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1. 发明授权

US08451540B2 Retardation film 有权
标题翻译：延迟膜
公开(公告)号：US08451540B2
公开(公告)日：2013-05-28
申请号：US12440819
申请日：2007-09-11
申请人： Kenji Kato , Katsushige Hayashi , Noriyuki Kato , Haruaki Eto , Syoichi Nito
发明人： Kenji Kato , Katsushige Hayashi , Noriyuki Kato , Haruaki Eto , Syoichi Nito
IPC分类号： G02B5/02 , G02B5/30
CPC分类号： G02B5/3083 , G02B5/0226
摘要： Disclosed is a film suitable for improvement of luminance, contrast and view angle of a liquid crystal display. Specifically disclosed is a retardation film having a thickness of 30-500 μm, a light transmittance of not less than 85%, and an Nz factor of not less than 10.
摘要翻译：公开了适用于提高液晶显示器的亮度，对比度和视角的膜。具体公开了厚度为30〜500μm，透光率为85％以上，Nz系数为10以上的延迟膜。

2. 发明授权

US5777064A Production method of polycarbonate 失效
标题翻译：聚碳酸酯的生产方法
公开(公告)号：US5777064A
公开(公告)日：1998-07-07
申请号：US615466
申请日：1996-03-14
申请人： Katsushige Hayashi , Tsutomu Kawakami , Yuji Takeda , Katuhiro Iura
发明人： Katsushige Hayashi , Tsutomu Kawakami , Yuji Takeda , Katuhiro Iura
IPC分类号： B29C47/76 , B29C67/24 , C08G64/40 , C08G64/00
CPC分类号： C08G64/406 , B29C47/76 , B29C67/246 , B29C47/0009 , B29K2069/00
摘要： A method of producing a polycarbonate excellent in the hue, the thermal stability, and the electrolysis stability by supplying a polycarbonate obtained by a transesterification method to an extruder having vent(s), melting the polycarbonate, and adding an acidic compound to the molten polycarbonate followed by kneading to continuously devolatilize low molecular weight compounds remaining in the polycarbonate. Better result is obtained by adding water to the kneaded mixture of the polycarbonate and the acidic compound before devolatilizing the low molecular weight compounds.
摘要翻译：通过将通过酯交换方法获得的聚碳酸酯供给到具有排气口的挤出机，熔融聚碳酸酯并将酸性化合物加入到熔融聚碳酸酯中的方法，制备具有优异色调，热稳定性和电解稳定性的聚碳酸酯的方法，然后捏合以使剩余在聚碳酸酯中的低分子量化合物脱挥发分。在将低分子量化合物脱挥发分之前，通过向聚碳酸酯和酸性化合物的捏合混合物中加水来获得更好的结果。

3. 发明授权

US4861854A Photosensitive polyimide precursor 失效
标题翻译：感光聚酰亚胺前体
公开(公告)号：US4861854A
公开(公告)日：1989-08-29
申请号：US200864
申请日：1988-06-01
申请人： Akitoshi Sugio , Takao Kawaki , Makoto Kobayashi , Katsushige Hayashi , Masahito Watanabe
发明人： Akitoshi Sugio , Takao Kawaki , Makoto Kobayashi , Katsushige Hayashi , Masahito Watanabe
IPC分类号： C08G73/10 , G03F7/037 , G03F7/038
CPC分类号： G03F7/0387 , C08G73/10 , C08G73/1053 , C08G73/1064 , C08G73/1067 , C08G73/1071
摘要： A photosensitive polyimide precursor composed of the structural units (A) represented by the following general formula (I) and the structural units (B) represented by the following general formula (II), in which the ratio of the molar quantity of the structural units (A) to the sum of the molar quantity of the structural units (A) and that of the structural units (B) is 0.01 or greater, and having a viscosity of 100 cP or above as measured at 25.degree. C. in the state of a 10% by weight solution in N-methylpyrrolidone: ##STR1## wherein R.sub.1 represents a tetravalent aromatic hydrocarbon residue; R.sub.2 represents a divalent aromatic hydrocarbon residue; X, identical or different represents a halogen or an alkyl group; and m represents 0 or an integer from 1 to 4. The photosensitivity of the present photosensitive polyimide precursor is about 20 to 100 times that of conventional products. After heat dehydration cyclization, it shows a heat resistance of 400.degree. C. or above.
摘要翻译：由以下通式（I）表示的结构单元（A）和由以下通式（II）表示的结构单元（B））组成的光敏聚酰亚胺前体，其中结构单元（A）和结构单元（B）的摩尔量的总和为0.01以上，粘度为100cP以上，在该状态下在25℃下测定的10重量％的N-甲基吡咯烷酮溶液：其中R1表示四价芳烃残基;（I）其中R 1表示四价芳烃残基; R2表示二价芳烃残基; X相同或不同，表示卤素或烷基; m表示0或1〜4的整数。本发明的感光性聚酰亚胺前体的光敏度为常规产品的约20〜100倍。热脱水环化后，其耐热性为400℃以上。

