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1. 发明授权

US08084650B2 Adamantane derivative, resin composition containing same, and optoelectronic member and sealing agent for electronic circuit using those 有权
标题翻译：金刚烷衍生物，含有它的树脂组合物，以及光电元件和使用这些的电子电路密封剂
公开(公告)号：US08084650B2
公开(公告)日：2011-12-27
申请号：US12160534
申请日：2007-01-19
申请人： Yasunari Okada , Hajime Ito , Hideki Yamane , Nobuaki Matsumoto
发明人： Yasunari Okada , Hajime Ito , Hideki Yamane , Nobuaki Matsumoto
IPC分类号： C07C39/17 , C08L63/00 , B32B27/38
CPC分类号： C07C39/17 , C07C37/16 , C07C37/20 , C07C2603/74 , C07D301/28 , C07D303/30 , C08G59/24 , C08G59/4215 , C08G59/4223 , C08G59/621 , G03F7/038 , Y10T428/1073 , Y10T428/31511
摘要： Disclosed is an adamantane derivative which provides a cured product excellent in optical characteristics such as transparency and light resistance, long-term heat resistance, electrical characteristics such as and dielectric constant, and low water absorption. Also disclosed are a resin composition containing the adamantane derivative, a sealing agent for electronic circuits, optical electronic member, semiconductor device and copper-clad laminate all using the resin composition, and a radiation-sensitive resin composition which contains the above-mentioned adamantane derivative as a crosslinking agent. Specifically disclosed are an adamantane derivative represented by the formula (I-1) below, a resin composition containing the adamantane derivative, a sealing agent for electronic circuits, optical electronic member, semiconductor device and copper-clad laminate, all using the resin composition, and a radiation-sensitive resin composition which contains the above-mentioned adamantane derivative as a crosslinking agent.
摘要翻译：公开了一种金刚烷衍生物，其提供了透光性，耐光性，长期耐热性，电特性如介电常数，低吸水性等光学特性优异的固化物。还公开了含有金刚烷衍生物，电子电路用密封剂，光电子元件，半导体器件和覆铜层压板的树脂组合物，其全部使用该树脂组合物，以及含有上述金刚烷衍生物的辐射敏感性树脂组合物作为交联剂。具体公开了以下式（I-1）表示的金刚烷衍生物，含有金刚烷衍生物的树脂组合物，电子电路用密封剂，光电子部件，半导体装置和覆铜层压板，全部使用树脂组合物，以及含有上述金刚烷衍生物作为交联剂的辐射敏感性树脂组合物。

2. 发明授权

US08017800B2 Adamantyl group-containing epoxy-modified (meth)acrylate and resin composition containing the same 有权
标题翻译：含有金刚烷基的环氧改性（甲基）丙烯酸酯和含有其的树脂组合物
公开(公告)号：US08017800B2
公开(公告)日：2011-09-13
申请号：US12831763
申请日：2010-07-07
申请人： Yasunari Okada , Hajime Ito , Hideki Yamane , Nobuaki Matsumoto
发明人： Yasunari Okada , Hajime Ito , Hideki Yamane , Nobuaki Matsumoto
IPC分类号： C07C69/732
CPC分类号： C08F290/06 , C08F222/1006 , C08F290/061 , C08F290/064 , C08G59/186
摘要： The present invention provides an adamantyl group containing epoxy-modified (meth)acrylate and a resin composition containing it which are imparted by transparency, optical characteristics such as (durable) light resistance and the like, heat-resistance, and good mechanical properties.For example, they are an adamantyl group containing epoxy-modified (meth)acrylate having the following general formula (I) and a composition containing it. In the formula, R1 represents a hydrogen atom or a methyl group, and R2 represents a halogen atom or an aliphatic hydrocarbon group which may contain a hetero atom. Plural R2 may be the same or different, and m represents an integer of 0 to 4 and n represents an integer of 0 or more.
摘要翻译：本发明提供含有环氧改性（甲基）丙烯酸金刚烷基和含有它的树脂组合物，它们由透明性，耐光性等光学特性赋予耐热性和良好的机械性能。例如，它们是含有具有以下通式（I）的环氧改性（甲基）丙烯酸酯和含有它的组合物的金刚烷基。在该式中，R 1表示氢原子或甲基，R 2表示卤素原子或可含有杂原子的脂肪族烃基。多个R2可以相同或不同，m表示0〜4的整数，n表示0以上的整数。

