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1. 发明授权

US07732504B2 Functionalized photoinitiators 有权
标题翻译：官能化光引发剂
公开(公告)号：US07732504B2
公开(公告)日：2010-06-08
申请号：US10587584
申请日：2005-01-24
申请人： Kurt Dietliker , Rinaldo Hüsler , Jean-Luc Birbaum , Jean-Pierre Wolf
发明人： Kurt Dietliker , Rinaldo Hüsler , Jean-Luc Birbaum , Jean-Pierre Wolf
IPC分类号： C08F2/50
CPC分类号： C08F2/50 , B33Y70/00 , G03F7/0007 , G03F7/001 , G03F7/0037 , G03F7/031
摘要： The invention relates to novel photoinitiators of formula (I) wherein each of the substituents is given the definition as set forth in the Specification and the claims. The photoinitiators can be used to prepare multifunctional photoinitiators.
摘要翻译：本发明涉及式（I）的新型光引发剂，其中每个取代基都给出如本说明书和权利要求书中所阐述的定义。光引发剂可用于制备多功能光引发剂。

2. 发明申请

US20100022676A1 PHOTOCURABLE COMPOSITIONS COMPRISING A PHOTOINITIATOR OF THE PHENYLGLYOXYLATE TYPE 审中-公开
标题翻译：含有苯甲酸酯类型的光敏剂的可光性组合物
公开(公告)号：US20100022676A1
公开(公告)日：2010-01-28
申请号：US12442779
申请日：2007-09-24
申请人： Jonathan Rogers , Johannes Benkhoff , Karin Powell , Tunja Jung , Kurt Dietliker , Pascal Hayoz , Jean-Luc Birbaum , Thomas Vogel , Rinaldo Hüsler
发明人： Jonathan Rogers , Johannes Benkhoff , Karin Powell , Tunja Jung , Kurt Dietliker , Pascal Hayoz , Jean-Luc Birbaum , Thomas Vogel , Rinaldo Hüsler
IPC分类号： C08F2/46 , C08J7/18 , C07C69/67
CPC分类号： G03F7/031 , C07C59/90 , C07C69/738 , C07C2601/10 , C07C2601/14 , C08F2/50 , G03F7/0045 , G03F7/038
摘要： The invention provides a uv-curable colored composition, comprising (a) at least one selected ethylenically unsaturated photopolymerizable compound; (b) at least one selected curing agent; and (c) at least one selected colorant.
摘要翻译：本发明提供了一种紫外线固化着色组合物，其包含（a）至少一种选择的烯属不饱和光聚合化合物; （b）至少一种选择的固化剂; 和（c）至少一种选择的着色剂。

3. 发明授权

US07307192B2 Process for the preparation of 1-phenylindan photoinitiators 有权
标题翻译： 1-苯基吲哚类光引发剂的制备方法
公开(公告)号：US07307192B2
公开(公告)日：2007-12-11
申请号：US10553777
申请日：2004-04-26
申请人： Rinaldo Hüsler , Thomas Horni
发明人： Rinaldo Hüsler , Thomas Horni
IPC分类号： C07C45/00
CPC分类号： C08F2/50 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/81 , C07C49/792 , C07C49/813 , C07C49/83
摘要： The invention relates to a process for the preparation of a crystalline isomeric mixture of compounds of formulae (I) and (II) which process comprises the following steps: a) the slow addition of aluminium chloride, in portions, to a solution comprising 1,1,3-trimethyl-3-phenylindan and isobutyric acid halide in a suitable solvent at a reaction temperature of from −20° C. to 20° C., an isomeric mixture consisting of compounds of formulae (Ia) and (IIa) being obtained; b) enol chlorination of compounds (Ia) and (IIa), an isomeric mixture consisting of compounds of formulae (Ib) and (IIb) being obtained; c) hydrolysis of the chlorinated isomeric mixture from step b). The invention relates also to the preparation of the individual compounds (I) and (II).
摘要翻译：本发明涉及一种制备式（I）和（II）化合物的结晶异构体混合物的方法，该方法包括以下步骤：a）将氯化铝缓慢加入到包含1， 1,3-二甲基-3-苯基茚基和异丁酸卤化物在合适的溶剂中，在-20℃至20℃的反应温度下，由式（Ia）和（IIa）化合物组成的异构体混合物为获得; b）化合物（Ia）和（IIa）的烯醇氯化，得到由式（Ib）和（IIb）的化合物组成的异构体混合物; c）步骤b）中氯化异构体混合物的水解。本发明还涉及单个化合物（I）和（II）的制备。

