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1. 发明申请

US20100130391A1 PREPARATION OF STERICALLY HINDERED HYDROXYPHENYLCARBOXYLIC ACID ESTERS 有权
标题翻译：异味羟基苯甲酸酯的制备
公开(公告)号：US20100130391A1
公开(公告)日：2010-05-27
申请号：US12693685
申请日：2010-01-26
申请人： Vincent J. Gatto , Hassan Y. Elnagar , Chi Hung Cheng , J. Robert Adams
发明人： Vincent J. Gatto , Hassan Y. Elnagar , Chi Hung Cheng , J. Robert Adams
IPC分类号： C09K15/08 , C07C69/76 , C11D3/16 , C10M129/28 , C10M137/10
CPC分类号： C10M177/00 , C07C67/03 , C07C67/347 , C07C67/60 , C09K15/08 , C10M129/76 , C10M2207/026 , C10M2207/289 , C10N2230/10 , C10N2270/00 , C07C69/732
摘要： A novel manufacturing process is described for producing hindered phenolic alkyl esters, which may be useful as antioxidants. This process simplifies catalyst neutralization and removal during the preparation of hindered phenolic esters. Compositions that comprise the hindered phenolic esters produced according to these methods are also described.
摘要翻译：描述了用于制备受阻酚烷基酯的新颖的制造方法，其可用作抗氧化剂。该方法简化了在制备受阻酚酯期间的催化剂中和和去除。还描述了包含根据这些方法制备的受阻酚酯的组合物。

2. 发明授权

US5965781A Catalysis in halogen exchange reactions 失效
公开(公告)号：US5965781A
公开(公告)日：1999-10-12
申请号：US975924
申请日：1997-11-21
申请人： Bruce C. Berris , Chi-Hung Cheng
发明人： Bruce C. Berris , Chi-Hung Cheng
IPC分类号： C07C17/20 , C07C25/13 , C07F9/02 , C07F9/06 , C07F9/54
CPC分类号： C07F9/06 , C07C17/208 , C07F9/025
摘要： Impure tetra(dihydrocarbylamino)phosphonium halide is contacted with a liquid cyclic ether to dissolve the phosphonium halide and leave at least a portion of the impurities comprising at least quaternary ammonium halide or an amidophosphoxide remaining in the solid state. The solids and the liquid phase are separated from each other, an anhydrous non-solvent for the tetra(dihydrocarbylamino)phosphonium halide is mixed with the separated liquid phase to precipitate the tetra(dihydrocarbylamino)phosphonium halide, which is then separated from the liquid phase. The so-treated tetra(dihydrocarbylamino)phosphonium halide is more efficient as a catalyst for halogen exchange reactions than the original untreated tetra(dihydrocarbylamino)phosphonium halide.

3. 发明授权

US07988884B2 Preparation of sterically hindered hydroxyphenylcarboxylic acid esters 有权
标题翻译：空间位阻羟基苯基羧酸酯的制备
公开(公告)号：US07988884B2
公开(公告)日：2011-08-02
申请号：US12693685
申请日：2010-01-26
申请人： Vincent J. Gatto , Hassan Y Elnagar , Chi Hung Cheng , J. Robert Adams
发明人： Vincent J. Gatto , Hassan Y Elnagar , Chi Hung Cheng , J. Robert Adams
IPC分类号： C10M137/10 , C08K5/01 , C09K15/06 , C11D1/00 , C07C69/76 , C07C69/00
CPC分类号： C10M177/00 , C07C67/03 , C07C67/347 , C07C67/60 , C09K15/08 , C10M129/76 , C10M2207/026 , C10M2207/289 , C10N2230/10 , C10N2270/00 , C07C69/732
摘要： A novel manufacturing process is described for producing hindered phenolic alkyl esters, which may be useful as antioxidants. This process simplifies catalyst neutralization and removal during the preparation of hindered phenolic esters. Compositions that comprise the hindered phenolic esters produced according to these methods are also described.
摘要翻译：描述了用于制备受阻酚烷基酯的新颖的制造方法，其可用作抗氧化剂。该方法简化了在制备受阻酚酯期间的催化剂中和和去除。还描述了包含根据这些方法制备的受阻酚酯的组合物。