3. 发明授权

US07939682B2 Fluorine-containing adamantane derivative, fluorine-containing adamantane derivative having polymerizable group, and resin composition containing same 失效
标题翻译：含氟金刚烷衍生物，含有聚合性基团的含氟金刚烷衍生物和含有它们的树脂组合物
公开(公告)号：US07939682B2
公开(公告)日：2011-05-10
申请号：US12063685
申请日：2006-08-11
申请人： Yasunari Okada , Hideki Yamane , Nobuaki Matsumoto
发明人： Yasunari Okada , Hideki Yamane , Nobuaki Matsumoto
IPC分类号： C07D493/00
CPC分类号： C07D407/12 , C07C43/196 , C07C69/653 , C07C2603/74 , C07D303/28 , C08F222/1006 , G03F7/0007 , G03F7/091
摘要： Provided are a polymerizable group-containing and fluorine-containing adamantane derivative capable of affording a cured product having good heat resistance, good mechanical properties such as surface hardness and a low refractive index, a resin composition containing such a polymerizable group-containing adamantane derivative, and a fluorine-containing adamantane derivative which is useful as a reaction intermediate used for the production of the polymerizable group-containing and fluorine-containing adamantane derivative. Specifically provided are a fluorine-containing adamantane derivative represented by the general formula (I) below, a polymerizable group-containing and fluorine-containing adamantane derivative represented by the general formula (II) below, and a resin composition containing such a polymerizable group-containing and fluorine-containing adamantane derivative. In the formulas, X1 and X2 each represent OH or NH2, a, b and c each represent an integer of 0 or more and a+b+c≧1, for example a=b=0 and c=1, Z3 represents, for example, —C2H4—, s and t each represent an integer of 1 to 15, u represents an integer of 0 to 14, s+t+u=16, for example s=2, t=14, u=0, and X3 represents, for example, —O—CO—CH═CH2.
摘要翻译：提供能够提供具有良好耐热性，良好机械性能如表面硬度和低折射率的固化产物的含可聚合基团的含氟金刚烷衍生物，含有这种含聚合基团的金刚烷衍生物的树脂组合物，以及可用作制备含聚合基团和含氟金刚烷衍生物的反应中间体的含氟金刚烷衍生物。具体地提供由以下通式（I）表示的含氟金刚烷衍生物，下述通式（II）表示的可聚合基团的含氟金刚烷衍生物和含有这样的聚合性基团的树脂组合物，含氟和金属金刚烷衍生物。式中，X 1和X 2各自表示OH或NH 2，a，b和c各自表示0以上的整数，a + b +c≥1，例如a = b = 0，c = 1，Z 3表示例如-C 2 H 4 - ，s和t各自表示1〜15的整数，u表示0〜14的整数，s + t + u = 16，例如s = 2，t = 14，u = 0， X3表示例如-O-CO-CH = CH2。