4. 发明授权

US09199934B2 Alpha-hydroxyketones 有权
标题翻译： α-羟基酮
公开(公告)号：US09199934B2
公开(公告)日：2015-12-01
申请号：US12593025
申请日：2008-03-25
申请人： Kurt Dietliker , Peter Murer , Rinaldo Hüsler , Tunja Jung
发明人： Kurt Dietliker , Peter Murer , Rinaldo Hüsler , Tunja Jung
IPC分类号： G03F7/004 , C07C69/95 , C07D307/00 , C07D211/32 , G03F7/38 , G03F7/40 , C07C49/83 , C07C49/835 , C07C49/84 , C07C62/38 , C07C69/757 , C07C219/12 , C07C235/82 , C07D295/185 , C07D305/12 , C07F7/08 , C07F7/18
CPC分类号： C07D211/32 , C07C49/83 , C07C49/835 , C07C49/84 , C07C62/38 , C07C69/757 , C07C219/12 , C07C235/82 , C07C2601/14 , C07D295/185 , C07D305/12 , C07F7/0836 , C07F7/0838 , C07F7/1804 , G03F7/004 , G03F7/38 , G03F7/40
摘要： Compounds of the Formula (I) wherein x is an integer from 1-4; p is an integer from 1-3; q is an integer from 0-3; Ar is phenyl, naphthyl, anthryl or phenanthryl each of which optionally is substituted by one or more Cl, CN, OR5, C3-C5alkenyl or C1-C6alkyl which optionally is substituted by one or more OR6, COOR or halogen; R1 if x is 1, is OR7, O—X+, NR8R9, C1-C20alkyl optionally substituted by one or more COOR10, or is C2-C20alkyl interrupted by one ore more O, or is C2-C5alkenyl or phenyl-C1-C4alkyl; R1 if x is 2, is for example C1-C20alkylene; R1 if x is 3, is for example a tri-valent radical; R1 if x is 4, is for example a tetravalent radical; R2 and R3 are hydrogen or C1-C8alkyl, or R2 and R3 together are O, C1-C3alkylene or CH═CH; R4 is C1-C4alkyl; R5, R6, R7, R8, R9 and R10 are for example hydrogen or C1-C4alkyl; and X is a x-valent cationic counter ion; are in particular suitable as photoinitiators for the curing with UV-A light (320-450 nm).
摘要翻译：式（I）的化合物，其中x为1-4的整数; p是1-3的整数; q是0-3的整数; Ar是苯基，萘基，蒽基或菲基，其各自任选被一个或多个被一个或多个OR 6，COOR或卤素取代的C 1，CN，OR 5，C 3 -C 5链烯基或C 1 -C 6烷基取代; R 1如果x是1，是OR 7，O-X +，NR 8 R 9，任选被一个或多个COOR 10取代的C 1 -C 20烷基，或者是被一个或多个O取代的C 2 -C 20烷基，或者是C 2 -C 5烯基或苯基-C 1 -C 4烷基; R1如果x为2，例如为C 1 -C 20亚烷基; 如果x是3，则R1是例如三价基; R1如果x为4，则为例如四价基团; R 2和R 3是氢或C 1 -C 8烷基，或者R 2和R 3一起是O，C 1 -C 3亚烷基或CH = CH; R4是C1-C4烷基; R5，R6，R7，R8，R9和R10是例如氢或C1-C4烷基; X为x-阳离子抗衡离子; 特别适用于用UV-A光（320-450nm）固化的光引发剂。