4. 发明申请

US20080166741A1 Method for Diagnosing Membranous Glomerulonephritis Disease and a Kit Thereof 审中-公开
标题翻译：诊断膜性肾小球肾炎的方法及其试剂盒
公开(公告)号：US20080166741A1
公开(公告)日：2008-07-10
申请号：US11620064
申请日：2007-01-05
申请人： Tzu-Ling Tseng , Pei-Hsiu Liao , Ping-Fu Cheng , Chi-Hung Cheng
发明人： Tzu-Ling Tseng , Pei-Hsiu Liao , Ping-Fu Cheng , Chi-Hung Cheng
IPC分类号： G01N33/53 , G01N33/00
CPC分类号： G01N33/564 , G01N2800/347
摘要： Some specific autoantigens of MGN are discovered by using the integrated platform. Moreover, according to the specificity between antibodies and antigens, a method for diagnosing MGN are constructed. This diagnostic method is cooperated with ELISA, RIA, immunofluorescence, or other immunochromatography techniques. Finally, a diagnostic kit is provided to implement the method above.
摘要翻译：通过使用集成平台发现MGN的一些特定自身抗原。此外，根据抗体和抗原的特异性，构建了用于诊断MGN的方法。该诊断方法与ELISA，RIA，免疫荧光或其他免疫色谱技术相结合。最后，提供诊断套件来实现上述方法。

5. 发明授权

US06528665B1 Preventing undesired odor in and/or purifying alkanediols 失效
标题翻译：预防烷基二醇中和/或纯化不良气味
公开(公告)号：US06528665B1
公开(公告)日：2003-03-04
申请号：US10116482
申请日：2002-04-03
申请人： Chi Hung Cheng , Gerald M. Sulzer , John F. Balhoff
发明人： Chi Hung Cheng , Gerald M. Sulzer , John F. Balhoff
IPC分类号： C07D30132
CPC分类号： C07D301/12 , C07C29/106 , C07D301/32 , Y02P20/127 , C07C31/20
摘要： Epoxyalkanes are subjected to at least one of the following washing operations: (1) washing with aqueous inorganic base, and then with aqueous borohydride, or vice versa; or (2) washing with an aqueous solution of both inorganic base and borohydride. Undesirable odor is reduced or eliminated from alkanediol(s), if produced from the treated epoxyalkane(s) by hydrolysis. Use of such washing procedures in the production of alkanediols is also described.
摘要翻译：对环氧烷烃进行以下洗涤操作中的至少一种：（1）用无机碱水溶液洗涤，然后用硼氢化钠洗涤，反之亦然; 或（2）用无机碱和硼氢化钠的水溶液洗涤。如果通过水解由经处理的环氧烷烃生产，则从链烷二醇中减少或消除不希望的气味。还描述了在制备链烷二醇中使用这种洗涤方法。

6. 发明授权

US06525208B1 Epoxidation of olefins 失效
标题翻译：烯烃环氧化
公开(公告)号：US06525208B1
公开(公告)日：2003-02-25
申请号：US10116508
申请日：2002-04-03
申请人： Chi Hung Cheng , Gerald M. Sulzer
发明人： Chi Hung Cheng , Gerald M. Sulzer
IPC分类号： C07D30112
CPC分类号： C07D301/12
摘要： Mixed together are (i) hydrogen peroxide; (ii) 1-alkene; (iii) quaternary ammonium salt wherein at least one of the substituents contains at least six carbon atoms; (iv) boric acid, or both a 1,2-diol and boric acid; and (v) a preformed catalyst solution formed from hydrogen peroxide, at least one aqueous inorganic acid, and at least one tungstate salt, while water is continuously removed, such that a 1,2-epoxide is formed. A new method for purifying 1,2-epoxyalkanes is also described.
摘要翻译：混合在一起是（i）过氧化氢; （ii）1-烯烃; （iii）季铵盐，其中至少一个取代基含有至少6个碳原子; （iv）硼酸，或1,2-二醇和硼酸; 和（v）由过氧化氢，至少一种含水无机酸和至少一种钨酸盐形成的预成型催化剂溶液，同时连续除去水，从而形成1,2-环氧化物。还描述了用于纯化1,2-环氧烷烃的新方法。

