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    • 2. 发明授权
    • Polyunsaturated fatty acid monovalent and divalent metal salt synthesis
    • 多不饱和脂肪酸一价和二价金属盐合成
    • US07820842B2
    • 2010-10-26
    • US10598681
    • 2005-04-29
    • Daniel Nestor LuchiniGeorge K. StrohmaierEiler D. FrederiksenJames G. HawkesBob J. Dull
    • Daniel Nestor LuchiniGeorge K. StrohmaierEiler D. FrederiksenJames G. HawkesBob J. Dull
    • C07C51/00
    • C11C1/00A23D9/00A23K20/158A23K20/24A23K50/40A23L33/12Y10S426/807
    • Disclosed herein are methods for the preparation of a free-flowing, storage-stable fatty acid metal salt product by forming a reactive admixture comprising (a) an unsaturated fatty acid glyceride feedstock; and (b) from about 1 mol to about 3 mol of at least one monovalent metal hydroxide or at least one divalent metal hydroxide; and heating the admixture to a temperature at which said fatty acid glycerides saponify to form fatty acid metals salts; wherein said monovalent metal is potassium; and wherein said divalent metal is selected from the group consisting of calcium, copper, magnesium and zinc. The fatty acid glycerides may be saponified in an atmosphere in which the partial pressure of oxygen has been reduced by an amount effective to provide an improvement in storage stability until a free-flowing, storage-stage product is obtained, or prior to saponification, the fatty acid glycerides may blended with a stabilizing oil that promotes storage stability, or both. Storage stable metal salts of unsaturated fatty acids prepared by the inventive methods are also disclosed.
    • 本文公开了通过形成包含(a)不饱和脂肪酸甘油酯原料的反应性混合物来制备自由流动的储存稳定的脂肪酸金属盐产物的方法; 和(b)约1mol至约3mol的至少一种一价金属氢氧化物或至少一种二价金属氢氧化物; 并将所述混合物加热至所述脂肪酸甘油酯皂化以形成脂肪酸金属盐的温度; 其中所述一价金属是钾; 并且其中所述二价金属选自钙,铜,镁和锌。 脂肪酸甘油酯可以在氧气分压降低的气氛中被皂化,以有效提高储存稳定性,直到获得自由流动的储存阶段产物,或在皂化之前, 脂肪酸甘油酯可以与促进保存稳定性的稳定油或两者混合。 还公开了通过本发明方法制备的不稳定的不饱和脂肪酸的储存稳定金属盐。
    • 5. 发明授权
    • Treated peppers products having capsaicinoids removed
    • 处理含有辣椒素的辣椒制品
    • US6123970A
    • 2000-09-26
    • US869182
    • 1997-06-04
    • Bob J. Dull
    • Bob J. Dull
    • A23L5/20A23L19/00A23L27/10A23L1/211
    • A23L27/11A23L19/03A23L5/23A23V2002/00
    • A method is described for removing capsaicinoids from a pepper whereby the pepper's placental membrane is exposed to an oil. Preferably, the pepper or peppers will be cut in sizes ranging from minced to longitudinal cuts to expose and rupture the placental membrane, allowing an oil to contact and solubilize the capsaicinoids. In the preferred embodiment, the peppers are minced and placed in a heated edible oil. The edible oil pepper mixture is then agitated at a mixing speed tip velocity of between about 30 feet/minute and about 270 feet/minute. The peppers are then removed from the edible oil and rinsed to remove excess edible oil from the peppers. The method permits extraction of the capsaicinoids, while maintaining the peppers' natural flavor, texture, and color. The edible oil will include oils where the acyl groups are saturated fatty acids, unsaturated fatty acids, or a combination of saturated fatty acids and unsaturated fatty acids, with the most preferred edible oil being a vegetable oil.