5. 发明授权

US07723397B2 Difunctional photoinitiators 有权
标题翻译：双功能光引发剂
公开(公告)号：US07723397B2
公开(公告)日：2010-05-25
申请号：US10521650
申请日：2003-07-10
申请人： Rinaldo Hüsler , André Fuchs
发明人： Rinaldo Hüsler , André Fuchs
IPC分类号： C08F2/50 , C08F2/46 , C08J3/28
CPC分类号： G03F7/031 , B33Y70/00 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/68 , C07C49/83 , C07C49/84 , C08F2/50 , Y10S522/909 , C07C49/784 , C07C49/813
摘要： The invention relates to novel photoinitiators of formula (I) wherein A is —O—, —CH2−, CH(CH3)— or —C(CH3)2−, and R is methyl or trimethylsilyl, and R may in addition be hydrogen when A is simultaneously the group —C(CH3)2−. The invention relates also to compositions comprising (A) at least one ethylenically unsaturated compound, (B) a photoinitiator of formula (I), (C) optionally further binders or additives, (D) optionally further photoinitiators or co-initiators. Compositions comprising (A) an ethylenically unsaturated compound that contains at least one aminoacrylate, (B) a photoinitiator of formula (II) or (III), (C) optionally further binders or additives, (D) optionally further photoinitiators or co-initiators.
摘要翻译：本发明涉及式（I）的新型光引发剂，其中A为-O-，-CH 2 - ，CH（CH 3） - 或-C（CH 3）2 - ，R为甲基或三甲基甲硅烷基，R可另外为氢当A同时为-C（CH 3）2 - 基团时。本发明还涉及包含（A）至少一种烯键式不饱和化合物，（B）式（I）的光引发剂，（C）任选的其它粘合剂或添加剂的组合物，（D）任选的其它光引发剂或共引发剂。包含（A）含有至少一个氨基丙烯酸酯的烯键式不饱和化合物，（B）式（II）或（III）的光引发剂，（C）任选的其它粘合剂或添加剂的组合物，（D）任选的另外的光引发剂或共引发剂。

6. 发明授权

US07084183B2 Difunctional photoinitiators 有权
标题翻译：双功能光引发剂
公开(公告)号：US07084183B2
公开(公告)日：2006-08-01
申请号：US10494593
申请日：2002-10-31
申请人： André Fuchs , Rinaldo Hüsler , Christian Schregenberger , Martin Kunz
发明人： André Fuchs , Rinaldo Hüsler , Christian Schregenberger , Martin Kunz
IPC分类号： C08F2/50 , C07C49/83 , C07C45/64 , C07C45/81 , G03F7/031
CPC分类号： G03F7/031 , B33Y70/00 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/81 , C07C49/83 , C08F2/50 , C07C49/784 , C07C49/813
摘要： The invention relates to α-hydroxy ketones of formula I or IIa; or mixtures of compounds of formula I and II; or mixtures of compounds of formulae Ia and IIa
摘要翻译：本发明涉及式I或IIa的α-羟基酮; 或式I和II化合物的混合物; 或式Ia和IIa化合物的混合物