4. 发明申请

US20100203332A1 METHOD FOR PRODUCING POLYTETRAFLUOROETHYLENE FIBER AND POLYTETRAFLUOROETHYLENE FIBER 有权
标题翻译：聚氟乙烯纤维和聚四氟乙烯纤维的生产方法
公开(公告)号：US20100203332A1
公开(公告)日：2010-08-12
申请号：US12665231
申请日：2008-06-16
申请人： Daisuke Kitagawa , Takashi Wano , Hideki Yamane , Yoshihito Takagi
发明人： Daisuke Kitagawa , Takashi Wano , Hideki Yamane , Yoshihito Takagi
IPC分类号： B29C51/08 , C08F214/26 , D02G3/00
CPC分类号： D01F6/12 , D01D5/08 , D01D5/12 , Y10T428/298
摘要： The present invention provides a method for producing a PTFE fiber that makes it possible, unlike the emulsion spinning process, to obtain a polytetrafluoroethylene (PTFE) fiber, particularly a long PTFE fiber, without using a matrix material, is more productive than conventional production methods such as a slit yarn process, and is capable of enhancing mechanical properties and the degree of freedom in diameter of the obtained fiber. The method for producing the PTFE fiber of the present invention includes the step of reducing a diameter of a string-shape PTFE-containing solid material (a first solid material) by drawing the first solid material at a temperature equal to or higher than a melting point of PTFE. The first solid material can be obtained from a PTFE-containing solid material (a second solid material) containing water and a surfactant, by reducing an amount of the water contained in the second solid material.
摘要翻译：本发明提供了一种PTFE纤维的制造方法，与乳液纺丝法不同，不需要使用基质材料即可获得聚四氟乙烯（PTFE）纤维，特别是长的PTFE纤维，与以往的制造方法相比，例如狭缝纱工艺，并且能够提高所获得的纤维的机械性能和直径的自由度。本发明的PTFE纤维的制造方法包括通过在等于或高于熔融的温度下拉伸第一固体材料来降低线状含PTFE固体材料（第一固体材料）的直径的步骤 PTFE点。通过减少第二固体材料中所含的水量，可以从含有水和表面活性剂的含PTFE固体材料（第二固体材料）获得第一固体材料。

5. 发明授权

US07662325B2 Polyhydroxyalkanoic acid fibers with high strength, fibers with high strength and high modulus of elasticity, and processes for producing the same 失效
标题翻译：高强度的聚羟基链烷酸纤维，高强度，高弹性模量的纤维及其制造方法
公开(公告)号：US07662325B2
公开(公告)日：2010-02-16
申请号：US11670342
申请日：2007-02-01
申请人： Tadahisa Iwata , Yoshiharu Doi , Hideki Yamane
发明人： Tadahisa Iwata , Yoshiharu Doi , Hideki Yamane
IPC分类号： D01D5/12
CPC分类号： D01F6/625 , Y10T428/2913 , Y10T428/2967
摘要： The present invention is a process for producing a fiber, comprising: melt-extruding polyhydroxyalkanoic acid; solidifying the polyhydroxyalkanoic acid by quenching it to its glass transition temperature +15° C. or less, to form an amorphous fiber; cold-drawing the amorphous fiber at its glass transition temperature +20° C. or less; and subjecting the fiber to heat treatment under tension. The present invention can provide: a process for producing a fiber with high strength, and the fiber produced through the process; and a process for producing a fiber with high strength and high modulus of elasticity and the fiber with high strength and high modulus of elasticity produced through the process, regardless of molecular weights of PHAs varying depending on origins such as a wild type PHAs-producing microorganism product, a genetically modified product, and a chemical product.
摘要翻译：本发明是一种纤维的制造方法，其特征在于，包括：熔融挤出聚羟基链烷酸; 通过将聚羟基链烷酸淬火至其玻璃化转变温度+ 15℃以下来固化，形成非晶纤维; 在其玻璃化转变温度+ 20℃或更低温度下冷拉伸无定形纤维; 并在拉伸下对纤维进行热处理。本发明可以提供一种高强度纤维的制造方法和通过该方法制造的纤维; 以及通过该方法生产具有高强度和高弹性模量的纤维和具有高强度和高弹性模量的纤维的方法，而不管根据诸如野生型PHA生产微生物的来源变化的PHAs的分子量如何产品，转基因产品和化学产品。

