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1. 发明授权

US08497340B2 Fluorosilicone mold release composition 有权
标题翻译：氟硅酮脱模组合物
公开(公告)号：US08497340B2
公开(公告)日：2013-07-30
申请号：US12305738
申请日：2007-06-15
申请人： Yasuo Itami , Hisashi Mitsuhashi , Tetsuya Masutani , Peter Cheshire Hupfield , Don Lee Kleyer
发明人： Yasuo Itami , Hisashi Mitsuhashi , Tetsuya Masutani , Peter Cheshire Hupfield , Don Lee Kleyer
IPC分类号： C08L83/04 , C08G77/16 , C08G77/00 , B22C1/205
CPC分类号： B29C33/64 , C08G77/385 , C08G77/50 , C08L83/08 , C09D183/14
摘要： Disclosed in a mold release composition comprising a fluorosilicone compound of the formula (I): (I) wherein R1, R2, R4, R5, R6, R7, R8 and R9 each is, the same or different, a substituted or unsubstituted alkyl group, or a substituted or unsubstituted aryl group, R3 and R10 each is; the same or different, a substituted or unsubstituted alkyl group, or a substituted or unsubstituted aryl group, or Rf—X—, or Z—Y— in which X and Y each is; the same or different, a divalent organic group, Rf is a C1-6 fluoroalkyl group, Z is a silyl group containing a hydrolyzable site, m is 1-100, n is 1-50, and o is 0-200. The mold release composition can give excellent mold releasability and durability of mold releasability (repeated mold releasability).
摘要翻译：公开在包含式（I）的氟硅酮化合物：（I）的脱模剂组合物中，其中R 1，R 2，R 4，R 5，R 6，R 7，R 8和R 9各自为相同或不同的取代或未取代的烷基，或取代或未取代的芳基，R 3和R 10各自为取代或未取代的烷基或取代或未取代的芳基，或者Rf-X-或Z-Y-，其中X和Y各自为二价有机基团，Rf为C1-6氟烷基，Z为含有可水解位点的甲硅烷基，m为1-100，n为1-50，o为0-200。脱模组合物可以提供脱模性和脱模性（反复脱模性）的优异的脱模性和耐久性。

2. 发明申请

US20130078880A1 Fluoropolymers And Surface Treatment Agent 有权
标题翻译：含氟聚合物和表面处理剂
公开(公告)号：US20130078880A1
公开(公告)日：2013-03-28
申请号：US13510796
申请日：2010-11-18
申请人： Norimasa Uesugi , Masashi Nanri , Ikuo Yamamoto , Peter Cheshire Hupfield
发明人： Norimasa Uesugi , Masashi Nanri , Ikuo Yamamoto , Peter Cheshire Hupfield
IPC分类号： C08L33/16 , D06M15/277
CPC分类号： C08L33/16 , C08F220/24 , C08K5/16 , D06M15/227 , D06M15/277 , D06M15/285 , D06M15/576 , D06M15/63 , D06M15/6436 , D06M2200/11 , D06M2200/12 , Y10T442/2172
摘要： Disclosed is a fluorine-containing polymer prepared by polymerizing: (I) a polyfluoroalkyl group-containing (meth)acrylate, in the presence of: (II) an isocyanate compound blocked with a pyrazole compound or a malonate ester. A water- and oil-repellent composition containing the fluorine-containing polymer can impart the excellent water- and oil-repellency, and excellent durability thereof to substrates.
摘要翻译：公开了通过在（II）用吡唑化合物或丙二酸酯封端的异氰酸酯化合物的存在下聚合：（I）含有多氟烷基的（甲基）丙烯酸酯而制备的含氟聚合物。含有含氟聚合物的拒水拒油剂可赋予基材优异的拒水拒油性和优异的耐久性。

