标题翻译：合成高表面积聚集的贵金属烧绿石化合物的方法
公开(公告)号：US4440670A
公开(公告)日：1984-04-03
申请号：US430237
申请日：1982-09-30
申请人： Harold S. Horowitz , Joseph T. Lewandowski
发明人： Harold S. Horowitz , Joseph T. Lewandowski
IPC分类号： C01G21/00 , B01J23/00 , C01G29/00 , C01G55/00 , H01B1/08
CPC分类号： C01G55/00
摘要： A method of preparing electrically conductive pyrochlore compounds of high surface area and unagglomerated form, having the formulaA.sub.2 [B.sub.2-x A.sub.x ]O.sub.7-yis disclosed wherein A is selected from lead, bismuth and mixtures thereof, B is selected from ruthenium, iridium and mixtures thereof, 0
摘要翻译：公开了一种制备具有式A2 [B2-xAx] O7-y的高表面积和非聚集形式的导电烧绿石化合物的方法，其中A选自铅，铋及其混合物，B选自钌，铱和其混合物，0

82. 发明授权

US4434240A Recovery of noble metal values from carbonylation residues 失效
标题翻译：从羰基化残留物中回收贵金属价值
公开(公告)号：US4434240A
公开(公告)日：1984-02-28
申请号：US321362
申请日：1981-11-16
申请人： Joseph Pugach
发明人： Joseph Pugach
IPC分类号： C22B11/00 , B01J23/96 , B01J27/28 , B01J31/40 , B01J38/00 , C01G1/04 , C01G55/00 , C07C45/00 , C07C45/50 , C07C51/00 , C07C51/56 , C07C51/573 , C07C53/12 , C07C67/00 , C07C67/37 , C07C69/16 , C07C51/10
CPC分类号： B01J31/4046 , B01J31/20 , B01J31/26 , B01J31/4038 , C22B11/048 , B01J2231/34 , B01J2531/82 , B01J2531/822 , B01J27/08 , B01J27/10 , B01J31/146 , Y02P10/214
摘要： Heavy residues produced by noble metal catalyzed carbonylation reactions and containing Group VIII noble metals, particularly rhodium, are treated with reagents to precipitate solids containing substantially all of the noble metal contained in the residues. The solids may be further treated to recover the noble metals or they may be returned directly for reuse in the carbonylation reaction. Suitable reagents include alkali metal hydroxides, alkali metal peroxides, alkali metal borohydrides, and other reducing agents, such as formaldehyde and acidified sodium bisulfite.
摘要翻译：通过贵金属催化的羰基化反应产生的含有VIII族贵金属，特别是铑的重残余物用试剂处理以沉淀含有残留物中所含的基本上所有贵金属的固体。可以进一步处理固体以回收贵金属，或者它们可以直接返回以在羰基化反应中重新使用。合适的试剂包括碱金属氢氧化物，碱金属过氧化物，碱金属硼氢化物和其它还原剂，如甲醛和酸化的亚硫酸氢钠。

83. 再颁专利

USRE31437E Resistance material 失效
公开(公告)号：USRE31437E
公开(公告)日：1983-11-01
申请号：US399052
申请日：1982-07-16
申请人： Alexander H. Boonstra , Cornelis A. H. A. Mutsaers , Franciscus N. G. R. van der Kruijs
发明人： Alexander H. Boonstra , Cornelis A. H. A. Mutsaers , Franciscus N. G. R. van der Kruijs
IPC分类号： H01C7/00 , C01G55/00 , H01B1/06 , H01C7/02 , H01C7/04 , H01C17/065
CPC分类号： H01C7/043 , H01B1/06 , H01C17/0654 , H01C7/021
摘要： .[.Resistance material consisting of a mixture of metal oxidic compounds, metal oxides, a permanent binder and a temporary binder, the resistance-determining component consisting of barium-rhodate BaRh.sub.6 O.sub.12..]. .Iadd.Resistance material consisting essentially of a mixture of a permanent binder, a temporary binder and, as a resistance determining component, a barium-rhodate of the formula BaRh.sub.6 O.sub.12. .Iaddend.This component has a linear positive temperature coefficient of the resistance (TCR) and enables the production of a resistor having a very low TCR by combining the material with a material having a negative TCR. The resistor is obtained by firing this resistance material after it has been applied onto a substrate.

84. 发明授权

US4413118A Process for removal of homogeneous catalyst group VIII metals from process streams 失效
标题翻译：从工艺流中除去均相催化剂VIII族金属的方法
公开(公告)号：US4413118A
公开(公告)日：1983-11-01
申请号：US239726
申请日：1981-03-02
申请人： F. Edward Roberts , Victor J. Grenda
发明人： F. Edward Roberts , Victor J. Grenda
IPC分类号： C07H17/08 , A62D3/00 , B01J31/40 , B01J38/00 , C01G55/00 , C07C333/20 , C07F15/00 , C07F15/04 , C22B3/34
CPC分类号： C22B3/0031 , C01G55/00 , C01G55/001 , C07F15/004 , C07F15/0066 , C07F15/045 , Y02P10/234
摘要： Organic sulfur compounds containing a carbon-sulfur double bond are used to remove homogeneous catalyst group VIII metals from chemical process streams.
摘要翻译：含有碳 - 硫双键的有机硫化合物用于从化学工艺流中除去均匀的催化剂VIII族金属。