6. 发明申请

US20080306306A1 Method for Producing 2-Adamantanol and 2-Adamantanone 审中-公开
标题翻译：生产2-金刚烷醇和2-金刚烷酮的方法
公开(公告)号：US20080306306A1
公开(公告)日：2008-12-11
申请号：US11571800
申请日：2005-06-30
申请人： Akio Kojima , Hideki Yamane , Kenji Okamoto
发明人： Akio Kojima , Hideki Yamane , Kenji Okamoto
IPC分类号： C07C45/27
CPC分类号： C07C49/453 , C07C29/56 , C07C2603/74 , C07C35/37
摘要： The present invention is a process for producing 2-adamantanol and 2-adamantanone from 1-adamantanol, by using as a catalyst a substance comprising at least one kind of acid catalyst selected from Lewis acid(s) and solid acid(s) that coexist with at least one kind selected from the group consisting of carboxylic acids, sulfonic acids, and phosphoric acids, and provides a process suitable for mass production of 2-adamantanol and 2-adamantanone selectively with high efficiency without using sulfuric acid as a catalyst, thereby enabling laborsaving in waste acid treatment step and drastic reduction of the reaction time.
摘要翻译：本发明是一种由1-金刚烷生产2-金刚烷醇和2-金刚烷酮的方法，其通过使用选自共存的至少一种选自路易斯酸和固体酸的至少一种酸催化剂作为催化剂，具有选自羧酸，磺酸和磷酸的至少一种，并且提供了适合于高效率地选择性地大规模生产2-金刚烷酮和2-金刚烷酮的方法，而不用硫酸作催化剂。在废酸处理步骤中实现劳动，并大大减少反应时间。

7. 发明申请

US20060063892A1 Method for producing petroleum resin and hydrogenated petroleum resin 审中-公开
标题翻译：生产石油树脂和氢化石油树脂的方法
公开(公告)号：US20060063892A1
公开(公告)日：2006-03-23
申请号：US10535668
申请日：2003-12-01
申请人： Hideki Yamane
发明人： Hideki Yamane
IPC分类号： C08F112/08
CPC分类号： C08F232/06 , C08F8/04 , C08F212/08 , C08L57/00 , C08L91/00 , C08L2205/02 , C08L2666/02 , C09J123/0853
摘要： The present invention relates to a process for producing a petroleum resin which comprises subjecting a cyclopentadiene based compound and a vinyl-substituted aromatic compound substantially free from a high molecular weight substance to copolymerization reaction in the presence of a solvent. According to the present invention, it is made possible thereby to obtain a petroleum resin and a hydrogenated petroleum resin which are each minimized in the amounts of high molecular weight substances and which have each narrow molecular weight distribution.
摘要翻译：石油树脂的制造方法技术领域本发明涉及石油树脂的制造方法，其特征在于，在溶剂的存在下，使环戊二烯系化合物和基本上不含高分子量物质的乙烯基取代芳香族化合物进行共聚反应。根据本发明，可以获得石油树脂和氢化石油树脂，其各自以高分子量物质的量最小化，并且具有窄的分子量分布。

8. 发明授权

US5272221A Nylon composition having increased hydrolyzability and method for increasing hydrolyzability of nylon 失效
标题翻译：具有增加的水解性的尼龙组合物和增加尼龙的水解性的方法
公开(公告)号：US5272221A
公开(公告)日：1993-12-21
申请号：US863085
申请日：1992-04-03
申请人： Toshio Kitao , Yoshiharu Kimura , Hideki Yamane , Hiroki Nakata , Hosei Shinoda
发明人： Toshio Kitao , Yoshiharu Kimura , Hideki Yamane , Hiroki Nakata , Hosei Shinoda
IPC分类号： A61L31/04 , C08L77/00 , C08G69/48
CPC分类号： A61L31/041 , C08L77/00 , Y10S525/937
摘要： The present invention provides a nylon composition having increased hydrolyzability which is obtained by physically mixing 100 parts by weight of a nylon with 1 to 50 parts by weight of at least one polymer selected from the group consisting of polylactic acid, polyglycolic acid and a copolymer containing 50 mol % or more of a lactic acid unit or a glycolic acid unit as a repeating unit in its chain; and a method for increasing the hydrolyzability of a nylon by preparing such a composition. High hydrolyzability can be imparted to the nylon inherently having extremely low hydrolyzability without impairing its original mechanical strength. Therefore, various molded articles made from the nylon can be hydrolyzed under natural circumstances, and thus the wastes are not stored.
摘要翻译：本发明提供了具有增加的水解性的尼龙组合物，其通过将100重量份的尼龙与1至50重量份的至少一种选自聚乳酸，聚乙醇酸和含有 50重量％以上的乳酸单元或乙醇酸单元作为其链中的重复单元; 以及通过制备这种组合物来提高尼龙的水解性的方法。可以将高水解性赋予固有地具有极低水解性的尼龙，而不损害其原始的机械强度。因此，由尼龙制成的各种成型体在自然条件下可以水解，因此不会将废物进行储存。