3. 发明申请

US20120295503A1 Fluoropolymers And Treatment Agent 有权
标题翻译：含氟聚合物和处理剂
公开(公告)号：US20120295503A1
公开(公告)日：2012-11-22
申请号：US13510787
申请日：2010-11-18
申请人： Norimasa Uesugi , Kouji Kubota , Ikuo Yamamoto , Peter Cheshire Hupfield
发明人： Norimasa Uesugi , Kouji Kubota , Ikuo Yamamoto , Peter Cheshire Hupfield
IPC分类号： C08F220/56 , B32B5/02 , C09D133/26 , C08K5/3445
CPC分类号： D06M15/657 , C08F220/24 , C08G77/442 , C08K5/16 , C09K3/18 , C09K2003/1081 , D06M15/277 , D06M15/576 , Y10T442/2172 , C08L33/16 , C08F220/18 , C08F2220/1891 , C08F2220/281 , C08F220/58
摘要： Disclosed is a fluorine-containing polymer prepared by polymerizing (I) a polyfluoroalkyl group-containing (meth)acrylate which is substituted at alpha-position, in the presence of (II) a blocked isocyanate compound. A water- and oil-repellent composition containing the fluorine-containing polymer can impart the excellent water- and oil-repellency, and excellent durability thereof to substrates.
摘要翻译：公开了通过在（II）封端异氰酸酯化合物的存在下，使（I）在α-位被取代的含有多氟烷基的（甲基）丙烯酸酯聚合而制备的含氟聚合物。含有含氟聚合物的拒水拒油剂可赋予基材优异的拒水拒油性和优异的耐久性。

4. 发明申请

US20110306713A1 METHOD OF PREPARING WATER- AND OIL-REPELLENT SOIL-RESISTANT COMPOSITION 有权
标题翻译：制备耐水和耐油的土壤抗性组合物的方法
公开(公告)号：US20110306713A1
公开(公告)日：2011-12-15
申请号：US13128464
申请日：2009-11-10
申请人： Akihiko Ueda , Yasuo Itami , Tetsuya Masutani , Peter Cheshire Hupfield , Janet Smith , Jean-Paul Lecomte
发明人： Akihiko Ueda , Yasuo Itami , Tetsuya Masutani , Peter Cheshire Hupfield , Janet Smith , Jean-Paul Lecomte
IPC分类号： C08K5/5419 , C09D143/04 , C08K5/5415 , C09D133/16
CPC分类号： C08F220/24 , C08F2/04 , C08F220/18 , C08F230/08 , Y10T428/31663 , Y10T428/31855 , Y10T428/31935
摘要： The present invention provides a water- and oil-repellent soil-resistant composition comprising (A) a fluorine-containing polymer having repeating units derived from a monomer comprising a fluorine-containing monomer and (B) a silane compound. The water- and oil-repellent soil-resistant composition comprising the fluorine-containing acrylate polymer can impart the excellent water- and oil-repellency and soil resistance to the porous substrate and is free from an organic solvent.
摘要翻译：本发明提供一种拒水拒油防污组合物，其包含（A）含有衍生自含有单体的单体的重复单元和（B）硅烷化合物的含氟聚合物。包含含氟丙烯酸酯聚合物的拒水防油组合物可以赋予多孔基材优异的拒水拒油性和耐污性，并且不含有机溶剂。