4. 发明授权

US4670535A Photosensitive polyimide precursor and process for producing the same 失效
标题翻译：感光聚酰亚胺前体及其制备方法
公开(公告)号：US4670535A
公开(公告)日：1987-06-02
申请号：US875044
申请日：1986-06-17
申请人： Akitoshi Sugio , Takao Kawaki , Katsushige Hayashi
发明人： Akitoshi Sugio , Takao Kawaki , Katsushige Hayashi
IPC分类号： C08G73/00 , C08F290/00 , C08F299/02 , C08G73/10 , C08G73/12 , G03F7/038 , C08G16/00
CPC分类号： C08G73/1082 , G03F7/0387
摘要： The photosensitive polyimide precursor of the invention has a recurring unit represented by the following general formula [I]: ##STR1## (R.sub.1 represents a tetravalent aromatic hydrocarbon residue; R.sub.2 and R.sub.3 each represent a divalent aromatic or aliphatic hydrocarbon residue; and R.sub.4 represents a divalent aromatic hydrocarbon residue represented by ##STR2## wherein R.sub.5, R.sub.6, R.sub.7, R.sub.8, R.sub.9, R.sub.10, R.sub.11 and R.sub.12, identical or different, each represent hydrogen atom, a halogen group or an alkyl group). The photosensitive polyimide precursor of the invention has a viscosity of 50 centipoises or above as measured at 23.degree. C. in the state of a 10% (by weight) solution in N,N-dimethylacetamide. Its photosensitivity is as high as about 20-100 times that of prior products. After heat cyclization, it exhibits a heat resistance of 400.degree. C. or above.The photosensitive polyimide precursor of the invention can be produced by subjecting a tetracarboxylic acid dianhydride and a diamino compound to a polycondensation reaction in an organic polar solvent.
摘要翻译：本发明的光敏聚酰亚胺前体具有由以下通式[I]表示的重复单元：（R 1表示四价芳烃残基; R 2和R 3各自表示二价芳族或脂族烃 R4代表由下式表示的二价芳烃残基：其中R5，R6，R7，R8，R9，R10，R11和R12相同或不同，分别代表氢原子，卤素基团或烷基）。本发明的光敏聚酰亚胺前体在23℃下的粘度为10厘泊（N，N-二甲基乙酰胺）溶液的状态下的粘度为50厘泊或更高。其光敏度高达现有产品的约20-100倍。热环化后，其耐热性为400℃以上。本发明的感光性聚酰亚胺前体可以通过在有机极性溶剂中使四羧酸二酐和二氨基化合物进行缩聚反应来制造。

5. 发明授权

US08790766B2 Polymer film 有权
标题翻译：聚合物膜
公开(公告)号：US08790766B2
公开(公告)日：2014-07-29
申请号：US12520558
申请日：2007-12-21
申请人： Kenji Kato , Katsushige Hayashi , Jun Yokoyama , Mitsuo Miura , Tsutomu Nara
发明人： Kenji Kato , Katsushige Hayashi , Jun Yokoyama , Mitsuo Miura , Tsutomu Nara
IPC分类号： B32B3/10 , G02B5/02 , C08J5/18 , G02F1/1335 , B29C59/04
CPC分类号： C08J5/18 , B29C59/04 , C08J2369/00 , G02B5/0221 , G02B5/0278 , G02F1/133606 , Y10T428/24355
摘要： The present invention can provide a polymer film having an Ra (arithmetic average roughness) of 0.5 μm to 2.5 μm, an Ry (maximum height) of 3 μm to 11 μm, an Rz (ten-point average height) of 3 μm to 8 μm, and a light transmittance of 85% or higher. A preferable embodiment of the present invention can provide, at the same time, an optical diffusion function, an improved luminance, a transmittance and the like which are of a sufficient level not realized conventionally. In a still preferable embodiment, Sm (average concave-concave/convex-convex interval) of 90 μm to 160 μm and the average inter-local peak interval (S) is 5 μm to 15 μm.
摘要翻译：本发明可以提供Ra（算术平均粗糙度）为0.5μm〜2.5μm，Ry（最大高度）为3μm〜11μm，Rz（10点平均高度）为3μm〜8μm的聚合物膜 μm，透光率为85％以上。本发明的优选实施方式可以同时提供通常没有实现的足够水平的光学扩散功能，改善的亮度，透射率等。在一个更优选的实施方式中，90μm〜160μm的Sm（平均凹入/凸凸间隔）和平均局部间间隔间隔（S）为5μm〜15μm。