9. 发明授权

US08163849B2 Process of producing polylactic acid 失效
标题翻译：生产聚乳酸的方法
公开(公告)号：US08163849B2
公开(公告)日：2012-04-24
申请号：US12526456
申请日：2008-02-06
申请人： Kiyotsuna Toyohara , Midori Ikegame , Hideki Yamane , Yoshiharu Kimura , Daisuke Masaki , Shin To
发明人： Kiyotsuna Toyohara , Midori Ikegame , Hideki Yamane , Yoshiharu Kimura , Daisuke Masaki , Shin To
IPC分类号： C08G63/91
CPC分类号： D01F6/625 , C08G63/08 , C08G63/88 , C08G63/912 , C08J3/005 , C08J2367/04 , D01F6/92
摘要： It is an object of the present invention to produce a polylactic acid having a high molecular weight such as a weight average molecular weight (Mw) of more than 100,000 from which only a stereocomplex crystal is grown even by repeating melting and crystallization. The present invention is a process of producing a polylactic acid, including the steps of: (i) obtaining a solid by kneading together poly(L-lactic acid) and poly(D-lactic acid) at a temperature of 160 to 225° C. and crystallizing the kneaded product; and (ii) melt kneading the obtained solid.
摘要翻译：本发明的目的是制备具有高分子量的重均分子量（Mw）超过100,000的聚乳酸，即使通过重复熔融和结晶也仅生长立体络合物晶体。本发明是一种制备聚乳酸的方法，包括以下步骤：（i）通过在160-225℃的温度下将聚（L-乳酸）和聚（D-乳酸）捏合在一起获得固体并使捏合产物结晶; 和（ii）熔融捏合所得固体。

10. 发明申请

US20100266954A1 ADAMANTANE DERIVATIVE, METHOD FOR PRODUCING THE SAME, AND CURING COMPOSITION CONTAINING ADAMANTANE DERIVATIVE 审中-公开
标题翻译：衍生物，其制备方法和含有ADAMANTANE衍生物的固化组合物
公开(公告)号：US20100266954A1
公开(公告)日：2010-10-21
申请号：US12742379
申请日：2008-11-10
申请人： Katsuki Ito , Shinji Tanaka , Naoya Kawano , Hideki Yamane , Hidetoshi Ono
发明人： Katsuki Ito , Shinji Tanaka , Naoya Kawano , Hideki Yamane , Hidetoshi Ono
IPC分类号： G03F7/004 , G03F7/20 , C07C69/608 , C08F20/10
CPC分类号： C07C69/54 , C07C2603/74 , C08F220/18 , C08F220/28 , G03F7/027 , G03F7/0397
摘要： An adamantane derivative capable of affording a cured product which is excellent in optical characteristics such as transparency and light resistance, durability such as long-term heat resistance, and electrical characteristics such as dielectric constant, a process for producing such an adamantane derivative, and a curable composition containing such an adamantane derivative, the adamantane derivative being represented by the general formula (I) shown below and having a group selected from an acrylate group, a methacrylate group and a trifluoromethacrylate group, where R1 represents a group selected from a hydroxyl group, an acrylate group, a methacrylate group and a trifluoromethacrylate group, R2 represents a group selected from a hydrogen atom, a methyl group and a trifluoromethyl group, k is an integer of 0 to 4 and n is an integer of 1 to 6.
摘要翻译：能够提供透明性，耐光性等光学特性，长期耐热性等耐久性，介电常数等电气特性，制造金刚烷衍生物的方法等的固化物的金刚烷衍生物，以及含有这种金刚烷衍生物的固化性组合物，金刚烷衍生物由下述通式（I）表示，具有选自丙烯酸酯基，甲基丙烯酸酯基和三氟甲基丙烯酸酯基的基团，其中R 1表示选自羟基的基团丙烯酸酯基，甲基丙烯酸酯基和三氟甲基丙烯酸酯基，R 2表示选自氢原子，甲基和三氟甲基的基团，k为0〜4的整数，n为1〜6的整数。

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