85. 发明授权

US4340570A Recovery of rhodium from carbonylation residues 失效
标题翻译：从羰基化残基中回收铑
公开(公告)号：US4340570A
公开(公告)日：1982-07-20
申请号：US241181
申请日：1981-03-06
申请人： Walter C. Davidson
发明人： Walter C. Davidson
IPC分类号： C22B11/00 , B01J31/40 , C01G55/00 , C07C51/56 , C22B3/28 , C22B3/32
CPC分类号： B01J31/4046 , B01J31/04 , B01J31/20 , B01J31/2234 , B01J31/2404 , B01J31/26 , B01J31/4038 , C01G55/00 , C01G55/005 , C07C51/56 , C07C67/00 , C07C67/37 , C22B3/0012 , C22B3/0024 , B01J2231/34 , B01J23/40 , B01J2531/82 , B01J2531/822 , B01J27/08 , B01J31/0237 , Y02P10/234 , Y02P20/584
摘要： Residues are formed in the carbonylation of esters or ethers, particularly in the production of acetic anhydride or ethylidene diacetate. Such residues contain noble metal, typically rhodium used as a catalyst, which must be recovered before the residues can be disposed of. In the process of the invention, the rhodium values are freed from the residues by a series of treatments with amines and other reagents, thereby enabling the rhodium to be extracted by subsequent contact with an aqueous halogen acid.
摘要翻译：残留物在酯或醚的羰基化中形成，特别是在制备乙酸酐或亚乙基二乙酸酯时。这种残留物含有贵金属，通常用作催化剂的铑，必须在残留物被处理之前回收。在本发明的方法中，通过用胺和其它试剂进行一系列处理，可以将铑值从残余物中除去，从而使铑能够随后与含卤酸的接触而被萃取。

86. 发明授权

US4340569A Treatment of carbonylation residues 失效
标题翻译：羰基化残留物的处理
公开(公告)号：US4340569A
公开(公告)日：1982-07-20
申请号：US241180
申请日：1981-03-06
申请人： Walter C. Davidson , Richard V. Porcelli
发明人： Walter C. Davidson , Richard V. Porcelli
IPC分类号： C07C69/16 , B01J23/00 , B01J31/40 , B01J38/00 , C01G55/00 , C07B31/00 , C07B41/12 , C07B61/00 , C07C27/00 , C07C45/00 , C07C50/08 , C07C51/00 , C07C51/56 , C07C53/08 , C07C53/12 , C07C67/00 , C07F15/00 , C22B3/26 , C22B3/28
CPC分类号： B01J31/4046 , B01J31/04 , B01J31/20 , B01J31/2234 , B01J31/2404 , B01J31/26 , B01J31/4038 , C01G55/00 , C01G55/001 , C01G55/005 , C07C51/56 , C07C67/36 , C07C67/37 , C22B3/0009 , C22B3/001 , C22B3/0012 , B01J2231/34 , B01J23/40 , B01J2531/82 , B01J2531/822 , B01J27/08 , B01J31/0237 , Y02P10/234 , Y02P20/584
摘要： Residues are formed in the carbonylation of esters or ethers, particularly in the production of acetic anhydride or ethylidene diacetate. When such residues contain noble metal, typically rhodium, used as a catalyst, the noble metals must be recovered before the residues can be disposed of. The metal values are freed from the residues by treatment with amines, thereby enabling the rhodium to be extracted by subsequent contact with an aqueous halogen acid. The residues are pretreated with alkanols and concentrated by evaporation to improve the effect of such amine treatments.
摘要翻译：残留物在酯或醚的羰基化中形成，特别是在制备乙酸酐或亚乙基二乙酸酯时。当这种残留物含有用作催化剂的贵金属（通常为铑）时，贵金属必须在残留物被处理之前被回收。金属值通过用胺处理从残余物中除去，从而使铑通过随后与卤酸水溶液的接触而被萃取。残余物用链烷醇预处理并通过蒸发浓缩以改善这种胺处理的效果。

87. 发明授权

US4335087A Process for preparing cis-Pt(NH.sub.3).sub.2 Cl.sub.2 失效
标题翻译：顺式Pt（NH3）2Cl2的制备方法
公开(公告)号：US4335087A
公开(公告)日：1982-06-15
申请号：US206883
申请日：1980-11-14
申请人： Richard N. Rhoda
发明人： Richard N. Rhoda
IPC分类号： A61K33/24 , C01G55/00
CPC分类号： A61K33/24 , C01G55/002
摘要： A process is provided for preparing cis-Pt(NH.sub.3).sub.2 Cl.sub.2 and intermediates. The cis-Pt(NH.sub.3).sub.2 Cl.sub.2 is provided in high yield and purity.
摘要翻译：提供了制备顺式Pt（NH 3）2 Cl 2和中间体的方法。以高产率和纯度提供顺式Pt（NH 3）2 Cl 2。