6. 发明授权

US5457174A Method for preparing polycarbonates by transesterification in a steel reactor 失效
标题翻译：在钢铁反应器中通过酯交换制备聚碳酸酯的方法
公开(公告)号：US5457174A
公开(公告)日：1995-10-10
申请号：US278136
申请日：1994-07-21
申请人： Katsushige Hayashi , Mitsuhiko Masumoto , Masayuki Nakajima , Takuya Hasaki , Masahiko Ishikawa , Atsushi Hirashima
发明人： Katsushige Hayashi , Mitsuhiko Masumoto , Masayuki Nakajima , Takuya Hasaki , Masahiko Ishikawa , Atsushi Hirashima
IPC分类号： C08G64/30 , C08G64/00
CPC分类号： C08G64/307
摘要： A process for preparing a polycarbonate which comprises performing a transesterification and a polycondensation reaction with a diarylcarbonate and dihydroxyaryl compound, in a reaction apparatus composed of stainless steel comprising at least 12% by weight of Ni, and at least 22% by weight of Cr, and having Fe as the remaining main component. A polycarbonate which has a good color, is stable to hydrolysis and resistant to heat-yellowing is the resulting product.
摘要翻译：一种制备聚碳酸酯的方法，包括在由包含至少12重量％的Ni和至少22重量％的Cr的不锈钢构成的反应装置中进行与二芳基碳酸酯和二羟基芳基化合物的酯交换和缩聚反应，并且具有Fe作为剩余的主要成分。具有良好颜色的聚碳酸酯，对于水解稳定并且耐黄变是产生的产物。

7. 发明授权

US5310944A Process for producing carboxylated compound 失效
标题翻译：羧化化合物的制备方法
公开(公告)号：US5310944A
公开(公告)日：1994-05-10
申请号：US975444
申请日：1992-01-17
申请人： Takao Kawaki , Yuh Miyauchi , Toshio Watanabe , Katsushige Hayashi , Satoshi Ueno , Hiroshi Ogawa , Fumiya Zaima
发明人： Takao Kawaki , Yuh Miyauchi , Toshio Watanabe , Katsushige Hayashi , Satoshi Ueno , Hiroshi Ogawa , Fumiya Zaima
IPC分类号： C07B41/08 , C07B41/12 , C07C51/285 , C07D315/00 , C07D313/04 , C07D307/33 , C07D309/30
CPC分类号： C07D315/00 , C07B41/08 , C07B41/12 , C07C51/285
摘要： A process for producing a carboxylated compound, which comprises reacting a carbonyl compound with hydrogen peroxide in the presence of an organo-arsenic acid of the formula (1), ##STR1## wherein: R.sup.1 is a C.sub.1 -C.sub.12 alkyl group which may be substituted or an aryl group which may be substituted,R.sup.2 is a hydroxyl group or the same group as that which defines R.sup.1,or alternatively, R.sup.1 and R.sup.2 may bond to each other to form a five-membered or six-membered ring together with As atoms to which these groups are bonded, andthe substituent(s) substituted on the above groups is/are selected from hydroxyl, carboxyl, carbonyl, sulfonyl, sulfonium, an amino group, an ammonium group, an alkyl group, an alkoxyl group and a halogen atom,while a water concentration in a reaction system is maintained at not more than 2% by weight, thereby to form a corresponding carboxylated compound.
摘要翻译：一种羧化化合物的制备方法，其包括在式（1）的有机砷酸存在下使羰基化合物与过氧化氢反应，其中：R1是C1-C12烷基，可以被取代，或者可以被取代的芳基，R 2是与定义R 1的羟基或者相同的基团，或者，R 1和R 2可以彼此键合以形成五元或六元环在一起与这些基团键合的As原子，并且上述取代基的取代基选自羟基，羧基，羰基，磺酰基，锍，氨基，铵基，烷基，烷氧基基团和卤素原子，而反应体系中的水浓度保持在不超过2重量％，从而形成相应的羧化化合物。