7. 发明授权

US07642296B2 Photoinitiators 有权
标题翻译：光引发剂
公开(公告)号：US07642296B2
公开(公告)日：2010-01-05
申请号：US11578595
申请日：2005-04-11
申请人： Rinaldo Hüsler , Thomas Horni , André Fuchs , Tunja Jung , Reinhard H. Sommerlade
发明人： Rinaldo Hüsler , Thomas Horni , André Fuchs , Tunja Jung , Reinhard H. Sommerlade
IPC分类号： C08F2/50 , C03C25/10 , C07C49/84
CPC分类号： C07C45/46 , B33Y70/00 , C07C45/58 , C07C45/63 , C07C45/64 , C07C45/71 , C07C45/74 , C07C49/792 , C07C49/82 , C07C49/83 , C07C49/84 , C07C69/96 , C07C271/12 , C07C317/24 , C07D295/108 , C07D295/112 , C07D493/08 , C08F2/50 , C07C49/76 , C07C49/80 , C07C49/813
摘要： The invention relates to novel photoinitators of formulae (I), (II), (III), (IV), (V) and (VI) wherein R1 and R2 are each independently of the other C1-C8alkyl; C1-C4alkyl substituted by OH, C1-C4alkoxy, —COO(C1-C8alkyl), (C1-C4alkyl)-COO—, —CN, benzyl, phenyl or by —N(R15)(R16); C3-C6alkerlyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; or R1 and R2 together are unbranched or branched C2-C9alkylene or C3-C6-oxa- or -azaalkylene; R3, R4, R5 and R6 are each independently of the others hydrogen, C1-C8alkyl, C3-C6alkenyl, benzyl, —CH2—C6H4—(C1-C4alkyl) or phenyl; R3 and R4 together and/or R5 and R6 together are unbranched or branched C2-C9alkylene; A is CI, Br, —O—R9, —N(R11)(R12) or —S—R18, A′ is —O—, —NH— or —NR11—; A″ is CI, Br, —O—R9, —N(R11)(R12) or —S—R18 or hydrogen, X is —O—R10 or —N(R13)(R14), n is an integer from 1 to 10, preferably an integer from 1 to 4, especially 1, 2 or 3; R7 is a linker; R8 is a bivalent C2-C3alkylele radical.
摘要翻译：本发明涉及式（I），（II），（III），（IV），（V）和（VI）的新型光引发剂，其中R 1和R 2各自独立地为C 1 -C 8烷基; 被OH，C1-C4烷氧基，-COO（C1-C8烷基），（C1-C4烷基）-COO-，-CN，苄基，苯基或-N（R15）（R16）取代的C1-C4烷基; C3-C6链烯基，苄基，-CH2-C6H4-（C1-C4烷基）或苯基; 或R 1和R 2一起是非支链或支链C 2 -C 9亚烷基或C 3 -C 6 - 氧杂 - 或 - 亚烷基; R 3，R 4，R 5和R 6各自独立地为氢，C 1 -C 8烷基，C 3 -C 6烯基，苄基，-CH 2 -C 6 H 4 - （C 1 -C 4烷基）或苯基; R 3和R 4一起和/或R 5和R 6一起是非支链或支链C 2 -C 9亚烷基; A是Cl，Br，-O-R9，-N（R11）（R12）或-S-R18，A'是-O - ， - NH-或-NR11-; A“是Cl，Br，-O-R9，-N（R11）（R12）或-S-R18或氢，X是-O-R10或-N（R13）（R14），n是 1至10，优选1至4的整数，特别是1,2或3; R7是连接体; R8是二价C2-C3烷基基团。