5. 发明申请

US20110287678A1 FLUOROSILICONE POLYMERS AND SURFACE TREATMENT AGENT 有权
标题翻译：氟聚合物聚合物和表面处理剂
公开(公告)号：US20110287678A1
公开(公告)日：2011-11-24
申请号：US13063809
申请日：2009-09-11
申请人： Shinichi Minami , Takashi Enomoto , Tetsuya Masutani , Masahiro Miyahara , Mitsuhiro Usugaya , Rumi Takeuchi , Ikuo Yamamoto , Peter Cheshire Hupfield
发明人： Shinichi Minami , Takashi Enomoto , Tetsuya Masutani , Masahiro Miyahara , Mitsuhiro Usugaya , Rumi Takeuchi , Ikuo Yamamoto , Peter Cheshire Hupfield
IPC分类号： B32B5/02 , C09K3/00 , C08G77/28
CPC分类号： D06M15/6436 , C08F283/122 , C08F290/068 , D06M15/277 , D06M15/3568 , Y10T442/2172 , C08F220/24 , C08F220/68
摘要： A surface treatment agent, which can impart the excellent water- and oil-repellency, soil resistance and feeling to the substrate, is obtained from a fluorine-containing polymer which contains: (A) a monomer which comprises; (A1) a fluorine-containing monomer of the formula: CH2═C(—X)—C(═O)—Y—Z—Rf wherein X is a hydrogen atom, a monovalent organic group, or a halogen atom, Y is —O— or —NH—, Z is a direct bond or a divalent organic group, and Rf is a fluoroalkyl group having 1 to 20 carbon atoms, and (A2) a (meth)acrylate monomer having a cyclic hydrocarbon group, and (B) at least one functional organopolysiloxane selected from the group consisting of a mercapto-functional organopolysiloxane, a vinyl-functional organopolysiloxane, a (meth)acrylamide-functional organopolysiloxane and a (meth)acrylate-functional group.
摘要翻译：可以从含有以下的含氟聚合物获得能够赋予基材优异的防水拒油性，耐污性和感觉的表面处理剂：（A）包含以下物质的单体：（A1）下式的含氟单体：CH2 = C（-X）-C（= O）-Y-Z-Rf其中X为氢原子，一价有机基团或卤素原子，Y为 -O-或-NH-，Z为直接键或二价有机基团，Rf为碳原子数1〜20的氟烷基，（A2）具有环状烃基的（甲基）丙烯酸酯单体，（ B）至少一种选自巯基官能的有机聚硅氧烷，乙烯基官能的有机聚硅氧烷，（甲基）丙烯酰胺官能的有机聚硅氧烷和（甲基）丙烯酸酯官能团的官能的有机聚硅氧烷。

6. 发明申请

US20100113700A1 CURABLE FLUORINE-CONTAINING POLYMER COMPOSITION 有权
标题翻译：可固化含氟聚合物组合物
公开(公告)号：US20100113700A1
公开(公告)日：2010-05-06
申请号：US12445354
申请日：2007-10-12
申请人： Katsuhiko Imoto , Tetsuo Shimizu , Tatsuya Morikawa , Masayuki Hayashi , Tomohiro Iimura , Peter Cheshire Hupfield
发明人： Katsuhiko Imoto , Tetsuo Shimizu , Tatsuya Morikawa , Masayuki Hayashi , Tomohiro Iimura , Peter Cheshire Hupfield
IPC分类号： C08F8/00 , C08F14/00
CPC分类号： C08G18/8108 , C08G18/6279 , C08G77/045 , C08G77/12 , C08G77/442 , C08K5/5419 , C08L27/12 , C08L31/02 , C08L83/04 , C09D127/12 , C09D127/18 , C09D127/20 , C09D131/02 , C08L2666/04 , C08L2666/14
摘要： There is provided a curable fluorine-containing polymer composition which is quickly cured at relatively low temperatures by hydrosilylation reaction and provides a coating film which has high hardness, excellent solvent resistance and flexibility. The curable fluorine-containing polymer composition comprises a fluorine-containing polymer comprising a fluorinated ethylenic monomer unit and a non-fluorinated ethylenic monomer unit, in which a part or the whole of the non-fluorinated ethylenic monomer units is a unit represented by the formula: wherein R1 is hydrogen or methyl; R2 is a hydrocarbon group having ethylenic C═C; X is —C(O)NH— or —C(O)—; R3 is —O—, —O[CH(R4)]mO—, —(CH2)mO—, —OC(O)—(CH2)mO— or —(CH2)mOC(O)—(CH2)nO—, where R4 is —H, —OH, —CH2OH or —O—X—R2, a siloxane compound having hydrogen atom bonded to silicon atom, and a catalyst for hydrosilylation reaction.
摘要翻译：提供一种通过氢化硅烷化反应在相对低的温度下快速固化的可固化含氟聚合物组合物，并提供具有高硬度，优异的耐溶剂性和柔性的涂膜。可固化含氟聚合物组合物包含含有氟化乙烯性单体单元和非氟化乙烯性单体单元的含氟聚合物，其中一部分或全部未氟化烯属单体单元为式其中R1是氢或甲基; R2是具有烯属C = C的烃基; X是-C（O）NH-或-C（O） - ; R 3是-O-，-O [CH（R 4）] m O - ， - （CH 2）m O - ， - OC（O） - （CH 2）m O-或 - （CH 2）mOC（O） - （CH 2）其中R4是-H，-OH，-CH2OH或-O-X-R2，具有与硅原子键合的氢原子的硅氧烷化合物和氢化硅烷化反应的催化剂。