8. 发明授权

US4473705A Process for producing oxalate diester 失效
标题翻译：生产草酸二酯的方法
公开(公告)号：US4473705A
公开(公告)日：1984-09-25
申请号：US451846
申请日：1982-12-21
申请人： Hiroshi Miyamori , Tadashi Simomura , Mituo Miura , Katsushige Hayashi
发明人： Hiroshi Miyamori , Tadashi Simomura , Mituo Miura , Katsushige Hayashi
IPC分类号： C07C67/36 , B01J23/54 , B01J27/00 , B01J27/057 , B01J27/186 , B01J27/24 , B01J31/00 , B01J31/28 , C07B61/00 , C07C69/36
CPC分类号： B01J27/186 , B01J23/54 , B01J27/0576
摘要： A process for producing an oxalate diester is provided. The oxalate diester is produced by reacting an aliphatic alcohol, carbon monoxide and molecular oxygen at an elevated temperature and under pressure in the presence of a catalyst comprising (1) metallic palladium or a palladium compound, (2) a heteropoly-acid and (3) at least one nitrogen compound selected from the group consisting of nitric acid, nitrogen oxides and esters of nitrous acid.
摘要翻译：提供了一种生产草酸二酯的方法。草酸二酯是通过使脂族醇，一氧化碳和分子氧在升高的温度和压力下，在包含（1）金属钯或钯化合物的催化剂存在下反应制备的，（2）杂多酸和（3 ）至少一种选自硝酸，氮氧化物和亚硝酸酯的氮化合物。

9. 发明申请

US20100136287A1 POLYMER FILM 有权
标题翻译：聚合物胶片
公开(公告)号：US20100136287A1
公开(公告)日：2010-06-03
申请号：US12520558
申请日：2007-12-21
申请人： Kenji Kato , Katsushige Hayashi , Jun Yokoyama
发明人： Kenji Kato , Katsushige Hayashi , Jun Yokoyama
IPC分类号： B32B3/10
CPC分类号： C08J5/18 , B29C59/04 , C08J2369/00 , G02B5/0221 , G02B5/0278 , G02F1/133606 , Y10T428/24355
摘要： The present invention can provide a polymer film having an Ra (arithmetic average roughness) of 0.5 μm to 2.5 μm, an Ry (maximum height) of 3 μm to 11 μm, an Rz (ten-point average height) of 3 μm to 8 μm, and a light transmittance of 85% or higher. A preferable embodiment of the present invention can provide, at the same time, an optical diffusion function, an improved luminance, a transmittance and the like which are of a sufficient level not realized conventionally. In a still preferable embodiment, Sm (average concave-concave/convex-convex interval) of 90 μm to 160 μm and the average inter-local peak interval (S) is 5 μm to 15 μm.
摘要翻译：本发明可以提供Ra（算术平均粗糙度）为0.5μm〜2.5μm，Ry（最大高度）为3μm〜11μm，Rz（10点平均高度）为3μm〜8μm的聚合物膜 μm，透光率为85％以上。本发明的优选实施方式可以同时提供通常没有实现的足够水平的光学扩散功能，改进的亮度，透射率等。在一个更优选的实施方式中，90μm〜160μm的Sm（平均凹入/凸凸间隔）和平均局部间间隔间隔（S）为5μm〜15μm。

10. 发明授权

US06255436B1 Aromatic polycarbonate 有权
标题翻译：芳香聚碳酸酯
公开(公告)号：US06255436B1
公开(公告)日：2001-07-03
申请号：US09444933
申请日：1999-11-22
申请人： Masatoshi Kimura , Michio Kawai , Hiroshi Takeguchi , Hiroshi Nakano , Masayuki Nakajima , Katsushige Hayashi
发明人： Masatoshi Kimura , Michio Kawai , Hiroshi Takeguchi , Hiroshi Nakano , Masayuki Nakajima , Katsushige Hayashi
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： An aromatic polycarbonate of the present invention is produced by reacting an aromatic dihydroxy compound with a compound capable of introducing a carbonate bond, and has a viscosity-average molecular weight of 12,000 to 40,000 and a content of a cyclic oligomer represented by the formula (1) of not more than 1,000 ppm, in which the percentage of the content of said cyclic oligomer represented by the formula (1) based on the total contents of the cyclic oligomer represented by the formula (1), an oligomer represented by the formula (2) and an oligomer represented by the formula (3) satisfies the following relational formula [I]: 0
摘要翻译：本发明的芳香族聚碳酸酯是通过使芳香族二羟基化合物与能够引入碳酸酯键的化合物反应而制造的，粘均分子量为12,000〜40,000，由式（1）表示的环状低聚物的含量）不超过1000ppm，其中由式（1）表示的所述环状低聚物的含量的百分比基于由式（1）表示的环状低聚物的总含量，由式（1）表示的低聚物 2）和式（3）表示的低聚物满足以下关系式[I]：其中（1），（2）和（3）是由上式（1），（2）表示的低聚物的含量，和（3）分别; Mv是所述芳族聚碳酸酯的粘均分子量。

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