88. 发明授权

US4332780A Preparation of cis-diammine diodo platinum (II) 失效
标题翻译：顺式二胺二碘铂（II）的制备
公开(公告)号：US4332780A
公开(公告)日：1982-06-01
申请号：US241946
申请日：1981-03-09
申请人： Richard N. Rhoda , Jeffrey N. Crosby
发明人： Richard N. Rhoda , Jeffrey N. Crosby
IPC分类号： A61K33/24 , C01G55/00
CPC分类号： C01G55/002 , A61K33/24 , C01P2006/60
摘要： A process for preparing cis - Pt (NH.sub.3).sub.2 I.sub.2 from K.sub.2 PtI.sub.4 by adding NH.sub.4 OH under controlled conditions of temperature and pH.
摘要翻译：通过在温度和pH值的控制条件下加入NH 4 OH，从K2PtI4制备顺式 - （NH3）2I2的方法。

89. 发明授权

US4329321A Method for the recovery of salts of group VIII noble metals from solutions 失效
标题翻译：从溶液中回收第VIII族贵金属盐的方法
公开(公告)号：US4329321A
公开(公告)日：1982-05-11
申请号：US195972
申请日：1980-10-10
申请人： Augustine I. Dalton, Jr. , Ronald W. Skinner
发明人： Augustine I. Dalton, Jr. , Ronald W. Skinner
IPC分类号： B01J20/20 , C01B31/08 , C01G55/00 , C22B11/00
CPC分类号： C22B11/04 , C01G55/001 , C22B3/24 , Y02P10/234
摘要： Salts of Group VIII noble metals are recovered from neutral or acidic solutions by admixing with the solution up to 10% by weight of hydrogen peroxide, adsorbing the salt of the Group VIII noble metal from the peroxide-containing solution on activated carbon and separating activated carbon containing the adsorbed Group VIII noble metal salts from solution diminished in concentration thereof.
摘要翻译：将VIII族贵金属的盐从中性或酸性溶液中回收，与溶液最多混合10％（重量）的过氧化氢，将含有过氧化物的溶液中的第Ⅷ族贵金属的盐吸附在活性炭上并分离活性炭含有来自溶液的吸附的VIII族贵金属盐的浓度降低。

90. 发明授权

US4311770A Novel ferromagnetic chromium dioxide and rhodium dioxide material and its preparation 失效
标题翻译：新型铁磁二氧化铬和二氧化铑材料及其制备
公开(公告)号：US4311770A
公开(公告)日：1982-01-19
申请号：US945007
申请日：1978-09-22
申请人： Gerard Demazeau , Patrick Maestro , Theophile Plante , Michel Pouchard , Paul Hagenmuller
发明人： Gerard Demazeau , Patrick Maestro , Theophile Plante , Michel Pouchard , Paul Hagenmuller
IPC分类号： C01G37/02 , C01G55/00 , G11B5/706 , C01G37/027
CPC分类号： C01G55/00 , C01G37/02 , G11B5/70636 , C01P2002/54 , C01P2006/42
摘要： Process for making a novel ferromagnetic chromium dioxide and rhodium dioxide material in the form of a solid solution Cr.sub.1-x Rh.sub.x O.sub.2 where x is a number between 0 and 0.5.It essentially comprises oxidation, under suitable conditions of temperature and pressure, of hydrated or anhydrous Cr.sub.2 O.sub.3 or of a precursor of Cr.sub.2 O.sub.3, in the presence of (1) an appropriate amount of a compound of rhodium III able to give RhO.sub.2 under reaction conditions and (2) of an oxidizing agent consisting of an oxygenated compound free from metallic cations other than chromium and having, under the reaction conditions, a partial oxygen pressure at least equal to that corresponding, under the same conditions of temperature and pressure, to the equilibria Cr.sub.2 O.sub.3 +1/2O.sub.2 .revreaction.2CrO.sub.2 and Rh.sub.2 O.sub.3 +1/2O.sub.2 .revreaction.2RhO.sub.2 as well as eventually (3) of dilution water and/or of at least an additional doping agent acting as buffer in the reaction medium and/or a conventional modifying agent.The invention is useful for the manufacture of a ferromagnetic material possessing improved magnetic characteristics.
摘要翻译：制备以固溶Cr1-xRhxO2形式的新型铁磁二氧化铬和二氧化铑材料的方法，其中x为0至0.5之间的数字。它主要包括在合适的温度和压力条件下，在（1）适当量的能够在反应条件下产生RhO 2的铑III化合物的存在下，在水合或无水的Cr 2 O 3或Cr 2 O 3的前体下， 2）氧化剂，其由不含铬的金属阳离子的氧化化合物组成，并且在反应条件下，在相同的温度和压力条件下，至少等于相应的温度和压力条件下的部分氧气压力与平衡Cr 2 O 3 + 1 / 2O2 - > < - 2CrO2和Rh2O3 + 1 / 2O2 - > < - 2RhO2以及最终（3）稀释水和/或至少一种作为反应介质中缓冲液的附加掺杂剂和/或常规改性剂。本发明对于制造具有改进的磁特性的铁磁材料是有用的。

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