8. 发明授权

US07462650B2 Trifunctional photoinitiators 有权
标题翻译：三功能光引发剂
公开(公告)号：US07462650B2
公开(公告)日：2008-12-09
申请号：US10552952
申请日：2004-05-04
申请人： Reinhard H. Sommerlade , Rinaldo Hüsler , Stephan Ilg , André Fuchs , Souâd Boulmaâz , Jean-Luc Birbaum
发明人： Reinhard H. Sommerlade , Rinaldo Hüsler , Stephan Ilg , André Fuchs , Souâd Boulmaâz , Jean-Luc Birbaum
IPC分类号： C08F2/46 , C07C49/00
CPC分类号： G03F7/0295 , B33Y70/00 , C07C45/46 , C07C45/63 , C07C45/64 , C07C45/71 , C07C49/784 , C07C49/813 , C07C49/83 , C07C49/84 , C07C225/22 , C07C271/20 , C07C2601/14 , C08F2/50 , G03F7/029 , G03F7/031
摘要： The Invention relates to novel ketones of formulae (I) and (II) wherein R1, R2, R3 and R4 are, for example, C1-C8alkyl, R5 is, for example, hydrogen, A is CI, Br, -0-R7, —NR8R9 or —S—R16, A′ is —O—, —NH— or —NR8—, X and Y are each independently of the other —O—R10 or —N(R11)(R12), n is an integer from 1 to 10, R6 is, for example, an n-valent radical of linear or branched C2-C20alkyl the carbon chain of which may be interrupted by cyclohexanediyl, phenylene, —CH(OH)—, —C(C2H5)(CH2—CH2—OH)—, —C(CH3)(CH2—CH2—OH)—, —C(CH2—CH2—OH)2—, —N(CH3)—, —N(C2H5)—, —N(CH2—CH2—OH)—, —CO—O—, —O—CO—, —P(CH2—CH2—OH)—, —P(O)(CH2—CH2—OH)—, -0-P(O—CH2—CH2—OH)—O—, -0-P(O)(0-CH2—CH2—OH)—O—, —O-cyclohexanediyl-C(CH3)2-Cyclohexanediyl-O—, —O-phenylene-C(CH3)2-phenylene-O—, —O-phenylene-CH2-phenylene-O—, —Si(CH3)2—, -0-Si(CH3)2—O—, —O—Si(CH3)(0-CH3)—O—, —Si(CH3)(R17)—O—Si(CH3)(R18)—, 5-(2-hydroxyethyl)-[1,3,5]triazinane-2,4,6-trione-1,3-diyl and/or by from one to nine oxygen atoms.
摘要翻译：本发明涉及式（I）和（II）的新型酮，其中R 1，R 2，R 3和R 4是例如C 1 -C 8烷基，R 5是例如氢，A是Cl，Br，-O-R 7 ，-NR 8 R 9或-S-R 16，A'为-O-，-NH-或-NR 8 - ，X和Y各自独立地为O-R 10或-N（R 11）（R 12），n为 R 1为例如直链或支链C 2 -C 20烷基的n价基团，其碳链可以被环己二基，亚苯基，-CH（OH） - ， - C（C 2 H 5）（ CH 2 -CH 2 -OH） - ， - C（CH 3）（CH 2 -CH 2 -OH） - ， - C（CH 2 -CH 2 OH）2 - ， - N（CH 3） - ， - N（C 2 H 5）（CH2-CH2-OH） - ， - CO-O - ， - O-CO-，-P（CH2-CH2-OH） - ，-P（O）（CH2-CH2-OH）（O-CH 2 -CH 2 -OH）-O-，-O-P（O）（O-CH 2 -CH 2 -OH）-O-，-O-环己二基-C（CH 3）2 - 环己烷二基-O-， - O-亚苯基-C（CH 3）2 - 亚苯基-O - ， - 亚苯基-CH 2 - 亚苯基-O-，-Si（CH 3）2 - ， - O-Si（CH 3）2 -O-，-O- Si（CH 3）（O-CH 3）-O-，-Si（CH 3）（R 17）-O-Si（CH 3）（R 18） - ，5-（2-羟乙基） - [1,3,5] 2,4,6-三酮-1,3-二基和/或1-9个氧原子。

9. 发明申请

US20100104979A1 ALPHA-HYDROXYKETONES 有权
标题翻译：阿尔法羟基酮
公开(公告)号：US20100104979A1
公开(公告)日：2010-04-29
申请号：US12593025
申请日：2008-03-25
申请人： Kurt Dietliker , Peter Murer , Rinaldo Hüsler , Tunja Jung
发明人： Kurt Dietliker , Peter Murer , Rinaldo Hüsler , Tunja Jung
IPC分类号： G03F7/20 , C07C59/76 , C07D307/00 , C07D305/12 , C07F7/08 , C07D265/30 , C07C69/95 , C07D211/06 , C07C233/00 , G03F7/004 , C08F2/46
CPC分类号： C07D211/32 , C07C49/83 , C07C49/835 , C07C49/84 , C07C62/38 , C07C69/757 , C07C219/12 , C07C235/82 , C07C2601/14 , C07D295/185 , C07D305/12 , C07F7/0836 , C07F7/0838 , C07F7/1804 , G03F7/004 , G03F7/38 , G03F7/40
摘要： Compounds of the Formula (I) wherein x is an integer from 1-4; p is an integer from 1-3; q is an integer from 0-3; Ar is phenyl, naphthyl, anthryl or phenanthryl each of which optionally is substituted by one or more Cl, CN, OR5, C3-C5alkenyl or C1-C6alkyl which optionally is substituted by one or more OR6, COOR or halogen; R1 if x is 1, is ORS, O—X+, NR8R9, C1-C20alkyl optionally substituted by one or more COOR10, or is C2-C20alkyl interrupted by one ore more O, or is C2-C5alkenyl or phenyl-C1-C4alkyl; R1 if x is 2, is for example C1-C20alkylene; R1 if x is 3, is for example a tri-valent radical; R1if x is 4, is for example a tetravalent radical; R2and R3are hydrogen or C1-C8alkyl, or R2and R3 together are O, C1-C3alkylene or CH═CH; R4 is C1-C4alkyl; R5, R6, R7, R8, R9 and R10 are for example hydrogen or C1-C4alkyl; and X is a x-valent cationic counter ion; are in particular suitable as photoinitiators for the curing with UV-A light (320-450 nm).
摘要翻译：式（I）的化合物，其中x是1-4的整数; p是1-3的整数; q是0-3的整数; Ar是苯基，萘基，蒽基或菲基，其各自任选被一个或多个被一个或多个OR 6，COOR或卤素取代的C 1，CN，OR 5，C 3 -C 5链烯基或C 1 -C 6烷基取代; R 1如果x是1，是ORS，O-X +，NR 8 R 9，任选被一个或多个COOR 10取代的C 1 -C 20烷基，或是被一个或多个O取代的C 2 -C 20烷基，或者是C 2 -C 5烯基或苯基-C 1 -C 4烷基; R1如果x为2，例如为C 1 -C 20亚烷基; 如果x是3，则R1是例如三价基; R1if x为4，例如为四价基团; R 2和R 3为氢或C 1 -C 8烷基，或R 2和R 3一起为O，C 1 -C 3亚烷基或CH = CH; R4是C1-C4烷基; R5，R6，R7，R8，R9和R10是例如氢或C1-C4烷基; X为x-阳离子抗衡离子; 特别适用于用UV-A光（320-450nm）固化的光引发剂。