7. 发明申请

US20100018659A1 GREASEPROOF PAPER 有权
标题翻译：防油纸
公开(公告)号：US20100018659A1
公开(公告)日：2010-01-28
申请号：US12375086
申请日：2007-07-24
申请人： Peter Cheshire Hupfield , Tetsuya Masutani , Shinichi Minami , Ikuo Yamamoto
发明人： Peter Cheshire Hupfield , Tetsuya Masutani , Shinichi Minami , Ikuo Yamamoto
IPC分类号： D21H17/34 , C08F14/18
CPC分类号： C09D133/16 , C08F283/122 , D21H17/59 , D21H21/16 , Y10T428/31663 , C08F220/24
摘要： A greaseproof paper is provided for use in food processing and/or packaging of foods in which paper has been rendered oleophobic by treatment with a fluorine-containing polymer. The fluorine-containing polymer may be prepared by polymerizing a fluorine-containing monomer in the presence of a mercapto group-containing organopolysiloxane. The fluorine-containing polymer may be applied to paper by coating onto pre-formed paper, or by applying the polymer as a size during a papermaking process.
摘要翻译：提供防油纸用于食品加工和/或包装通过用含氟聚合物处理已经产生疏油性的食品。含氟聚合物可以通过在含巯基的有机聚硅氧烷的存在下聚合含氟单体来制备。含氟聚合物可以通过涂布在预成型纸上或通过在造纸过程中以聚合物的尺寸施加到纸上。

8. 发明授权

US09988759B2 Fluorosilicone polymers and surface treatment agent 有权
公开(公告)号：US09988759B2
公开(公告)日：2018-06-05
申请号：US13063809
申请日：2009-09-11
申请人： Shinichi Minami , Takashi Enomoto , Tetsuya Masutani , Masahiro Miyahara , Mitsuhiro Usugaya , Rumi Takeuchi , Ikuo Yamamoto , Peter Cheshire Hupfield
发明人： Shinichi Minami , Takashi Enomoto , Tetsuya Masutani , Masahiro Miyahara , Mitsuhiro Usugaya , Rumi Takeuchi , Ikuo Yamamoto , Peter Cheshire Hupfield
IPC分类号： B32B27/04 , D06M15/643 , C08F283/12 , C08F290/06 , D06M15/277 , D06M15/356
CPC分类号： D06M15/6436 , C08F283/122 , C08F290/068 , D06M15/277 , D06M15/3568 , Y10T442/2172 , C08F220/24 , C08F220/68
摘要： A surface treatment agent, which can impart the excellent water- and oil-repellency, soil resistance and feeling to the substrate, is obtained from a fluorine-containing polymer which contains: (A) a monomer which comprises; (A1) a fluorine-containing monomer of the formula: CH2═C(—X)—C(═O)—Y—Z—Rf wherein X is a hydrogen atom, a monovalent organic group, or a halogen atom, Y is —O— or —NH—, Z is a direct bond or a divalent organic group, and Rf is a fluoroalkyl group having 1 to 20 carbon atoms, and (A2) a (meth)acrylate monomer having a cyclic hydrocarbon group, and (B) at least one functional organopolysiloxane selected from the group consisting of a mercapto-functional organopolysiloxane, a vinyl-functional organopolysiloxane, a (meth)acrylamide-functional organopolysiloxane and a (meth)acrylate-functional group.