    • 描述了从胡椒中除去辣椒素的方法,由此将辣椒的胎盘膜暴露于油中。 优选地,胡椒或辣椒将被切割成从小切割到纵向切割的尺寸,以暴露和破裂胎盘膜,允许油接触和溶解辣椒素。 在优选的实施方案中,将辣椒切碎并置于加热的食用油中。 然后将食用油胡椒混合物以约30英尺/分钟至约270英尺/分钟的混合速度尖端速度搅拌。 然后将辣椒从食用油中取出并漂洗以从辣椒中除去多余的食用油。 该方法允许提取辣椒素,同时保持辣椒的天然风味,质地和颜色。 食用油将包括其中酰基是饱和脂肪酸,不饱和脂肪酸或饱和脂肪酸和不饱和脂肪酸的组合的油,最优选的食用油是植物油。
    • 6. 发明授权
    • Method for removal of capsaicinoids from peppers
    • 从辣椒去除辣椒素的方法
    • US5714192A
    • 1998-02-03
    • US631831
    • 1996-04-10
    • Bob J. DullDavid J. DominguesThomas E. Heinzen
    • Bob J. DullDavid J. DominguesThomas E. Heinzen
    • A23L5/20A23L19/00A23L27/10A23L1/211
    • A23L27/11A23L19/03A23L5/23A23V2002/00
    • A method is described for removing capsaicinoids from a pepper whereby the pepper's placental membrane is exposed to an aqueous solution. Preferably, the pepper or peppers will be cut in sizes ranging from minced to longitudinal cuts to expose and rupture the placental membrane, allowing an aqueous solution to contact, physically wash, and solubilize the capsaicinoids. In the preferred embodiment, the peppers are minced and placed in a heated aqueous solution. The aqueous solution pepper mixture is then agitated at a mixing speed tip velocity of between about 30 feet/minute and about 270 feet/minute. The peppers are then removed from the aqueous solution and rinsed to remove excess aqueous solution from the peppers. The method permits extraction of the capsaicinoids, while maintaining the peppers' natural flavor, texture, and color.
    • 描述了从胡椒中除去辣椒素的方法,由此胡椒的胎盘膜暴露于水溶液中。 优选地,胡椒或辣椒将被切割成从切片到纵向切割的尺寸,以暴露和破裂胎盘膜,允许水溶液接触,物理洗涤和溶解辣椒素。 在优选的实施方案中,将辣椒切碎并置于加热的水溶液中。 然后将水溶液胡椒混合物以约30英尺/分钟至约270英尺/分钟的混合速度尖端速度搅拌。 然后从水溶液中除去胡椒并冲洗以从辣椒中除去过量的水溶液。 该方法允许提取辣椒素,同时保持辣椒的天然风味,质地和颜色。
    • 9. 发明申请
    • Method for Producing Sweet Bran and the Resultant Product
    • 生产甜麸和产品的方法
    • US20140370151A1
    • 2014-12-18
    • US14302001
    • 2014-06-11
    • Bob J. Dull
    • Bob J. Dull
    • A23L1/10A23L1/105
    • A23L7/115A23K10/37A23L7/107Y02P60/877
    • Provided herein is a method for treating untreated rice bran to produce a treated rice bran. The method comprises inactivating lipase in the untreated rice bran, saponifying the fatty acids in the untreated rice bran to fatty acid salts, and contacting the untreated rice bran with a source of bisulfite anions so that an aldehyde or ketone in the untreated rice bran forms an organosulfite. The method produces the treated rice bran, wherein the amount and characterization of protein and fiber between the treated rice bran and the untreated rice bran remain unchanged. A treated rice bran composition is also provided, which comprises fatty acid salts, inactivated lipase, organosulfites, between about 14% and about 16% by weight protein, and between about 8% and about 10% by weight fiber.
    • 本文提供了一种处理未经处理的米糠以生产经处理的米糠的方法。 该方法包括使未处理的米糠中的脂肪酶失活,将未处理的米糠中的脂肪酸皂化成脂肪酸盐,并将未处理的米糠与亚硫酸氢盐阴离子接触,使得未处理的米糠中的醛或酮形成 有机亚硫酸盐 该方法生产经处理的米糠,其中经处理的米糠和未处理的米糠之间的蛋白质和纤维的量和表征保持不变。 还提供了处理的米糠组合物,其包含脂肪酸盐,灭活的脂肪酶,有机亚硫酸盐,约14重量%至约16重量%的蛋白质和约8重量%至约10重量%的纤维。