10. 发明授权

US07588880B2 Incorporable photoinitiator 有权
标题翻译：可并入的光引发剂
公开(公告)号：US07588880B2
公开(公告)日：2009-09-15
申请号：US10512300
申请日：2003-04-17
申请人： Jean-Pierre Wolf , Rinaldo Hüsler , Wolfgang Peter , Reinhard H. Sommerlade , Souâd Boulmaâz
发明人： Jean-Pierre Wolf , Rinaldo Hüsler , Wolfgang Peter , Reinhard H. Sommerlade , Souâd Boulmaâz
IPC分类号： G03C1/73 , G03C1/735 , G03F7/028 , C08F2/50 , C07C49/12
CPC分类号： C08F2/50 , B33Y70/00
摘要： Compounds of formula I Y is, for example, C3-C12alkylene, butenylene, butynylene, or C4-C12alkylene interrupted one or more times by non-consecutive —O— or —NR2—; R1 is a reactive group selected from OH, SH, NR3R4, —(CO)—OH, —(CO)—NH2, SO3H, —C(R5)═CR6R7, oxiranyl, —O—(CO)—NH—R8—NCO and —O—(CO)—R9—(CO)—X; R2 is hydrogen, C1-C4alkyl or C2-C4hydroxyalkyl; R3 and R4 are each independently of the other hydrogen, C1-C4alkyl or C2-C4hydroxyalkyl; R5, R6 and R7 are each independently of the others hydrogen or methyl; R8 is, for example, linear or branched C4-C12alkylene, or phenylene; R9 is, for example, linear or branched C1-C16alkylene, —CH═CH—, —CH═CH—CH2—, C6-cycloalkylene, phenylene or naphthylene; and X, X1 and X2 are each independently of the others OH, Cl, OCH3 or OC2H5; are suitable as photoinitiators that can be incorporated in a formulation to be cured.
摘要翻译：式I Y的化合物是例如C 3 -C 12亚烷基，亚丁烯基，亚丁炔基或C 4 -C 12亚烷基被非连续的-O-或-NR 2 - 间隔一次或多次; R1是选自OH，SH，NR3R4， - （CO）-OH， - （CO）-NH2，SO3H，-C（R5）-CR6R7，环氧乙烷基，-O-（CO）-NH-R8- NCO和-O-（CO）-R9-（CO）-X; R2是氢，C1-C4烷基或C2-C4羟烷基; R 3和R 4各自独立地为氢，C 1 -C 4烷基或C 2 -C 4羟烷基; R5，R6和R7各自独立地为氢或甲基; R8是例如直链或支链C 4 -C 12亚烷基或亚苯基; R 9为例如直链或支链C 1 -C 16亚烷基，-CH-CH-，-CH-CH-CH 2 - ，C 6 - 亚环烷基，亚苯基或亚萘基; X，X 1和X 2各自独立地为OH，Cl，OCH 3或OC 2 H 5; 适合作为可引入待固化制剂中的光引发剂。

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