7. 发明授权

US6046358A Catalysis in halogen exchange reactions 失效
标题翻译：卤素交换反应中的催化
公开(公告)号：US6046358A
公开(公告)日：2000-04-04
申请号：US351888
申请日：1999-07-13
申请人： Bruce C. Berris , Chi-Hung Cheng
发明人： Bruce C. Berris , Chi-Hung Cheng
IPC分类号： C07C17/20 , C07C25/13 , C07F9/02 , C07F9/06 , C07F9/54
CPC分类号： C07F9/06 , C07C17/208 , C07F9/025
摘要： Impure tetra(dihydrocarbylamino)phosphonium halide is contacted with a liquid cyclic ether to dissolve the phosphonium halide and leave at least a portion of the impurities comprising at least quaternary ammonium halide or an amidophosphoxide remaining in the solid state. The solids and the liquid phase are separated from each other, an anhydrous non-solvent for the tetra(dihydrocarbylamino)phosphonium halide is mixed with the separated liquid phase to precipitate the tetra(dihydrocarbylamino)phosphonium halide, which is then separated from the liquid phase. The so-treated tetra(dihydrocarbylamino)phosphonium halide is more efficient as a catalyst for halogen exchange reactions than the original untreated tetra(dihydrocarbylamino)phosphonium halide.
摘要翻译：不纯的四（二烃基氨基）鏻卤化物与液体环状醚接触以溶解卤化鏻，并使至少一部分杂质至少包含季铵卤化物或酰胺二氧化物保持在固态。将固体和液相彼此分离，用于四（二烃基氨基）鏻卤化物的无水非溶剂与分离的液相混合以沉淀四（二烃基氨基）鏻卤化物，然后将其从液相中分离出来。如此处理的四（二烃基氨基）鏻卤化物作为卤素交换反应的催化剂比原始未处理的四（二烃基氨基）鏻卤化物更有效。

8. 发明授权

US5884523A Scoop with a counter 失效
标题翻译：舀一个柜台
公开(公告)号：US5884523A
公开(公告)日：1999-03-23
申请号：US120305
申请日：1998-07-22
申请人： Jung-kuang Cheng , Chi-hung Cheng
发明人： Jung-kuang Cheng , Chi-hung Cheng
IPC分类号： G01F19/00 , G02F19/00
CPC分类号： G01F19/002
摘要： A scoop with a counter for powder material includes a scooping cup with a handle and a pusher that can slide to and fro on the handle of the scoop. On the front end of the pusher is a cover ring and on the rear end of the pusher is a top plate. At the end of the handle of the scooping cup is fitted a housing that is composed of a left casing and a right casing. On each casing there is a window and inside the casings is fitted a counter ratchet. A digit frame in a ring arrangement is attached to both sides of the counter ratchet. On the lower part of the housing is an opening so a toothed side of the counter ratchet is exposed to facilitate resetting adjustment. Also in the housing and at the toothed side of the counter ratchet is a flexible fixing plate to fix the counter ratchet. In operation, the pusher may be slid across the scooping cup where the cover ring at the front end of the pusher will level the powder material in the scooping cup to obtain a constant quantity of powder material. When the pusher is slid back, the top plate at the rear of the pusher will push and turn the counter ratchet which will then turn the next digit of the digit frame to count scooping frequency.
摘要翻译：具有用于粉末材料的计数器的勺子包括具有手柄的舀取杯和可在勺子的手柄上来回滑动的推动器。在推动器的前端是一个盖环，并且推动器的后端是顶板。在舀杯的手柄的末端装有由左壳体和右壳体组成的壳体。在每个外壳上都有一个窗户，里面的外壳里装有一个反棘轮。环形布置中的数字框架连接到计数棘轮的两侧。在壳体的下部是开口，因此反向棘轮的齿面被暴露以便于复位调整。另外在壳体中，在棘轮棘齿的齿形侧是用于固定反棘轮的柔性固定板。在操作中，推动器可以滑动穿过舀杯，其中推动器前端处的盖环将使舀杯中的粉末材料平整以获得恒定量的粉末材料。当推动器滑动时，推动器后部的顶板将推动并转动副棘爪，然后转动数字框的下一位数以计数舀取频率。