9. 发明申请

US20130184482A1 Process For Preparing An Acryloyloxysilane 有权
标题翻译：制备丙烯酰氧基硅烷的方法
公开(公告)号：US20130184482A1
公开(公告)日：2013-07-18
申请号：US13825633
申请日：2011-09-20
申请人： Peter Cheshire Hupfield , Xiaobing Zhou
发明人： Peter Cheshire Hupfield , Xiaobing Zhou
IPC分类号： C07F7/02
CPC分类号： C07F7/025 , C07F7/1892 , C07F7/20
摘要： A process for preparing an acryloyloxysilane, the process comprising reacting a metal salt of a carboxylic acid having the formula [CR22═CR1COO−]aMa+ (I), with a haloorganoalkoxysilane having the formula XR3Si(OR4)nR53—n (II) in the presence of mineral spirits and a phase transfer catalyst at a temperature of from 50 to 160° C. to form a mixture comprising an acryloyloxysilane and a metal halide having the formula Ma+X−a (III), wherein R1 is H or C1-C6 hydrocarbyl, each R2 is independently R1 or [COO−]aMa+, Ma+ is an alkali metal cation or alkaline earth metal cation, a is 1 or 2, X is halo, R3 is C1-C6 hydrocarbylene, each R4 is independently C1-C10 Q hydrocarbyl, each R5 is independently R1 and n is an integer from 1 to 3.
摘要翻译：一种制备丙烯酰氧基硅烷的方法，该方法包括使具有式[CR22 = CR1COO-] aMa +（I）的羧酸的金属盐与式XR3Si（OR4）nR53-n（II）的卤代有机烷氧基硅烷在在50至160℃的温度下存在矿物油精和相转移催化剂以形成包含丙烯酰氧基硅烷和具有式Ma + Xa（III）的金属卤化物的混合物，其中R 1为H或C 1 -C 6烃基，每个R 2独立地是R 1或[COO-] a M a +，Ma +是碱金属阳离子或碱土金属阳离子，a是1或2，X是卤素，R 3是C 1 -C 6亚烃基，每个R 4独立地是C 1 -C 10 Q 烃基，每个R 5独立地为R 1，n为1至3的整数。

10. 发明申请

US20110274936A1 FLUORINE- AND SILICON-CONTAINING TREATMENT AGENT FOR CONCRETES 审中-公开
标题翻译：含氟和含硅的混凝土处理剂
公开(公告)号：US20110274936A1
公开(公告)日：2011-11-10
申请号：US13123754
申请日：2009-10-09
申请人： Teruyuki Fukuda , Shinichi Minami , Peter Cheshire Hupfield , Samantha Reed , Janet Smith
发明人： Teruyuki Fukuda , Shinichi Minami , Peter Cheshire Hupfield , Samantha Reed , Janet Smith
IPC分类号： B32B13/12 , C08L83/04 , C08G77/04
CPC分类号： C04B41/63 , C04B41/4842 , C08F283/122 , C08L51/085 , Y10T428/31663 , C04B41/483 , C04B41/4961 , C08F220/24
摘要： The present invention provides a surface treatment agent comprising a fluorine-containing polymer having repeating units derived from a monomer comprising a fluorine-containing monomer, wherein the fluorine-containing polymer has a silicone moiety possessed by a mercapto group-containing silicone. When a porous substrate is treated under drying at normal temperature, the surface treatment agent comprising the fluorine-containing acrylate polymer can impart the excellent water- and oil-repellency and soil resistance to the porous substrate.
摘要翻译：本发明提供一种表面处理剂，其含有含有含有含氟单体的单体的重复单元的含氟聚合物，其中含氟聚合物具有含有巯基的硅酮所具有的硅氧烷部分。当在常温下干燥处理多孔基材时，包含含氟丙烯酸酯聚合物的表面处理剂可赋予多孔基材优异的拒水拒油性和耐污性。

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