9. 发明授权

US5871667A Inhibiting ferrous metal corrosion by aqueous ammoniate solutions 失效
标题翻译：用氨水溶液抑制黑色金属腐蚀
公开(公告)号：US5871667A
公开(公告)日：1999-02-16
申请号：US786536
申请日：1997-01-21
申请人： Chi Hung Cheng , Gerald M. Sulzer
发明人： Chi Hung Cheng , Gerald M. Sulzer
IPC分类号： C07F9/22 , C23F11/06 , C01C1/16 , C01C1/28
CPC分类号： C07F9/224 , C23F11/06
摘要： Aqueous ammoniate solutions made during the manufacture of N-hydrocarbyl thiophosphoric triamides, consisting essentially of aqueous solutions of ammonium chloride and ammonia containing a water-soluble impurity normally tending to engender corrosion of ferrous metal are rendered corrosion-resistant by dissolving therein a small corrosion-inhibiting amount (e.g., up to about 5000 ppm (wt/wt) of a water-soluble salt or oxide of zinc, aluminum, arsenic, antimony or bismuth.
摘要翻译：在制造N-烃基硫代磷酸三酰胺期间制备的氨水溶液，其基本上由氯化铵的水溶液和含有通常倾向于引起黑色金属腐蚀的水溶性杂质的氨制成耐腐蚀性，抑制量（例如，高达约5000ppm（wt / wt）的锌，铝，砷，锑或铋的水溶性盐或氧化物。

10. 发明授权

US5770771A Preparation of N-hydrocarbylthiophosphoric triamides 失效
标题翻译： N-烃基硫代磷酸三酰胺的制备
公开(公告)号：US5770771A
公开(公告)日：1998-06-23
申请号：US786396
申请日：1997-01-21
申请人： Gerald M. Sulzer , Chi Hung Cheng , W. Dirk Klobucar , Charles H. Kolich
发明人： Gerald M. Sulzer , Chi Hung Cheng , W. Dirk Klobucar , Charles H. Kolich
IPC分类号： C01C1/16 , C07F9/02 , C07F9/22 , C07F9/26
CPC分类号： C01C1/164 , C07F9/025 , C07F9/224 , C07F9/26
摘要： Continuously fed to and mixed in a first reactor are (i) a preformed mixture of primary hydrocarbyl monoamine, tertiary amine and liquid inert organic solvent, and (ii) thiophosphoryl chloride while removing heat of reaction to maintain the reaction temperature in the range of about -20.degree. C. to about +50.degree. C. A reaction mixture containing N-hydrocarbylaminothiophosphoryl dichloride is formed. Ammonia and an effluent stream from the first reactor are continuously fed to and mixed in a second reactor in proportions of at least about 16 moles, of ammonia per mole of N-hydrocarbylaminothiophosphoryl dichloride that produce a reaction mixture containing N-hydrocarbylthiophosphoric triamide, and that keep in solution ammonium chloride co-product formed in the reaction. Heat of reaction is removed so that the temperature is high enough to keep ammonium chloride-ammonia complex from forming a solid phase in this reaction mixture, but low enough to avoid significant reduction in yield of N-hydrocarbylthiophosphoric triamide being formed. Effluent is withdrawn from the second reactor so as to maintain a substantially constant volume of reaction mixture in the second reactor. The process eliminates a difficult filtration of the co-product ammonium chloride formed in the second reaction. Also, it possible to accomplish this in a continuous process, with improved efficiency in large scale production of the N-hydrocarbylthiophosphoric triamides. Moreover, the ammonium chloride can be readily converted in the process to an industrially useful liquid co-product mixture.
摘要翻译：连续进料并混合在第一反应器中的是（i）主要烃基单胺，叔胺和液体惰性有机溶剂的预制混合物，和（ii）硫代磷酰氯，同时除去反应热，将反应温度保持在约 -20℃至约+ 50℃。形成含有N-烃基氨基硫代磷酰基二氯化物的反应混合物。将氨和来自第一反应器的流出物流连续地进料至第二反应器中，其比例为至少约16摩尔，每摩尔N-烃基氨基硫代磷酰二氯的氨，其产生含有N-烃基硫代磷酰三酰胺的反应混合物，并且保持反应中形成的溶液中氯化铵共同产物。去除反应热，使得温度足够高以使氯化铵 - 氨络合物在该反应混合物中形成固相，但足够低以避免形成的N-烃基硫代磷酰三酰胺的产率显着降低。将废水从第二反应器中排出，以便在第二反应器中维持反应混合物体积基本恒定。该方法消除了在第二反应中形成的副产物氯化铵的难以过滤。此外，可以在连续的方法中实现这一点，提高N-烃基硫代磷酸三酰胺的大规模生产的效率。此外，氯化铵可以在工艺中容易地转化成工业上有用的液体共产物混合物。

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